Sonochemical Synthesis of Silver Nanoparticles Using Starch: A Comparison
A novel approach was applied to synthesize silver nanoparticles using starch under sonication. Colloidal silver nanoparticles solution exhibited an increase of absorption from 420 to 440 nm with increase starch quantity. Transmission electron microscopy followed by selected area electron diffraction...
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Format: | Article |
Language: | English |
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Wiley
2014-01-01
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Series: | Bioinorganic Chemistry and Applications |
Online Access: | http://dx.doi.org/10.1155/2014/784268 |
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author | Brajesh Kumar Kumari Smita Luis Cumbal Alexis Debut Ravinandan Nath Pathak |
author_facet | Brajesh Kumar Kumari Smita Luis Cumbal Alexis Debut Ravinandan Nath Pathak |
author_sort | Brajesh Kumar |
collection | DOAJ |
description | A novel approach was applied to synthesize silver nanoparticles using starch under sonication. Colloidal silver nanoparticles solution exhibited an increase of absorption from 420 to 440 nm with increase starch quantity. Transmission electron microscopy followed by selected area electron diffraction pattern analysis indicated the formation of spherical, polydispersed, amorphous, silver nanoparticles of diameter ranging from 23 to 97 nm with mean particle size of 45.6 nm. Selected area electron diffraction (SAED) confirmed partial crystalline and amorphous nature of silver nanoparticles. Silver nanoparticles synthesized in this manner can be used for synthesis of 2-aryl substituted benzimidazoles which have numerous biomedical applications. The optimized reaction conditions include 10 ml of 1 mM AgNO3, 25 mg starch, 11 pH range, and sonication for 20 min at room temperature. |
format | Article |
id | doaj-art-d2e8776a3fed4e2db57ddb1d5262fbef |
institution | Kabale University |
issn | 1565-3633 1687-479X |
language | English |
publishDate | 2014-01-01 |
publisher | Wiley |
record_format | Article |
series | Bioinorganic Chemistry and Applications |
spelling | doaj-art-d2e8776a3fed4e2db57ddb1d5262fbef2025-02-03T01:24:07ZengWileyBioinorganic Chemistry and Applications1565-36331687-479X2014-01-01201410.1155/2014/784268784268Sonochemical Synthesis of Silver Nanoparticles Using Starch: A ComparisonBrajesh Kumar0Kumari Smita1Luis Cumbal2Alexis Debut3Ravinandan Nath Pathak4Centro de Nanociencia y Nanotecnologia, Universidad de las Fuerzas Armadas (ESPE), Sangolqui, EcuadorCentro de Nanociencia y Nanotecnologia, Universidad de las Fuerzas Armadas (ESPE), Sangolqui, EcuadorCentro de Nanociencia y Nanotecnologia, Universidad de las Fuerzas Armadas (ESPE), Sangolqui, EcuadorCentro de Nanociencia y Nanotecnologia, Universidad de las Fuerzas Armadas (ESPE), Sangolqui, EcuadorDepartment of Chemistry, Kolhan University, Chaibasa, Jharkhand 833202, IndiaA novel approach was applied to synthesize silver nanoparticles using starch under sonication. Colloidal silver nanoparticles solution exhibited an increase of absorption from 420 to 440 nm with increase starch quantity. Transmission electron microscopy followed by selected area electron diffraction pattern analysis indicated the formation of spherical, polydispersed, amorphous, silver nanoparticles of diameter ranging from 23 to 97 nm with mean particle size of 45.6 nm. Selected area electron diffraction (SAED) confirmed partial crystalline and amorphous nature of silver nanoparticles. Silver nanoparticles synthesized in this manner can be used for synthesis of 2-aryl substituted benzimidazoles which have numerous biomedical applications. The optimized reaction conditions include 10 ml of 1 mM AgNO3, 25 mg starch, 11 pH range, and sonication for 20 min at room temperature.http://dx.doi.org/10.1155/2014/784268 |
spellingShingle | Brajesh Kumar Kumari Smita Luis Cumbal Alexis Debut Ravinandan Nath Pathak Sonochemical Synthesis of Silver Nanoparticles Using Starch: A Comparison Bioinorganic Chemistry and Applications |
title | Sonochemical Synthesis of Silver Nanoparticles Using Starch: A Comparison |
title_full | Sonochemical Synthesis of Silver Nanoparticles Using Starch: A Comparison |
title_fullStr | Sonochemical Synthesis of Silver Nanoparticles Using Starch: A Comparison |
title_full_unstemmed | Sonochemical Synthesis of Silver Nanoparticles Using Starch: A Comparison |
title_short | Sonochemical Synthesis of Silver Nanoparticles Using Starch: A Comparison |
title_sort | sonochemical synthesis of silver nanoparticles using starch a comparison |
url | http://dx.doi.org/10.1155/2014/784268 |
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