Development and validation of fluoroquinolone detection method in chicken eggs using high-performance liquid chromatography
The method for the simultaneous detection of nine fluoroquinolone antibiotics (marbofloxacin, ofloxacin, pefloxacin, norfloxacin, ciprofloxacin, enrofloxacin, danofloxacin, sarafloxacin and difloxacin) in chicken eggs using high-performance liquid chromatography with fluorescence detection was devel...
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Da Vinci Media
2018-04-01
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| Series: | Ветеринария сегодня |
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| Online Access: | https://veterinary.arriah.ru/jour/article/view/229 |
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| author | A. A. Lugovskoy D. S. Bolshakov T. B. Nikeshina |
| author_facet | A. A. Lugovskoy D. S. Bolshakov T. B. Nikeshina |
| author_sort | A. A. Lugovskoy |
| collection | DOAJ |
| description | The method for the simultaneous detection of nine fluoroquinolone antibiotics (marbofloxacin, ofloxacin, pefloxacin, norfloxacin, ciprofloxacin, enrofloxacin, danofloxacin, sarafloxacin and difloxacin) in chicken eggs using high-performance liquid chromatography with fluorescence detection was developed. The detected range of fluoroquinolones is from 10 to 100 μg/kg in a 4g sample. Based on the validation studies the combined standard uncertainty and relative expanded uncertainty were calculated. The technique enables to detect antibiotic residues in their admissible levels equal to 100 μg/kg, in compliance with SanPiN 2.3.2.2804-10 and Common sanitary-epidemiological and hygienic requirements to the goods subject to sanitary and epidemiological surveillance (control). |
| format | Article |
| id | doaj-art-a68094024305443dad8b4c420921c634 |
| institution | Kabale University |
| issn | 2304-196X 2658-6959 |
| language | English |
| publishDate | 2018-04-01 |
| publisher | Da Vinci Media |
| record_format | Article |
| series | Ветеринария сегодня |
| spelling | doaj-art-a68094024305443dad8b4c420921c6342025-02-06T09:52:05ZengDa Vinci MediaВетеринария сегодня2304-196X2658-69592018-04-01013037229Development and validation of fluoroquinolone detection method in chicken eggs using high-performance liquid chromatographyA. A. Lugovskoy0D. S. Bolshakov1T. B. Nikeshina2FGBI "ARRIAH", VladimirFGBI "ARRIAH", VladimirFGBI "ARRIAH", VladimirThe method for the simultaneous detection of nine fluoroquinolone antibiotics (marbofloxacin, ofloxacin, pefloxacin, norfloxacin, ciprofloxacin, enrofloxacin, danofloxacin, sarafloxacin and difloxacin) in chicken eggs using high-performance liquid chromatography with fluorescence detection was developed. The detected range of fluoroquinolones is from 10 to 100 μg/kg in a 4g sample. Based on the validation studies the combined standard uncertainty and relative expanded uncertainty were calculated. The technique enables to detect antibiotic residues in their admissible levels equal to 100 μg/kg, in compliance with SanPiN 2.3.2.2804-10 and Common sanitary-epidemiological and hygienic requirements to the goods subject to sanitary and epidemiological surveillance (control).https://veterinary.arriah.ru/jour/article/view/229фторхинолоныантибиотикикуриные яйцавысокоэффективная жидкостная хроматографияфлуориметрическое детектированиевалидацияfluoroquinolonesantibioticschicken eggshigh-performance liquid chromatographyfluorescence detectionvalidation |
| spellingShingle | A. A. Lugovskoy D. S. Bolshakov T. B. Nikeshina Development and validation of fluoroquinolone detection method in chicken eggs using high-performance liquid chromatography Ветеринария сегодня фторхинолоны антибиотики куриные яйца высокоэффективная жидкостная хроматография флуориметрическое детектирование валидация fluoroquinolones antibiotics chicken eggs high-performance liquid chromatography fluorescence detection validation |
| title | Development and validation of fluoroquinolone detection method in chicken eggs using high-performance liquid chromatography |
| title_full | Development and validation of fluoroquinolone detection method in chicken eggs using high-performance liquid chromatography |
| title_fullStr | Development and validation of fluoroquinolone detection method in chicken eggs using high-performance liquid chromatography |
| title_full_unstemmed | Development and validation of fluoroquinolone detection method in chicken eggs using high-performance liquid chromatography |
| title_short | Development and validation of fluoroquinolone detection method in chicken eggs using high-performance liquid chromatography |
| title_sort | development and validation of fluoroquinolone detection method in chicken eggs using high performance liquid chromatography |
| topic | фторхинолоны антибиотики куриные яйца высокоэффективная жидкостная хроматография флуориметрическое детектирование валидация fluoroquinolones antibiotics chicken eggs high-performance liquid chromatography fluorescence detection validation |
| url | https://veterinary.arriah.ru/jour/article/view/229 |
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