The Optical Properties of Crystalline Zn3Nb2O8 Nanomaterials Obtained by Hydrothermal Method

The present study is focused on the obtaining of the Zn3Nb2O8 nanomaterial using the hydrothermal method and its characterization through different techniques. X-ray diffraction at room temperature revealed that a novel crystalline form of the nanomaterial forms at 1100°C belonging to monoclinic spa...

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Main Authors: Mihaela Birdeanu, Mirela Vaida, Eugenia Fagadar-Cosma
Format: Article
Language:English
Published: Wiley 2015-01-01
Series:Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2015/752089
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author Mihaela Birdeanu
Mirela Vaida
Eugenia Fagadar-Cosma
author_facet Mihaela Birdeanu
Mirela Vaida
Eugenia Fagadar-Cosma
author_sort Mihaela Birdeanu
collection DOAJ
description The present study is focused on the obtaining of the Zn3Nb2O8 nanomaterial using the hydrothermal method and its characterization through different techniques. X-ray diffraction at room temperature revealed that a novel crystalline form of the nanomaterial forms at 1100°C belonging to monoclinic space group C2/c. Field-emission scanning electron microscopy evidenced the columnar morphology of the particle’s agglomeration and the high resolution electron transmission microscopy confirms the measured interplanar distances calculated from the X-ray diffraction experiments. Using the UV-VIS spectrum and Kubelka-Munk equations, the absorbance and the band gap for the Zn3Nb2O8 nanomaterial were calculated. PL spectrum reveals a single peak at 465 nm corresponding to the blue color fluorescence. The novel crystalline nanomaterial might find applications in fluorescence covering of technical devices, due to its capacity to preserve blue fluorescence both in acrylic based paint and after embedding in isopropyl alcohol.
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institution Kabale University
issn 2090-9063
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language English
publishDate 2015-01-01
publisher Wiley
record_format Article
series Journal of Chemistry
spelling doaj-art-d6da1aebc65a40d5b7291b790f4d35552025-02-03T06:08:15ZengWileyJournal of Chemistry2090-90632090-90712015-01-01201510.1155/2015/752089752089The Optical Properties of Crystalline Zn3Nb2O8 Nanomaterials Obtained by Hydrothermal MethodMihaela Birdeanu0Mirela Vaida1Eugenia Fagadar-Cosma2Politehnica University of Timisoara, Vasile Parvan Avenue 6, 300223 Timisoara, RomaniaPolitehnica University of Timisoara, Vasile Parvan Avenue 6, 300223 Timisoara, RomaniaInstitute of Chemistry Timisoara of Romanian Academy, 24 M. Viteazu Avenue, 300223 Timisoara, RomaniaThe present study is focused on the obtaining of the Zn3Nb2O8 nanomaterial using the hydrothermal method and its characterization through different techniques. X-ray diffraction at room temperature revealed that a novel crystalline form of the nanomaterial forms at 1100°C belonging to monoclinic space group C2/c. Field-emission scanning electron microscopy evidenced the columnar morphology of the particle’s agglomeration and the high resolution electron transmission microscopy confirms the measured interplanar distances calculated from the X-ray diffraction experiments. Using the UV-VIS spectrum and Kubelka-Munk equations, the absorbance and the band gap for the Zn3Nb2O8 nanomaterial were calculated. PL spectrum reveals a single peak at 465 nm corresponding to the blue color fluorescence. The novel crystalline nanomaterial might find applications in fluorescence covering of technical devices, due to its capacity to preserve blue fluorescence both in acrylic based paint and after embedding in isopropyl alcohol.http://dx.doi.org/10.1155/2015/752089
spellingShingle Mihaela Birdeanu
Mirela Vaida
Eugenia Fagadar-Cosma
The Optical Properties of Crystalline Zn3Nb2O8 Nanomaterials Obtained by Hydrothermal Method
Journal of Chemistry
title The Optical Properties of Crystalline Zn3Nb2O8 Nanomaterials Obtained by Hydrothermal Method
title_full The Optical Properties of Crystalline Zn3Nb2O8 Nanomaterials Obtained by Hydrothermal Method
title_fullStr The Optical Properties of Crystalline Zn3Nb2O8 Nanomaterials Obtained by Hydrothermal Method
title_full_unstemmed The Optical Properties of Crystalline Zn3Nb2O8 Nanomaterials Obtained by Hydrothermal Method
title_short The Optical Properties of Crystalline Zn3Nb2O8 Nanomaterials Obtained by Hydrothermal Method
title_sort optical properties of crystalline zn3nb2o8 nanomaterials obtained by hydrothermal method
url http://dx.doi.org/10.1155/2015/752089
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