Shynthesis and Characterizations of Calcium Hydroxyapatite Derived from Crabs Shells (Portunus pelagicus) and Its Potency in Safeguard against to Dental Demineralizations

Crab’s shells of Portunus pelagicus species were used as raw materials for synthesis of hydroxyapatite were used for protection against demineralization of teeth. Calcination was conducted to crab’s shells of Portunus pelagicus at temperature of 1000°C for 5 hours. The results of calcination was rea...

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Main Authors: Indah Raya, Erna Mayasari, Afdaliah Yahya, Muhammad Syahrul, Andi Ilham Latunra
Format: Article
Language:English
Published: Wiley 2015-01-01
Series:International Journal of Biomaterials
Online Access:http://dx.doi.org/10.1155/2015/469176
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author Indah Raya
Erna Mayasari
Afdaliah Yahya
Muhammad Syahrul
Andi Ilham Latunra
author_facet Indah Raya
Erna Mayasari
Afdaliah Yahya
Muhammad Syahrul
Andi Ilham Latunra
author_sort Indah Raya
collection DOAJ
description Crab’s shells of Portunus pelagicus species were used as raw materials for synthesis of hydroxyapatite were used for protection against demineralization of teeth. Calcination was conducted to crab’s shells of Portunus pelagicus at temperature of 1000°C for 5 hours. The results of calcination was reacted with (NH4)2HPO4, then dried at 110°C for 5 hours. Sintering was conducted to results of precipitated dried with temperature variations 400–1000°C for a hour each variation of temperature then characterized by X-ray diffractometer and FTIR in order to obtain the optimum formation temperature of hydroxyapatite is 800°C. The hydroxyapatite is then tested its effectiveness in protection against tooth demineralization using acetate buffer pH 5.0 with 1 M acetic acid concentration with the addition of hydroxyapatite and time variation of immersion. The results showed that the rate of tooth demineralization in acetate buffer decreased significantly with the provision of hydroxyapatite into a solution where the addition of the magnitude of hydroxyapatite is greater decrease in the rate of tooth demineralization.
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language English
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spelling doaj-art-31a5701cf94e43b29b6d6b2190d2ea6a2025-08-20T02:38:55ZengWileyInternational Journal of Biomaterials1687-87871687-87952015-01-01201510.1155/2015/469176469176Shynthesis and Characterizations of Calcium Hydroxyapatite Derived from Crabs Shells (Portunus pelagicus) and Its Potency in Safeguard against to Dental DemineralizationsIndah Raya0Erna Mayasari1Afdaliah Yahya2Muhammad Syahrul3Andi Ilham Latunra4Chemistry Department, Faculty of Mathematics and Natural Sciences, Hasanuddin University, Makassar 90245, IndonesiaChemistry Department, Faculty of Mathematics and Natural Sciences, Hasanuddin University, Makassar 90245, IndonesiaChemistry Department, Faculty of Mathematics and Natural Sciences, Hasanuddin University, Makassar 90245, IndonesiaChemistry Department, Faculty of Mathematics and Natural Sciences, Hasanuddin University, Makassar 90245, IndonesiaBiology Department, Faculty of Mathematics and Natural Sciences, Hasanuddin University, Makassar 90245, IndonesiaCrab’s shells of Portunus pelagicus species were used as raw materials for synthesis of hydroxyapatite were used for protection against demineralization of teeth. Calcination was conducted to crab’s shells of Portunus pelagicus at temperature of 1000°C for 5 hours. The results of calcination was reacted with (NH4)2HPO4, then dried at 110°C for 5 hours. Sintering was conducted to results of precipitated dried with temperature variations 400–1000°C for a hour each variation of temperature then characterized by X-ray diffractometer and FTIR in order to obtain the optimum formation temperature of hydroxyapatite is 800°C. The hydroxyapatite is then tested its effectiveness in protection against tooth demineralization using acetate buffer pH 5.0 with 1 M acetic acid concentration with the addition of hydroxyapatite and time variation of immersion. The results showed that the rate of tooth demineralization in acetate buffer decreased significantly with the provision of hydroxyapatite into a solution where the addition of the magnitude of hydroxyapatite is greater decrease in the rate of tooth demineralization.http://dx.doi.org/10.1155/2015/469176
spellingShingle Indah Raya
Erna Mayasari
Afdaliah Yahya
Muhammad Syahrul
Andi Ilham Latunra
Shynthesis and Characterizations of Calcium Hydroxyapatite Derived from Crabs Shells (Portunus pelagicus) and Its Potency in Safeguard against to Dental Demineralizations
International Journal of Biomaterials
title Shynthesis and Characterizations of Calcium Hydroxyapatite Derived from Crabs Shells (Portunus pelagicus) and Its Potency in Safeguard against to Dental Demineralizations
title_full Shynthesis and Characterizations of Calcium Hydroxyapatite Derived from Crabs Shells (Portunus pelagicus) and Its Potency in Safeguard against to Dental Demineralizations
title_fullStr Shynthesis and Characterizations of Calcium Hydroxyapatite Derived from Crabs Shells (Portunus pelagicus) and Its Potency in Safeguard against to Dental Demineralizations
title_full_unstemmed Shynthesis and Characterizations of Calcium Hydroxyapatite Derived from Crabs Shells (Portunus pelagicus) and Its Potency in Safeguard against to Dental Demineralizations
title_short Shynthesis and Characterizations of Calcium Hydroxyapatite Derived from Crabs Shells (Portunus pelagicus) and Its Potency in Safeguard against to Dental Demineralizations
title_sort shynthesis and characterizations of calcium hydroxyapatite derived from crabs shells portunus pelagicus and its potency in safeguard against to dental demineralizations
url http://dx.doi.org/10.1155/2015/469176
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