Preparation and Gas-Sensitive Properties of Square–Star-Shaped Leaf-Like BiVO<sub>4</sub> Nanomaterials

In this study, square–star-shaped leaf-like BiVO<sub>4</sub> nanomaterials were successfully synthesized using a conventional hydrothermal method. The microstructure, elemental composition, and gas-sensing performance of the materials were thoroughly investigated. Morphological analysis...

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Main Authors: Jin Liu, Mengdi Yang, Yuanyuan Lv, Yixin Gao, Danyang Bai, Neng Li, Haoru Guo, Anyi Wang
Format: Article
Language:English
Published: MDPI AG 2025-01-01
Series:Nanomaterials
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Online Access:https://www.mdpi.com/2079-4991/15/2/127
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author Jin Liu
Mengdi Yang
Yuanyuan Lv
Yixin Gao
Danyang Bai
Neng Li
Haoru Guo
Anyi Wang
author_facet Jin Liu
Mengdi Yang
Yuanyuan Lv
Yixin Gao
Danyang Bai
Neng Li
Haoru Guo
Anyi Wang
author_sort Jin Liu
collection DOAJ
description In this study, square–star-shaped leaf-like BiVO<sub>4</sub> nanomaterials were successfully synthesized using a conventional hydrothermal method. The microstructure, elemental composition, and gas-sensing performance of the materials were thoroughly investigated. Morphological analysis revealed that BiVO<sub>4</sub> prepared at different reaction temperatures exhibited square–star-shaped leaf-like structures, with the most regular and dense structures formed at 150 °C, exhibiting a large specific surface area of 2.84 m<sup>2</sup>/g. The response performance of the BiVO<sub>4</sub> gas sensors to different target gases was evaluated, and the results showed that the prepared BiVO<sub>4</sub> gas sensor exhibited a strong response to NH<sub>3</sub>. At the optimal operating temperature of 300 °C, its sensitivity to 5 ppm NH<sub>3</sub> reached 13.3, with a response time of 28 s and a recovery time of 16 s. Moreover, the gas sensor exhibited excellent repeatability and anti-interference performance. These findings indicate that square–star-shaped leaf-like BiVO<sub>4</sub> holds great potential in environmental monitoring and industrial safety detection, offering new insights for the development of high-performance gas sensors.
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institution Kabale University
issn 2079-4991
language English
publishDate 2025-01-01
publisher MDPI AG
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series Nanomaterials
spelling doaj-art-7b56cc30004a4f4da4420aced4d849d22025-01-24T13:44:14ZengMDPI AGNanomaterials2079-49912025-01-0115212710.3390/nano15020127Preparation and Gas-Sensitive Properties of Square–Star-Shaped Leaf-Like BiVO<sub>4</sub> NanomaterialsJin Liu0Mengdi Yang1Yuanyuan Lv2Yixin Gao3Danyang Bai4Neng Li5Haoru Guo6Anyi Wang7School of Communication and Information Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaSchool of Communication and Information Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaSchool of Communication and Information Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaSchool of Communication and Information Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaSchool of Communication and Information Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaSchool of Communication and Information Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaSchool of Communication and Information Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaSchool of Communication and Information Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaIn this study, square–star-shaped leaf-like BiVO<sub>4</sub> nanomaterials were successfully synthesized using a conventional hydrothermal method. The microstructure, elemental composition, and gas-sensing performance of the materials were thoroughly investigated. Morphological analysis revealed that BiVO<sub>4</sub> prepared at different reaction temperatures exhibited square–star-shaped leaf-like structures, with the most regular and dense structures formed at 150 °C, exhibiting a large specific surface area of 2.84 m<sup>2</sup>/g. The response performance of the BiVO<sub>4</sub> gas sensors to different target gases was evaluated, and the results showed that the prepared BiVO<sub>4</sub> gas sensor exhibited a strong response to NH<sub>3</sub>. At the optimal operating temperature of 300 °C, its sensitivity to 5 ppm NH<sub>3</sub> reached 13.3, with a response time of 28 s and a recovery time of 16 s. Moreover, the gas sensor exhibited excellent repeatability and anti-interference performance. These findings indicate that square–star-shaped leaf-like BiVO<sub>4</sub> holds great potential in environmental monitoring and industrial safety detection, offering new insights for the development of high-performance gas sensors.https://www.mdpi.com/2079-4991/15/2/127BiVO<sub>4</sub> nanomaterialshydrothermal methodgas-sensing performancegas sensorammonia
spellingShingle Jin Liu
Mengdi Yang
Yuanyuan Lv
Yixin Gao
Danyang Bai
Neng Li
Haoru Guo
Anyi Wang
Preparation and Gas-Sensitive Properties of Square–Star-Shaped Leaf-Like BiVO<sub>4</sub> Nanomaterials
Nanomaterials
BiVO<sub>4</sub> nanomaterials
hydrothermal method
gas-sensing performance
gas sensor
ammonia
title Preparation and Gas-Sensitive Properties of Square–Star-Shaped Leaf-Like BiVO<sub>4</sub> Nanomaterials
title_full Preparation and Gas-Sensitive Properties of Square–Star-Shaped Leaf-Like BiVO<sub>4</sub> Nanomaterials
title_fullStr Preparation and Gas-Sensitive Properties of Square–Star-Shaped Leaf-Like BiVO<sub>4</sub> Nanomaterials
title_full_unstemmed Preparation and Gas-Sensitive Properties of Square–Star-Shaped Leaf-Like BiVO<sub>4</sub> Nanomaterials
title_short Preparation and Gas-Sensitive Properties of Square–Star-Shaped Leaf-Like BiVO<sub>4</sub> Nanomaterials
title_sort preparation and gas sensitive properties of square star shaped leaf like bivo sub 4 sub nanomaterials
topic BiVO<sub>4</sub> nanomaterials
hydrothermal method
gas-sensing performance
gas sensor
ammonia
url https://www.mdpi.com/2079-4991/15/2/127
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