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- Physics 1
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1501
Synthesis of Mannich N-bases based on benzimidazole derivatives using SiO2OAlCl2 catalyst and their potential as antioxidant, antibacterial, and anticancer agents
Published 2025-01-01“…The results showed that the catalyst was successfully synthesized and characterized by The Fourier transform infrared (FTIR), X-ray diffraction (XRD), and Scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM-EDS). …”
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1502
Green synthesis of biocompatible fluorescent carbon dots from bitter gourd for effective metal sensing and biological applications
Published 2025-02-01“…The optical properties, luminescence, phase formation and crystal structure were measured using UV–Visible spectroscopy (UV–Vis), Photoluminescence (PL), X-ray diffraction (XRD) and Transmission electron microscopy (TEM) by varying the medium from acidic to basic by changing its pH (2−12) and temperature range (180-300οC) to assess the exact nature and properties of the synthesized C-dots. …”
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1503
Effect of low aluminum additions in the microstructure and mechanical properties of hot forged high-manganese steels
Published 2023-01-01“…Microstructural evolution was studied using microscopy techniques (OM, and SEM-EDS) and X-ray diffraction measurements for the as-cast and hot forged steels. …”
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1504
Carrageenan bionanocomposite films incorporating Ag and Zn-Doped CeO₂ nanoparticles for active food packaging applications
Published 2025-03-01“…Characterization techniques such as X-ray diffraction (XRD), transmission electron microscopy (TEM), and Zeta potential analysis confirmed the successful doping and stability of the nanoparticles. …”
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1505
RETRACTED: Mycosynthesis of Hematite (α-Fe<sub>2</sub>O<sub>3</sub>) Nanoparticles Using <em>Aspergillus niger</em> and Their Antimicrobial and Photocatalytic Activities
Published 2022-08-01“…The structural and optical properties of Hem-NPs were investigated using X-ray diffraction (XRD), transmission electron microscopy (TEM), dynamic light scattering (DLS), and UV-visible and Fourier-transform infrared (FTIR) spectroscopies. …”
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1506
Hydrogen production by methane decomposition over Ni-doped activated carbons: effect of the activation method
Published 2022-09-01“…The catalysts were characterized before and after reaction by $\mathrm{N}_{2}$ adsorption, X-ray Diffraction (XRD) and Transmission Electron Microscopy (TEM). …”
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1507
Luminescence properties of ZnSe single crystals co-doped with Fe and Cr
Published 2025-02-01“…Structural characterization by high-resolution X-ray diffraction (HR-XRD), electron paramagnetic resonance (EPR) and scanning electron microscopy (SEM) has revealed that the samples differ in terms of dopant concentration and intrinsic native defects. …”
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1508
Photocatalytic removal of textile wastewater-originated methylene blue and malachite green dyes using spent black tea extract-coated silver nanoparticles
Published 2025-01-01“…The characterization was conducted by X-Ray diffraction, Scanning electron microscopy, Zeta potential and energy dispersive X-ray (EDX). …”
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1509
Biosynthesis of reduced graphene oxide using Turbinaria ornata and its cytotoxic effect on MCF‐7 cells
Published 2021-06-01“…Biofunctionalized reduced graphene oxide (TrGO) nanosheets were synthesized using methanol extract of Turbinaria ornata, and bioreduction of graphene oxide was primarily confirmed and characterized using UV‐visible, Fourier transform infrared (FTIR), and X‐ray diffraction spectroscopy and further characterized by zeta potential and transmission electron microscopy. …”
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1510
Green synthesis of Au-Pt bimetallic nanoparticels using Croton caudatus Geisel leaf extract and their biological studies
Published 2025-01-01“…Utilizing transmission electron microscopy (TEM) examination and powder X-ray diffraction, the size of the synthesized nanoparticles was found to be between 12 and 33 nm. …”
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1511
Influence of increasing chromium content on additively manufactured tool steels: Microstructural and mechanical evolution before and after heat treatment
Published 2025-01-01“…Comprehensive microstructural characterization techniques, including optical microscopy, scanning electron microscopy, electron backscatter diffraction, and transmission electron microscopy unveiled a clear correlation between the Cr content and the resulting microstructural features and phase occurrences. …”
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1512
Interface effects in the phase determination of Hf0.5Zr0.5O2 epitaxial thin films
Published 2025-01-01“…This substrate effect is found to be more influential than any changes observed from varying the film thickness (7.5–60 nm), deposition environment (oxygen vs argon), and annealing temperature (400–600 °C) in vacuum (10−5 Torr). X-ray diffraction and scanning transmission electron microscopy verify the phases present, and capacitor-based studies reveal ferroelectric behavior (or lack thereof) consistent with the phases observed. …”
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1513
Chemical Pressure-Induced enhancement of electrochemical performance in Ni1-X CuxTe2 (X = 0 and 0.10) layered compounds
Published 2025-02-01“…This article employed the self-flux technique to successfully generate single crystalline Ni1-XCuXTe2 (X = 0 and 0.10) for electrochemical applications. The X-ray powder diffraction (XRPD) patterns revealed that both compounds have a CdI2-type trigonal structure with a P3m1 space group. …”
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1514
Enhancing water solubility of phytosterols through Co-amorphization with food-grade coformers
Published 2025-01-01“…A 20:1 (w/w) PS-Nic co-amorphous (CM) mixture, prepared via freeze-drying, achieved a solubility of 1536.4 μg/mL, significantly higher than pure PS. X-ray diffraction and differential scanning calorimetry confirmed the amorphous state of the mixture. …”
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1515
Preparation and Gas-Sensitive Properties of SnO<sub>2</sub>@Bi<sub>2</sub>O<sub>3</sub> Core-Shell Heterojunction Structure
Published 2025-01-01“…The SnO<sub>2</sub>@Bi<sub>2</sub>O<sub>3</sub> core-shell heterojunction structure was designed and synthesized via a hydrothermal method, and the structure and morphology of the synthesized samples were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and X-ray photoelectron spectroscopy (XPS). …”
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1516
Forming ability of the WC-based ceramic metal composites with different Fe-based binders by unique laser beam modulation
Published 2025-04-01“…Scanning electron microscope (SEM) and X-ray diffraction (XRD) analysis have been used to study the microstructure and phase formation in the fabricated parts. …”
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1517
Synthetic design and analysis on microwave dielectric properties of novel garnet-type Ca3MTiGe3O12 (M = Co, Ni) ceramics
Published 2025-01-01“…CCTG and CNTG ceramics sintered at optimal temperatures exhibit excellent microwave dielectric properties with εr = 11.64, Q×f = 45474.73 GHz, τf = −42.01 ppm/°C and εr = 11.58, Q×f = 41346.11 GHz, τf = −45.53 ppm/°C, respectively. X-ray diffraction analysis shows that the CCTG is single phase while secondary phase is present in CNTG. …”
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1518
Synthesis and Characterization of Copper Ferrite Nanoparticles for Efficient Photocatalytic Degradation of Organic Dyes
Published 2025-01-01“…The structure of the synthesized material was analyzed through x-ray diffraction (XRD) and further supported by Raman and FT-IR spectroscopy. …”
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1519
Exploring Adsorption Performance of Functionalized Mesoporous Silicas with a Different Pore Structure as Strong Cation-Exchange Sorbents for Solid-Phase Extraction of Atropine and...
Published 2025-01-01“…The synthesized materials were characterized by X-ray diffraction, transmission electron microscopy, scanning electron microscopy, nitrogen adsorption–desorption, Fourier-transform infrared spectroscopy, <sup>29</sup>Si solid-state nuclear magnetic resonance spectroscopy, and elemental analysis. …”
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1520
Synthesis, Crystal Structures, and Antimicrobial and Antitumor Studies of Two Zinc(II) Complexes with Pyridine Thiazole Derivatives
Published 2020-01-01“…Two pyridine thiazole derivatives, namely, 4-(pyridin-2-yl)-2-(2-(pyridin-2-ylmethylene)hydrazinyl)thiazole (L1) and 4-(pyridin-3-yl)-2-(2-(pyridin-4-ylmethylene)hydrazinyl)thiazole (L2), were afforded by a cyclization reaction between α-haloketone and thioamide, and their Zn(II) complexes were prepared by the reaction of ligands and corresponding metal salts, respectively, and characterized by X-ray diffraction and elemental analysis. Both crystals were obtained by ether diffusion and crystallized in a monoclinic system. …”
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