REGENERATION OF ION-EXCHANGE CATALYST BY SUPERCRITICAL FLUID EXTRACTION PROCESS
Supercritical fluid extraction regeneration of the ion-exchange KU-2FPP catalyst is investigated. Results of change of mass of the catalyst are presented during regeneration at T = 383-393 K and P = 15-25 MPa and IR spectrums of chloroformic extracts of the studied catalyst samples. Results of the c...
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| Main Authors: | , , , , , |
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| Format: | Article |
| Language: | English |
| Published: |
Kazan State Power Engineering University
2018-03-01
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| Series: | Известия высших учебных заведений: Проблемы энергетики |
| Subjects: | |
| Online Access: | https://www.energyret.ru/jour/article/view/444 |
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| Summary: | Supercritical fluid extraction regeneration of the ion-exchange KU-2FPP catalyst is investigated. Results of change of mass of the catalyst are presented during regeneration at T = 383-393 K and P = 15-25 MPa and IR spectrums of chloroformic extracts of the studied catalyst samples. Results of the conducted researches allow to draw a conclusion on effective removal of polar and unpolar organic compounds. However the collateral reaction connected with emergence of dialkylphthalate is a probable cause of inefficiency of regeneration process with participation of SC-CO2 as the extractant. And use supercritical propane - butane mix (T = 393 K, P = 10-15 MPa) as the supercritical extractant allows to restore activity of the catalyst to the level meeting the requirements of industrial use. |
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| ISSN: | 1998-9903 |