Semiempirical Efficiency Calibration in Semiconductor HPGe Gamma-Ray Spectroscopy

One of the main problems in quantitative gamma-ray spectroscopy is the determination of detection efficiency, for different energies, source-detector geometries, and composition of samples or sources. There are, in principle, three approaches to this issue: experimental, numerical, and semiempirical...

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Main Authors: Jelena Krneta Nikolić, Milica Rajačić, Dragana Todorović, Marija Janković, Nataša Sarap, Gordana Pantelić, Ivana Vukanac
Format: Article
Language:English
Published: Wiley 2018-01-01
Series:Journal of Spectroscopy
Online Access:http://dx.doi.org/10.1155/2018/5392658
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author Jelena Krneta Nikolić
Milica Rajačić
Dragana Todorović
Marija Janković
Nataša Sarap
Gordana Pantelić
Ivana Vukanac
author_facet Jelena Krneta Nikolić
Milica Rajačić
Dragana Todorović
Marija Janković
Nataša Sarap
Gordana Pantelić
Ivana Vukanac
author_sort Jelena Krneta Nikolić
collection DOAJ
description One of the main problems in quantitative gamma-ray spectroscopy is the determination of detection efficiency, for different energies, source-detector geometries, and composition of samples or sources. There are, in principle, three approaches to this issue: experimental, numerical, and semiempirical. Semiempirical approach is based on the calculation of the efficiency for the measured sample on the basis of an experimental efficiency measured on the same detector, but with a calibration source that can be of different size, geometry, density, or composition—the so-called efficiency transfer. The aim of this paper is to analyze the semiempirical approach, using EFFTRAN and MEFFTRAN software as a typical example. These software were used in the Department of Radiation and Environmental Protection, Vinča Institute of Nuclear Sciences, on three HPGe detectors. The results were compared to the experimentally obtained efficiency, and further validation is performed by measuring reference materials issued within the framework of several interlaboratory intercomparisons. The analysis of the results showed that the efficiency transfer produces good results with the discrepancies within the limits of the measurement uncertainty. Also, for intercomparison measurement, utest criterion for the trueness of the result was applied showing that the majority of the obtained results were acceptable. Some difficulties were identified, and the ways to overcome them were discussed.
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issn 2314-4920
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spelling doaj-art-9bc838c8e42644d8a3d0afce70e9804a2025-02-03T01:24:06ZengWileyJournal of Spectroscopy2314-49202314-49392018-01-01201810.1155/2018/53926585392658Semiempirical Efficiency Calibration in Semiconductor HPGe Gamma-Ray SpectroscopyJelena Krneta Nikolić0Milica Rajačić1Dragana Todorović2Marija Janković3Nataša Sarap4Gordana Pantelić5Ivana Vukanac6Institute of Nuclear Sciences “Vinča”, University of Belgrade, Mike Petrovica Alasa 12-16, 11001 Belgrade, SerbiaInstitute of Nuclear Sciences “Vinča”, University of Belgrade, Mike Petrovica Alasa 12-16, 11001 Belgrade, SerbiaInstitute of Nuclear Sciences “Vinča”, University of Belgrade, Mike Petrovica Alasa 12-16, 11001 Belgrade, SerbiaInstitute of Nuclear Sciences “Vinča”, University of Belgrade, Mike Petrovica Alasa 12-16, 11001 Belgrade, SerbiaInstitute of Nuclear Sciences “Vinča”, University of Belgrade, Mike Petrovica Alasa 12-16, 11001 Belgrade, SerbiaInstitute of Nuclear Sciences “Vinča”, University of Belgrade, Mike Petrovica Alasa 12-16, 11001 Belgrade, SerbiaInstitute of Nuclear Sciences “Vinča”, University of Belgrade, Mike Petrovica Alasa 12-16, 11001 Belgrade, SerbiaOne of the main problems in quantitative gamma-ray spectroscopy is the determination of detection efficiency, for different energies, source-detector geometries, and composition of samples or sources. There are, in principle, three approaches to this issue: experimental, numerical, and semiempirical. Semiempirical approach is based on the calculation of the efficiency for the measured sample on the basis of an experimental efficiency measured on the same detector, but with a calibration source that can be of different size, geometry, density, or composition—the so-called efficiency transfer. The aim of this paper is to analyze the semiempirical approach, using EFFTRAN and MEFFTRAN software as a typical example. These software were used in the Department of Radiation and Environmental Protection, Vinča Institute of Nuclear Sciences, on three HPGe detectors. The results were compared to the experimentally obtained efficiency, and further validation is performed by measuring reference materials issued within the framework of several interlaboratory intercomparisons. The analysis of the results showed that the efficiency transfer produces good results with the discrepancies within the limits of the measurement uncertainty. Also, for intercomparison measurement, utest criterion for the trueness of the result was applied showing that the majority of the obtained results were acceptable. Some difficulties were identified, and the ways to overcome them were discussed.http://dx.doi.org/10.1155/2018/5392658
spellingShingle Jelena Krneta Nikolić
Milica Rajačić
Dragana Todorović
Marija Janković
Nataša Sarap
Gordana Pantelić
Ivana Vukanac
Semiempirical Efficiency Calibration in Semiconductor HPGe Gamma-Ray Spectroscopy
Journal of Spectroscopy
title Semiempirical Efficiency Calibration in Semiconductor HPGe Gamma-Ray Spectroscopy
title_full Semiempirical Efficiency Calibration in Semiconductor HPGe Gamma-Ray Spectroscopy
title_fullStr Semiempirical Efficiency Calibration in Semiconductor HPGe Gamma-Ray Spectroscopy
title_full_unstemmed Semiempirical Efficiency Calibration in Semiconductor HPGe Gamma-Ray Spectroscopy
title_short Semiempirical Efficiency Calibration in Semiconductor HPGe Gamma-Ray Spectroscopy
title_sort semiempirical efficiency calibration in semiconductor hpge gamma ray spectroscopy
url http://dx.doi.org/10.1155/2018/5392658
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