Synthesis and Characterization of Copper(II)-Oxide Nanoparticles from Two Cu(II) Coordination Polymers
CuO nano particles were obtained by calcination of nano-sized [Cu(C4H4O4)(bipy)(H2O)2].2H2O (1) and [Cu(2‚2′-bipy)](C4H4O4)0.5(NO3)(H2O) (2) which are two Cu(II) coordination polymers. The two coordination polymers [Cu(C4H4O4)(bipy)(H2O)2].2H2O and [Cu(2‚2′-bipy)](C4H4O4)0.5(NO3)(H2O) were synthes...
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| Main Authors: | , |
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| Format: | Article |
| Language: | English |
| Published: |
University of Tehran
2016-04-01
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| Series: | Journal of Sciences, Islamic Republic of Iran |
| Subjects: | |
| Online Access: | https://jsciences.ut.ac.ir/article_56997_3a49598bff6cd56bd0be06de99f593e0.pdf |
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| Summary: | CuO nano particles were obtained by calcination of nano-sized [Cu(C4H4O4)(bipy)(H2O)2].2H2O (1) and [Cu(2‚2′-bipy)](C4H4O4)0.5(NO3)(H2O) (2) which are two Cu(II) coordination polymers. The two coordination polymers [Cu(C4H4O4)(bipy)(H2O)2].2H2O and [Cu(2‚2′-bipy)](C4H4O4)0.5(NO3)(H2O) were synthesized and characterized by Fourier transform infrared spectra (FT-IR spectroscopy), thermal gravimetric (TGA) and differential thermal analyses (DTA). CuO nano particles were characterized by X-ray powder diffraction (XRD) and scanning electron microscopy (SEM).The two coordination polymers obtained possessed nano sizes. |
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| ISSN: | 1016-1104 2345-6914 |