Development and validation of fluoroquinolone detection method in chicken eggs using high-performance liquid chromatography
The method for the simultaneous detection of nine fluoroquinolone antibiotics (marbofloxacin, ofloxacin, pefloxacin, norfloxacin, ciprofloxacin, enrofloxacin, danofloxacin, sarafloxacin and difloxacin) in chicken eggs using high-performance liquid chromatography with fluorescence detection was devel...
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| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
| Published: |
Da Vinci Media
2018-04-01
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| Series: | Ветеринария сегодня |
| Subjects: | |
| Online Access: | https://veterinary.arriah.ru/jour/article/view/229 |
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| Summary: | The method for the simultaneous detection of nine fluoroquinolone antibiotics (marbofloxacin, ofloxacin, pefloxacin, norfloxacin, ciprofloxacin, enrofloxacin, danofloxacin, sarafloxacin and difloxacin) in chicken eggs using high-performance liquid chromatography with fluorescence detection was developed. The detected range of fluoroquinolones is from 10 to 100 μg/kg in a 4g sample. Based on the validation studies the combined standard uncertainty and relative expanded uncertainty were calculated. The technique enables to detect antibiotic residues in their admissible levels equal to 100 μg/kg, in compliance with SanPiN 2.3.2.2804-10 and Common sanitary-epidemiological and hygienic requirements to the goods subject to sanitary and epidemiological surveillance (control). |
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| ISSN: | 2304-196X 2658-6959 |