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1101
The transport of polyphenols from Camellia fascicularis in Caco-2 cells based on UPLC-ESI-MS/MS
Published 2025-01-01“…Herein, digestion samples (DS) of C. fascicularis polyphenols (CFPs) were metabolically analyzed based on their bidirectional translocation in Caco-2 cells using ultraperformance liquid chromatography-electrospray ionization-tandem mass spectrometry. The results indicated that after DS transported via Caco-2 cell monolayer models nine polyphenol compounds in transit solution (TSB) from apical (AP) to basolateral (BL) side were upregulated, whereas seven in the transit solution (TSA) from BL to AP side were upregulated. …”
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1102
Interaction of human neutrophils with Trichomonas vaginalis protozoan highlights lactoferrin secretion
Published 2025-02-01“…We conducted a comprehensive profiling of soluble excretory/secretory proteins (ESPs), identifying 192 protein spots, of which 94 were successfully characterized through mass spectrometry analysis. Notably, the majority of induced ESPs from co-cultivation exhibited consistency with the trichomonad and neutrophil standalone groups, except for lactoferrin, which was observed exclusively following the interaction between neutrophils and T. vaginalis. …”
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1103
A new portable sampler of atmospheric methane for radiocarbon measurements
Published 2025-01-01“…In this study, we address this challenge by advancing the system in Zazzeri et al. (2021) into a much more compact and portable sampler and by coupling the sampler with the MICADAS (MIni CArbon DAting System) accelerator mass spectrometry (AMS) system at ETH Zurich, using a gas interface.…”
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1104
Two Cysteines in Raf Kinase Inhibitor Protein Make Differential Contributions to Structural Dynamics In Vitro
Published 2025-01-01“…Mutation of alanine or serine instead of cysteine in RKIP proteins did not affect the biochemical characteristics, while dynamic light scattering and liquid chromatography (LC) quadrupole time-of-flight (Q-TOF) mass spectrometry (MS) suggested distinct peaks in solution, which were identified via LC–MS/MS analyses, and further clarified the role of cysteine in RKIP dimerization. rhRKIP dimer formation was abrogated by a 32-aa peptide mimicking the region between two RKIP proteins for dimerization. …”
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1105
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1106
Tracing the Origin of Oxide Inclusions in Vacuum Arc Remelted Steel Ingots Using Trace Element Profiles and Strontium Isotope Ratios
Published 2025-01-01“…In this study, the potential of elemental and isotopic fingerprinting to trace the sources of macroscopic oxide NMIs found in VAR-treated steel ingots using SEM-EDX, inductively coupled plasma mass spectrometry (ICP-MS), laser ablation ICP-MS (LA-ICP-MS), and laser ablation multicollector ICP-MS (LA-MC-ICP-MS) were exploited. …”
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1107
Seasonal Changes in the Elemental Composition of Five Valuable Fish Species (<i>Sparidae</i>) from Bozcaada, North Aegean Sea: A Health Risk and Nutritional Benefit Assessment
Published 2025-01-01“…The concentrations of elements such as calcium, potassium, magnesium, phosphorus, copper, iron, manganese, zinc, chromium, nickel, selenium, cadmium, and mercury were analyzed using Inductively Coupled Plasma Mass Spectrometry (ICP-MS). The elemental concentrations varied as follows: Ca (11,388.46–55,470.76), K (17,230.83–27,594.86), Mg (1436.02–2326.73), Na (1962.30–7847.41), P (13,112.11–15,516.57), Fe (107.61–282.00), Cu (36.44–59.13), Mn (6.19–19.87), Zn (98.67–256.26), Cr (4.54–11.96), Ni (6.33–13.89), Se (0.82–7.33), Cd (0.08–0.32), and Hg (0.08–1.50) mg/kg. …”
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1108
Predictive value of bile acids as metabolite biomarkers for gallstone disease: A systematic review and meta-analysis.
Published 2024-01-01“…The level of serum DCA in the GSD patients was found to be increased by using chromatography, yet decreased by chromatography mass spectrometry.<h4>Conclusion</h4>The profiles of BAs demonstrated distinctive changes in GSD patients compared with healthy control subjects. …”
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1109
Novel Insights into the Nobilamide Family from a Deep-Sea <i>Bacillus</i>: Chemical Diversity, Biosynthesis and Antimicrobial Activity Towards Multidrug-Resistant Bacteria
Published 2025-01-01“…The integration of tandem mass spectrometry molecular networking and bioassay-guided fractionation unveiled this strain as a prolific factory of surfactins and nobilamides. …”
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1110
The concentration of selected organophosphorus pesticides associated with PM10 in agricultural ambient air in Iran: Health risk assessment using Monte Carlo simulation
Published 2025-01-01“…Active sampling was conducted using a SKC pump with a selective air inlet, and the samples were analyzed via liquid chromatography-mass spectrometry. The results indicated that Diazinon exhibited the highest average concentration among PM10-bound organophosphate pesticides, measuring 4.23 ng/m³ in suburban areas and 2.51 ng/m³ in urban environments. …”
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1111
Betaxanthin Profiling in Beta vulgaris Leaves and Gymnocalycium mihanovichii Grafted Cacti: A Comprehensive Study
Published 2023-12-01“…This study was focused on the identification and quantification of betaxanthins using high-performance liquid chromatography with a diode array detector coupled to electrospray ionisation mass spectrometry (HPLC-DAD-ESI-MS) in leaves of various cultivars of Beta vulgaris (beet) and Gymnocalycium mihanovichi i grafted cacti. …”
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1112
Comparative analysis of phytonutrients of Moringa oleifera leaves from South Africa and Nigeria, and their antimicrobial and antioxidant potentials by UPLC-ESI-QToF-MS and OPLS-DA...
Published 2025-01-01“…This study aimed to conduct a comparative analysis of the phytonutrients (nutrients protectors) or supplements, antioxidant, and antimicrobial potentials of M. oleifera leaves from Nigeria and South Africa to benchmark quality control protocols for commercial beverages such as Moringa porridge.MethodsStandard techniques, including high-performance liquid chromatography-photodiode array and ultra-high-performance liquid chromatography electrospray ionization quadruple time-of-flight mass spectrometry (UPLC-ESI-QToF-MS) and chemometrics orthogonal partial least square discriminant analysis (OPLS-DA) were employed for phytoconstituents fingerprinting. …”
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1113
Differences in central dopamine, but not serotonin, activity and welfare associated with age but not with preening cup use in commercial grow-out Pekin duck barns
Published 2025-01-01“…To evaluate the ducks’ affective state, we combined measuring welfare by walking a transect in the barn with mass spectrometry and qRT-PCR to measure brain neurotransmitter levels and gene expression for serotonin (5-HT) and dopamine (DA) synthesis and metabolism. 5-HT and DA have been established as indicators of mental state and emotions. …”
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1114
Antibiotic exposure is associated with minimal gut microbiome perturbations in healthy term infants
Published 2025-01-01“…Here, we use a prospective longitudinal birth cohort of n = 323 healthy term African American children to determine the association between antibiotic exposure and the gut microbiome through shotgun metagenomics sequencing as well as bile acid profiles through liquid chromatography-mass spectrometry. Results Stool samples were collected at ages 4, 12, and 24 months for antibiotic-exposed (n = 170) and unexposed (n = 153) participants. …”
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1115
Differential GTP-dependent in-vitro polymerization of recombinant Physcomitrella FtsZ proteins
Published 2025-01-01“…Here, we investigated the interaction of Physcomitrella FtsZ2-1 with FtsZ1 isoforms via co-immunoprecipitation and mass spectrometry, and found protein-protein interaction in vivo. …”
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1116
Phenotypic plasticity vs. local genetic adaptation: essential oil diversity of natural immortelle (Helichrysum italicum (Roth.) G.Don) populations along eastern Adriatic coast
Published 2025-02-01“…Eighteen natural immortelle populations were sampled, hydrodistilled and their essential oil composition determined by gas chromatography-mass spectrometry. A total of 84 compounds were identified. …”
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1117
Influence of Hydrodistillation Conditions on Yield and Composition of Coriander (Coriandrum sativum L.) Essential Oil
Published 2018-09-01“…The composition of the coriander essential oil was determined by using gas chromatography with mass spectrometry (GC-MS). The main components were linalool (78.45%), α-pinene (5.03%), camphor (3.90%), γ-terpinene (3.80%), D-limonene (2.58%) and geranyl acetate (2.13%). …”
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1118
Hyperandrogenism, Elevated 17-Hydroxyprogesterone and Its Urinary Metabolites in a Young Woman with Ovarian Steroid Cell Tumor, Not Otherwise Specified: Case Report and Review of t...
Published 2019-01-01“…While a diagnosis of polycystic ovary syndrome (PCOS) with its associated metabolic disturbances was initially considered, serum total testosterone, androstenedione, and 17-hydroxyprogesterone (17-OHP) measured by liquid chromatography tandem mass spectrometry (LC-MS/MS) were significantly increased. …”
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1119
The effect of trace minerals on the stability of retinol acetate, cholecalciferol and selenomethionine stability within premixes
Published 2021-05-01“…The SeMet content of the two SeMet-trace mineral premixes was analysed after 49 days in storage by high performance liquid chromatography – inductively coupled plasma mass spectrometry and the amount of SeMet present within each of the samples was compared to the quantity determined prior to storage. …”
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1120
Subchronic Exposure to Low-Dose Chlorfenapyr and Emamectin Benzoate Disrupts Kidney Metabolism in Rats
Published 2025-01-01“…Kidney metabolome alterations were analyzed by using gas chromatography–mass spectrometry. The results showed that combined exposure to CFP and EMB elevated BUN levels and induced pathological damage, which presented as thinner renal tubular epithelial cells, an abnormal glomerular morphology, and an increased fibrotic area. …”
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