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3801
Green synthesis and characterization of CuO/ZnO nanocomposite using Musa acuminata leaf extract for cytotoxic studies on colorectal cancer cells (HCC2998)
Published 2024-12-01“…Fourier transform infrared spectroscopy analysis showed the presence of functional groups, including hydroxyl groups, carbonyl groups, amines, alkanes, aromatic amines, Cu–O, and Zn–O. …”
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3802
The high value utilization characteristics of coal gangue powder with emulsified asphalt mastic through rheological and viscoelastic damage theory
Published 2025-01-01“…A series of tests, including frequency scanning, temperature scanning, Multiple Stress Creep Recovery (MSCR), Linear Amplitude Scanning (LAS), and Fourier Transform Infrared spectroscopy (FTIR) were conducted. Through rheology theory, viscoelastic damage theory, the impact of three fillers: Coal Gangue Powder (CGP), Limestone Powder (LP) and Portland Cement (PC), as well as four kinds of Powder-Binder ratios (P/B) (0.6, 0.9, 1.2, 1.5) on the high temperature rheology and medium temperature fatigue performance of EAM was analyzed. …”
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3803
Loading monocytes with magnetic nanoparticles enables their magnetic control without toxicity
Published 2025-01-01“…Finally, we compared and confirmed the experimentally generated magnetic enrichment data with computational simulations.Methods and resultsWhen THP-1 cells were incubated with citrate-coated SPIONs (SPIONCitrate) or citrate-stabilized gold-coated SPIONs (SPIONGold), cells ingested the particles, as determined via transmission electron microscopy and atomic emission spectroscopy. Flow cytometry showed that the particles were biocompatible and produced hardly any ROS. …”
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3804
Effect of Ionic Liquid Surfactants on Coal Oxidation and Structure
Published 2019-01-01“…The effects of six ionic liquids with surfactant property (1-hydroxyethyl-3-methyl imidazolium bis(trifluoromethylsulfonyl)imide ([HOEtMIm][NTf2]), 1-hydroxyethyl-3-methyl imidazolium tetrafluoroborate ([HOEtMIm][BF4]), 1-dodecyl-3- methyl imidazolium bromide ([C12MIm]Br), 1-tetradecyl-3- methyl imidazolium bromide ([C14MIm]Br), trioctyl methyl ammonium chloride ([N8,8,8,1])Cl, and tetraethyl ammonium chloride ([N2,2,2,2]Cl)) on the oxidation characteristics and functional groups of coal were studied by means of critical micelle concentration, surface tension, thermogravimetric analysis, temperature-programmed oxidation, and Fourier transform infrared spectroscopy (FTIR) measurements. The lower critical micelle concentration for the ionic liquids except the [N2,2,2,2]Cl suggests the favorable surface activity of these ionic liquids. …”
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3805
Asparagus officinalis polysaccharide-loaded liposomal gels alleviate skin inflammation via inhibiting the NF-κB/MAPK pathways
Published 2025-02-01“…WAPS, a pectin polysaccharide, was identified to coexist with α-glycosidic and β-glycosidic linkages glucan and probably has triple-helix confirmation suggested by Fourier-transform infrared and nuclear magnetic resonance spectroscopy. Cellular experiments indicated that WAPS attenuated the expression of inflammatory cytokines and enhanced macrophage viability. …”
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3806
Small- to Large-Scale Electron Beam Powder Bed Fusion of Functionally Graded Steels
Published 2024-12-01“…For the microstructural analysis, optical microscopy, scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy (EDX) were performed on the polished cross-sections. …”
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3807
Comparative Analysis of Chemical Composition and Antibacterial Activity of Essential Oils from Five Varieties of <i>Lavender</i> Extracted via Supercritical Fluid Extraction
Published 2025-01-01“…This study aimed to determine the chemical composition of five <i>Lavender</i> essential oils (LEOs) using the gas chromatography–mass spectroscopy technique and to assess their antibacterial activity against four marine <i>Vibrio</i> species, including <i>Shewanella algae</i>, <i>Shewanella maridflavi</i>, <i>Vibrio harveyi</i>, and <i>Vibrio alginolyticus</i>. …”
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3808
Boosting effect of ultrasonication on the oxygen evolution reaction during zinc electrowinning
Published 2025-01-01“…Electrochemical impedance spectroscopy (EIS), cyclic voltammetry (CV), linear sweep voltammetry (LSV), and zinc electrowinning tests were conducted to analyze the electrochemical behavior of the Pb-Ag anodes during zinc electrowinning. …”
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3809
Reversible multivalent carrier redox exceeding intercalation capacity boundary
Published 2025-01-01“…Operando X-ray absorption spectroscopy, operando synchrotron X-ray diffraction and composite ex situ characterization jointly demonstrated that intercalated divalent copper is preferentially involved in redox afforded extra electron transfer to form reversible monovalent copper pillars, thus not only ensuring stable topological de/intercalation with high capacity but also sustaining fast migration kinetic paths through reconfigurable pillar effects. …”
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3810
Structural and electronic features enabling delocalized charge-carriers in CuSbSe 2
Published 2025-01-01“…Herein, CuSbSe2 is investigated and discovered to have delocalized free carriers, as shown through optical pump terahertz probe spectroscopy and temperature-dependent mobility measurements. …”
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3811
Gelatin/PLA-loaded gold nanocomposites synthesis using Syzygium cumini fruit extract and their antioxidant, antibacterial, anti-inflammatory, antidiabetic and anti-Alzheimer’s acti...
Published 2025-01-01“…This innovative study synthesizes and characterizes Ge/PLA/AuNCs (gelatin/PLA/gold nanocomposites) using Syzygium cumini extract to evaluate their various biomedical applications. The UV–Visible spectroscopy results in an absorption peak at 534 nm were primarily confirmed by Ge/PLA/AuNCs synthesis. …”
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3812
An Evaluation of the Biocompatibility and Chemical Properties of Two Bioceramic Root Canal Sealers in a Sealer Extrusion Model of Rat Molars
Published 2025-01-01“…The elemental composition and chemical composition of the extruded EBC and NBG were analyzed at Day 1 and 28 using an electron probe microanalyzer and micro-Raman spectroscopy. No periapical lesions were observed with the sealer extrusion. …”
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3813
Studies on the Effect of Laser Shock Peening Intensity on the Mechanical Properties of Wire Arc Additive Manufactured SS316L
Published 2024-12-01“…Energy dispersive spectroscopy (EDS) analysis confirmed the formation of an oxide layer post-LSP, with an increase in carbon (C) and oxygen (O) elements and a decrease in chromium (Cr) and nickel (Ni) elements on the surface, attributed to localized pressure and heat impacts. …”
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3814
A New Nanocomposite for Inducing Demineralized Dentin Remineralization
Published 2025-02-01“…The solution underwent comprehensive characterization using various techniques, including Fourier Transform Infrared Spectroscopy (FTIR), X-Ray Diffraction (XRD), Transmission Electron Microscopy (TEM), STEM-EDX mapping, and Selected Area Electron Diffraction (SAED). …”
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3815
Photochemistry Aspects of the Laser Pyrolysis Addressing the Preparation of Oxide Semiconductor Photocatalysts
Published 2008-01-01“…Temperature-dependent Mossbauer spectroscopy shows that mainly maghemite is present in the sample obtained at higher laser power. …”
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3816
Recent advances in detection techniques for vitamin analysis: A comprehensive review
Published 2025-02-01“…Here, we propose a comprehensive and critical evaluation of detection methods for water- and fat-soluble vitamins that have been studied over the past five years, including microbiology-, spectroscopy-, liquid chromatography–mass spectrometry-, electrochemistry-, sensor-, and immunoassay-based analysis techniques. …”
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3817
Comprehensive Evaluation of Quality Characteristics and Processing Suitability of Different Varieties of Large-fruited Sea Buckthorn Juice from Xinjiang Using Multivariate Analysis...
Published 2025-02-01“…This study assessed the quality characteristics juice and processing suitability of six varieties of large-fruited sea buckthorn juice from Xinjiang using gas chromatography-ion mobility spectroscopy (GC-IMS) and multivariate physicochemical analysis combined with correlation and principal component analysis. …”
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3818
Source and Ecological Risk Assessment of Potentially Toxic Metals in Urban Riverine Sediments Using Multivariate Analytical and Statistical Tools
Published 2024-12-01“…Additionally, techniques such as X-ray Diffraction (XRD) and Scanning Electron Microscopy–Energy Dispersive X-ray Spectroscopy (SEM-EDS) were employed to investigate the mineralogical and morphological aspects. …”
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3819
Advancement of eco-friendly slag-based high-strength geopolymer concrete
Published 2025-01-01“…Scanning electron microscope (SEM) and energy dispersive X-ray (EDX) spectroscopy analyses were performed on selected HSGC mixes. …”
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3820
Synthesis and Advanced NMR Characterization of Ordered 3D Reticular Materials with PolySilicate Nodes and Hydrophobic OrganoSilicone Linkers
Published 2025-01-01“…Advanced solid-state NMR spectroscopy allowed us to unravel the molecular order of the nodes and their interconnection by the silicone linkers. …”
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