Synthesis and crystal structure of 5,10-bis(phenylsulfonyl)tetrahydrodibenzopentalene

Synthesis and crystal structure of 5,10-bis(phenylsulfonyl)tetrahydrodibenzopentalene

5,10-Bis(phenylsulfonyl)tetrahydrodibenzopentalene, C28H22O4S2, 1, was successfully synthesized via the photocatalyst-promoted hydrogenative transannulation of disulfonylcyclooctatetraene, 2, using perylene as the photocatalyst in the presence of (i-Pr)2NEt under UV-light irradiation (398 nm, 30 W)....

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Bibliographic Details
Main Authors: Toshiki Sakami, Hikaru Watanabe, Takuma Sato, Yasuhiro Okuda, Kan Wakamatsu, Haruo Akashi, Akihiro Orita
Format: Article
Language:English
Published: International Union of Crystallography 2025-02-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
transannulation
ethenyl sulfone
hydrogenation
tetrahydrodibenzopentalene
Online Access:https://journals.iucr.org/paper?S205698902500060X
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