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241
Simultaneous Quantification of Aspirin, Its Metabolite Salicylic Acid, and Salvianolic Acid B in Human Plasma Using UPLC-MS/MS
Published 2021-01-01“…The analytes and internal standard were extracted from the acidified plasma by liquid-liquid extraction with ethyl acetate and then separated by gradient elution with acetonitrile/0.5% formic acid in water on a C18 column. …”
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242
Impact of Pretreatment and Drying Factors on Chemical and Biochemical Attributes of Moroccan Thompson Seedless Grapes
Published 2023-01-01“…Also, in these conditions, a lower browning rate (14.48%), a lower 5-hydroxymethylfurfural content (12.40 mg/100 g DW), and a higher level of polyphenols (135.79±13.17 mg GAE/100 g DW) and flavonoid content (57.81±3.08 mg Qeq/100 g DW) have been recorded while meeting international standards for SO2 content and microbial quality.…”
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243
Development and Validation of Analytical Procedure for Elemental Impurities in Rosuvastatin Calcium Tablets by ICP-MS and Microwave Digestion
Published 2024-01-01“…The measurement mode was collision cell mode with kinetic energy discrimination (KED). 209Bi+, 115In+, and 89Y+ were chosen as internal standard elements. The recoveries of the limit of quantitation (LOQ) ranged from 90.5% to 106.4%, concentrations of the abovementioned elements in LOQ were 0.25 µg·L−1, 0.25 µg·L−1, 0.75 µg·L−1, 1.5 µg·L−1, 2.5 µg·L−1, 5 µg·L−1, and 8 µg·L−1 , respectively, linear correlation coefficients were above 0.9997, the recoveries in accuracy item ranged from 91.8% to 103.6%, and relative standard deviations (RSDs) of recovery in precision were not more than 1.8%, reflecting a reliable method of high sensitivity, strong anti-interference capacity, and good precision, and that it was suitable for the determination of elemental impurities in drugs.…”
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244
Diagnosis and Treatment of Low Anterior Resection Syndrome
Published 2025-01-01“…., which is a patient-reported outcome measure to evaluate the severity of bowel dysfunction following rectal surgery by scoring the major symptoms of LARS, facilitates the diagnosis and assessment of LARS and enables international comparison and validation through the use of validated scores generated according to the international standards. Based on comparisons with other evaluation instruments, the use of the LARS score is strongly recommended internationally for LARS screening in patients following rectal resection. …”
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245
Validation of Colchicine Assay Method for Therapeutic Drug Monitoring in Human Plasma
Published 2022-12-01“…In our study, to 1ml plasma sample, 0.25 ml internal standard solution was added. The solution was extracted by liquid-liquid extraction (LLE). …”
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246
Optimization of the suspension procedure by Box-Behnken design for the determination of manganese, iron, and zinc in zeolite clinoptilolite with the TXRF system and insight into it...
Published 2024-12-01“…Based on the results obtained, sample suspensions were prepared by weighing 10 mg of the sample and adding 1 mL of 5 % Triton X-100 with 10 mL Ga as internal standard and deposition volume was set at 10 mL. …”
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247
Production and characterization of biodiesel from Argemone mexicana seed oil
Published 2025-01-01“…Overall, the results suggest that A. mexicana oil is a viable and sustainable feedstock for biodiesel production, with fuel properties that meet international standards for biodiesel use.…”
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248
The Effect of Solar Panels and Vegetation Strategy on the Sustainability of Open Spaces
Published 2024-12-01“…The results revealed a decrease in (PET) by (8.32) degrees Celsius, which achieved international standards for outdoor pedestrian comfort. As well as shading areas less exposed to sunlight with trees, in addition to providing shade to protect cars from weather factors, and finally providing electricity to homes.…”
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249
Key Success Factors for Export Structure Optimization in East Asian Countries Through Global Value Chain (GVC) Reorganization
Published 2025-01-01“…Policies that enhance market access, promote international standards, and support investments in digital platforms demonstrate strong influence within the GVC system. …”
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250
Police identification of the causes and characteristics of domestic violence against children
Published 2021-12-01“…It is stated that in accordance with international standards and world practice, the interview of a child who is a victim of violent crimes, domestic violence or witnessed violence should be conducted in a child-friendly atmosphere, where they feel protected and comfortable. …”
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251
Age of detection of congenital hearing loss in South Africa: A systematic review
Published 2025-01-01“…Conclusion: These findings show that congenital or early-onset HL in SA is identified later than the national and international standards, that is, 1 month of age. These findings are important for future research, priority setting and implementation of strategies to reduce the burden and impact of HL. …”
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252
Honeys from the Argentine Phytogeographic Provinces Chaqueña and Monte in Catamarca and La Rioja
Published 2023-03-01“…Honeys were authentic and traceable, and complied with the specifications of national and/or international standards, verifying their blossom origin, high quality, good maturity and freshness. …”
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253
Determination of Scopolamine Distribution in Plasma and Brain by LC-MS/MS in Rats
Published 2022-01-01“…Gradient elution of scopolamine and internal standard was performed on a ZORBAX Eclipse Plus C18 (2.1∗100 mm, 3.5 μm) column with water containing 0.1% formic acid (v/v) and acetonitrile as a mobile phase. …”
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254
Simultaneous Determination of 34 Amino Acids in Tumor Tissues from Colorectal Cancer Patients Based on the Targeted UHPLC-MS/MS Method
Published 2020-01-01“…The average recovery and matrix effect for 34 amino acids and 3 internal standards were 39.00%∼146.95% and 49.45%∼173.63%, respectively. …”
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255
High Throughput Quantitative Bioanalytical LC/MS/MS Determination of Gemifloxacin in Human Urine
Published 2013-01-01“…Gemifloxacin and ofloxacin (internal standard) were rapidly extracted from urine samples without any tedious pretreatment procedure. …”
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256
Determination of the market value for goods in the process of forensic commodity expertise
Published 2024-12-01“…It is also noted that the integration of international experience will help to improve the efficiency of forensic commodity expertise in Ukraine and ensure that expert activity complies with international standards. Finally, the study provides proposals for improving the regulatory framework for expert activity and introducing innovative technologies, which allows solving current problems of market valuation under martial law.…”
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257
Application of a Stability-Indicating HPTLC Method for Simultaneous Quantitative Determination of Olmesartan Medoxomil and Hydrochlorothiazide in Pharmaceutical Dosage Forms
Published 2013-01-01“…The method used amlodipine as internal standard (IS). Chromatographic separations were achieved on silica gel 60 F254 plates using toluene-methanol-ethyl acetate-acetone (2.5 : 1 : 0.5 : 2, v/v/v/v) as mobile phase. …”
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258
Assessment of Noise Levels of Equipment Used in the Practical Dental Teaching Activities
Published 2021-01-01“…These results are below the thresholds of the legislation and international standards. However, we have recorded punctual peaks that exceed the recommended level, requiring the introduction of the means of prevention and the measures of safety against the noise as well at the level of the practical activity classroom and the realization of more in-depth studies concerning the evaluation of the daily exposure of the professors, students, and teaching staff to noise.…”
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259
Pancasila in the Context of Indonesian Legal Reform: A Critical Evaluation and International Debate
Published 2024-12-01“…The urgency of this research stems from growing critiques of Indonesia’s legal alignment with international standards while preserving its ideological roots. …”
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260
Legal Regulation of Interaction of Security Service of Ukraine with Civil Society in Counteracting Terrorism
Published 2019-09-01“…In general, Ukraine's anti-terrorist system meets international standards in the field of counteracting terrorism. …”
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