Preparation of Improved p-n Junction NiO/TiO2 Nanotubes for Solar-Energy-Driven Light Photocatalysis

Self-organized TiO2 nanotubes (TNTs) with average inner diameter of 109 nm, wall thickness of 15 nm, and tube length of 7–10 μm were loaded with nickel oxide (NiO) nanoparticles via incipient wet impregnation method. The molar concentration of Ni(NO3)2·6H2O aqueous solution varied in a range of 0.5 ...

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Main Authors: Lan Ching Sim, Kai Wern Ng, Shaliza Ibrahim, Pichiah Saravanan
Format: Article
Language:English
Published: Wiley 2013-01-01
Series:International Journal of Photoenergy
Online Access:http://dx.doi.org/10.1155/2013/659013
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author Lan Ching Sim
Kai Wern Ng
Shaliza Ibrahim
Pichiah Saravanan
author_facet Lan Ching Sim
Kai Wern Ng
Shaliza Ibrahim
Pichiah Saravanan
author_sort Lan Ching Sim
collection DOAJ
description Self-organized TiO2 nanotubes (TNTs) with average inner diameter of 109 nm, wall thickness of 15 nm, and tube length of 7–10 μm were loaded with nickel oxide (NiO) nanoparticles via incipient wet impregnation method. The molar concentration of Ni(NO3)2·6H2O aqueous solution varied in a range of 0.5 M–2.5 M. The samples were characterized for crystalline phase, morphology, topography, chemical composition, Raman shift, and UV-Vis diffusion reflection properties. The finding shows that the loading of NiO did not influence the morphology, structure, and crystalline phase of TNTs but it exhibited significant effect on crystallite size and optical absorption properties. Further, the solar-energy-driven the photocatalytic activity of NiO/TNTs and pure TNTs was evaluated by degrading methylene blue (MB). The results confirm that photocatalytic efficiency of NiO/TNTs is higher than that of TNTs.
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institution Kabale University
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publishDate 2013-01-01
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spelling doaj-art-5ac7b24b2ad147e3ac735bbd0c28a97e2025-02-03T05:54:09ZengWileyInternational Journal of Photoenergy1110-662X1687-529X2013-01-01201310.1155/2013/659013659013Preparation of Improved p-n Junction NiO/TiO2 Nanotubes for Solar-Energy-Driven Light PhotocatalysisLan Ching Sim0Kai Wern Ng1Shaliza Ibrahim2Pichiah Saravanan3Environmental Engineering Laboratory, Department of Civil Engineering, Faculty of Engineering, University of Malaya, 50603 Kuala Lumpur, MalaysiaEnvironmental Engineering Laboratory, Department of Civil Engineering, Faculty of Engineering, University of Malaya, 50603 Kuala Lumpur, MalaysiaEnvironmental Engineering Laboratory, Department of Civil Engineering, Faculty of Engineering, University of Malaya, 50603 Kuala Lumpur, MalaysiaEnvironmental Engineering Laboratory, Department of Civil Engineering, Faculty of Engineering, University of Malaya, 50603 Kuala Lumpur, MalaysiaSelf-organized TiO2 nanotubes (TNTs) with average inner diameter of 109 nm, wall thickness of 15 nm, and tube length of 7–10 μm were loaded with nickel oxide (NiO) nanoparticles via incipient wet impregnation method. The molar concentration of Ni(NO3)2·6H2O aqueous solution varied in a range of 0.5 M–2.5 M. The samples were characterized for crystalline phase, morphology, topography, chemical composition, Raman shift, and UV-Vis diffusion reflection properties. The finding shows that the loading of NiO did not influence the morphology, structure, and crystalline phase of TNTs but it exhibited significant effect on crystallite size and optical absorption properties. Further, the solar-energy-driven the photocatalytic activity of NiO/TNTs and pure TNTs was evaluated by degrading methylene blue (MB). The results confirm that photocatalytic efficiency of NiO/TNTs is higher than that of TNTs.http://dx.doi.org/10.1155/2013/659013
spellingShingle Lan Ching Sim
Kai Wern Ng
Shaliza Ibrahim
Pichiah Saravanan
Preparation of Improved p-n Junction NiO/TiO2 Nanotubes for Solar-Energy-Driven Light Photocatalysis
International Journal of Photoenergy
title Preparation of Improved p-n Junction NiO/TiO2 Nanotubes for Solar-Energy-Driven Light Photocatalysis
title_full Preparation of Improved p-n Junction NiO/TiO2 Nanotubes for Solar-Energy-Driven Light Photocatalysis
title_fullStr Preparation of Improved p-n Junction NiO/TiO2 Nanotubes for Solar-Energy-Driven Light Photocatalysis
title_full_unstemmed Preparation of Improved p-n Junction NiO/TiO2 Nanotubes for Solar-Energy-Driven Light Photocatalysis
title_short Preparation of Improved p-n Junction NiO/TiO2 Nanotubes for Solar-Energy-Driven Light Photocatalysis
title_sort preparation of improved p n junction nio tio2 nanotubes for solar energy driven light photocatalysis
url http://dx.doi.org/10.1155/2013/659013
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AT kaiwernng preparationofimprovedpnjunctionniotio2nanotubesforsolarenergydrivenlightphotocatalysis
AT shalizaibrahim preparationofimprovedpnjunctionniotio2nanotubesforsolarenergydrivenlightphotocatalysis
AT pichiahsaravanan preparationofimprovedpnjunctionniotio2nanotubesforsolarenergydrivenlightphotocatalysis