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2421
Improving the Physical Properties of Nanofibers Prepared by Electrospinning from Polyvinyl Chloride and Polyacrylonitrile at Low Concentrations
Published 2023-01-01“…For the investigation of the homogeneity and compatibility of mixture polymer solutions, it is examined by rheological properties such as viscosity, shear stress, shear rate, and calculation of the flow behavior index, while the investigation of the stability and high density of nanofibers without beads used field-emission scanning electron microscopy (FE-SEM), Fourier transform near-infrared spectroscopy (FT-NIR), X-ray diffraction (XRD), and differential scanning calorimetry-thermogravimetric analysis (DSC-TGA). The results show that blending of PAN with PVC leads to improving of the electro spun ability of PVC with more stability, and the mean nanofiber diameter was 90.873±40.82 nm at 25 : 75 PVC: PAN. …”
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2422
Synthesis, DNA-Binding, Anticancer Evaluation, and Molecular Docking Studies of Bishomoleptic and Trisheteroleptic Ru-Diimine Complexes Bearing 2-(2-Pyridyl)-quinoxaline
Published 2021-01-01“…The complexes were characterized by elemental analysis, TGA, 1H-NMR, FT-IR, UV-Vis, emission spectroscopy, and electrochemistry. …”
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2423
Preparation of quaternary ammonium-modified silica and its adsorption of vanadium(V)
Published 2025-01-01“…In this study, a quaternary ammonium modified silica(SiO2@DMOA) material was synthesized for the adsorption of vanadium(Ⅴ) in aqueous solution. The results of TGA, FT-IR, SEM, and EDS confirmed the successful synthesis of SiO2@DMOA composite. …”
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2424
Synthesis, Characterization, and Cytotoxicity Research of Sulfur-Containing Metal Complexes
Published 2025-01-01“…The structure of the complex was analyzed using infrared Fourier transform infrared spectroscopy (FT-IR), ultraviolet–visible spectroscopy (UV–Vis), nuclear magnetic resonance (NMR), and electrospray mass spectrometry (ESI-MS), and the thermal stability and composition of the complex were detected via thermogravimetry (TGA). In terms of application, the biological activity of complexes (I)–(III) in human cancer cell lines (lung cancer A549, liver cancer SMMC-7721, breast cancer MDA-MB-231, and colon cancer SW480) was tested using the MTS method. …”
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2425
Greener Synthesis, Characterization, and Antimicrobiological Effects of Helba Silver Nanoparticle-PMMA Nanocomposite
Published 2019-01-01“…Modification of thermal stabilities of AgNP/PMMA nanocomposites was confirmed using thermogravimetric analysis (TGA). The green AgNP/PMMA nanocomposites showed improved thermal stabilities. …”
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2426
Investigation of Characteristics Whey Protein Isolate/Chitosan with Silica Addition in Biocomposite Film
Published 2025-01-01“…The functional groups, morphology, structure, mechanical, thermal, and transparency of the biocomposite films were evaluated by Fourier transform infrared (FTIR) spectroscopy, Scanning electron microscope (SEM), X-ray diffraction (XRD), tensile strength, thermogravimetric (TGA), differential scanning calorimetry (DSC), thickness, swelling, and UV-Vis. …”
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2427
The Effect of Active Chitosan Films Containing Bacterial Cellulose Nanofiber and ZnO Nanoparticles on the Shelf Life of Loaf Bread
Published 2023-01-01“…Differential scanning calorimetric (DSC), thermal gravimetry analysis (TGA), and derivative thermogravimetry (DTG) showed that ZnO NPCs increased the thermal stability of chitosan films. …”
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2428
Silybin Cocrystals with Improved Solubility and Bioavailability
Published 2025-01-01“…<b>Methods:</b> Silybin-L-proline cocrystal was synthesized and the physicochemical properties of the cocrystal were characterized by PXRD, TGA, DSC, and FTIR. Dissolution tests were conducted in various pH solutions, and the impact of precipitation inhibitors was evaluated. …”
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2429
Structure and Electrochemical Behavior of Minor Mn-Doped Olivine LiMnxFe1−xPO4
Published 2019-01-01“…The synthesized olivines were well crystallized in olivine structure, with larger lattice parameters compared with LiFePO4. The EXD and TGA results confirmed the coated carbon of 4.14% for LiMn0.1Fe0.9PO4 and 6.86% for LiMn0.2Fe0.8PO4. …”
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2430
Optimization of COD removal of raw landfill leachate using the magnetic graphene oxide/WO3 nanocomposite: Isotherms, kinetics, and thermodynamics studies
Published 2023-11-01“…The obtained products were characterized using X-ray diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR), Scanning Electron Microscopy (SEM), Thermogravimetric analysis (TGA), and Vibrating sample magnetometer (VSM) analysis. …”
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2431
Fabrication of a Porous Metal-Organic Framework with Polar Channels for 5-Fu Delivery and Inhibiting Human Osteosarcoma Cells
Published 2018-01-01“…The structure of the obtained crystalline product has been fully determined by the X-ray single-crystal diffraction, TGA, elemental analysis, XRD, and the gas sorption measurement. …”
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2432
Facile grafting method achieves Unprecedented dispersion stability of carbon black in PP fiber
Published 2025-02-01“…Characterization techniques (FTIR, XPS, Raman, TGA, etc.) confirm successful grafting and demonstrate excellent dispersion stability of modified CB in organic media. …”
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2433
Design of Highly Porous Materials Based on Chitosan/Pectin Interpolyelectrolyte Complex for Wound Healing Application
Published 2024-01-01“…The chitosan-/aldehyde-functionalized pectin (Chit/AF-Pect) polyelectrolyte complex sponges obtained are characterized using SEM, FTIR spectroscopy, and TGA. The swelling capacity study reveals a higher swelling ratio of IPEC sponges with an increase in both the molecular weight and content of chitosan: for Chit30/AF-Pect, the swelling ratio rises from 327% to 480%, while for Chit1200/AF-Pect, from 681% to 1,066%. …”
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2434
Preparation and characterization of jute cellulose nanocrystals using tetrabutylammonium fluoride and dimethyl sulfoxide solutions
Published 2025-01-01“…The crystallinity was measured at 79.14% for scoured and 73.59% for bleached jute CNCs. TGA results indicated suitable thermal stability of the produced jute CNCs, demonstrating stability up to 210°C before starting cellulose decomposition. …”
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2435
Removal of the Textile Dye Indanthrene Olive Green from Aqueous Solution Using Chitosan
Published 2009-12-01“…The chitosan was characterised in terms of its average degree of de-acetylation (DD) and by XRD, TGA/DTG, IR, SEM and specific BET surface area methods. …”
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2436
Green adsorbents for water remediation: Removal of Cr(vi) and Ni(ii) using Prosopis glandulosa sawdust and biochar
Published 2025-01-01“…Both the adsorbents were characterized via SEM, FTIR spectroscopy, EDX, and TGA and were applied for the effective removal of Ni(ii) and Cr(vi) at optimum values of experimental conditions, and the mechanism was assessed via adsorption isotherm and kinetic models. …”
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2437
Synthesis and Spectroscopic Studies of Axially Ligated Zn(II)5,10,15,20-meso-tetra(p-chlorophenyl)porphyrin with Oxygen and Nitrogen Donors
Published 2013-01-01“…The four-coordinated zinc porphyrin accepts one axial ligand in 1 : 1 molar ratio to form five-coordinated complex, which is purified by column chromatography and characterized by IR spectra, 1H NMR, electronic absorption spectra, elemental analysis, mass spectroscopy, and TGA/DTA studies. IR spectra confirms the appearance of Zn– at 500–400 cm−1, Zn– at 650–570 cm−1 and Zn–O at 650–350 cm−1. 1H NMR spectra show that the protons of the Phenolic ring axially attached to the central metal ion are merged with the protons of the tetraphenyl rings of the porphyrin moiety. …”
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2438
Mechanochemical Functionalization of Oxidized Carbon Black with PLA
Published 2024-12-01“…The functionalized carbon black (f-CB) was characterized by Fourier transform infrared spectroscopy (FTIR), elemental analysis (EA), and thermogravimetric analysis (TGA) to confirm the successful modification. At the same time, the influence of f-CB as a nanofiller of residual PLA waste was evaluated using differential scanning calorimetry (DSC) and gel permeation chromatography (GPC), demonstrating its stabilization effect during melt extrusion by preserving the molecular weight of the starting polymer. …”
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2439
Synthesis, Spectral Characterization, and Thermal and Cytotoxicity Studies of Cr(III), Ru(III), Mn(II), Co(II), Ni(II), Cu(II), and Zn(II) Complexes of Schiff Base Derived from 5-H...
Published 2018-01-01“…Elemental analytical data, IR, NMR (1H, 13C, and 15N), EPR, XRD, SEM, TEM, EDX, TGA, mass, molar conductance, magnetic moment, and UV-Visible spectra techniques were used to confirm the structure of the synthesized chelates. …”
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2440
Improving the Performance and Biodegradability of Biocomposites Made from Banana Sap and Banana Fibres
Published 2024-01-01“…We used thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), scanning electron microscopy (SEM), and Fourier transform infrared (FTIR) spectroscopy for the physicochemical characterisation of BSMF before and after composting and measured carbon dioxide evolved during the biodegradation to calculate biodegradability. …”
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