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881
Dual Wavelength RP-HPLC Method for Simultaneous Determination of Two Antispasmodic Drugs: An Application in Pharmaceutical and Human Serum
Published 2013-01-01“…Mobile phase ingredients consist of Acetonitrile : buffer : sulfuric acid 0.1 M (50 : 50 : 0.3 v/v/v), at flow rate 1.0 mL/min using a Hibar μBondapak ODS C18 column monitored at dual wavelength of 266 nm and 205 nm for phloroglucinol and trimethylphloroglucinol, respectively. …”
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882
Multi-platform observations and constraints reveal overlooked urban sources of black carbon in Xuzhou and Dhaka
Published 2025-01-01“…Our daily high-resolution findings reveal smaller black carbon cores and spatially variable morphology dominate both regions. Column loadings reveal higher black carbon mass in Dhaka, while higher total aerosol mass and number are observed in Xuzhou. …”
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883
QuEChERS Method Followed by Solid Phase Extraction Method for Gas Chromatographic-Mass Spectrometric Determination of Polycyclic Aromatic Hydrocarbons in Fish
Published 2015-01-01“…PAHs were separated on a GCMS with HP-5ms Ultra Inert GC Column (30 m, 0.25 mm, and 0.25 µm). Mean recovery ranged from 56 to 115%. …”
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884
Bernese Periacetabular Osteotomy in a Hip Extra-Articular Resection Followed by Reconstruction Using an Extracorporeal Irradiated Acetabulum Autograft with Megaprosthesis, for Prox...
Published 2015-01-01“…Extra-articular resection of the hip using a periacetabular osteotomy technique enabled us to achieve wide margins and leave an intact posterior column to optimize acetabular reconstruction stability. …”
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885
Spatial Variations in PAHs and Nitro-PAHs Bound to Total Suspended Solids in Urban Locations in Taiwan
Published 2024-01-01“…Analysis was performed using a gas chromatograph tandem mass spectrometer (GC-MS/MS) Agilent 7890A GC, USA, equipped with a ZB-EPA-EU 30 m × 0.25 mm × 0.20 µm, column (Agilent, J&W, USA), coupled to Waters Xevo TQ-S (Waters, UK). …”
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886
Quantitative Determination of 7 Saikosaponins in Xiaochaihu Granules Using High-Performance Liquid Chromatography with Charged Aerosol Detection
Published 2021-01-01“…The saikosaponins were purified on an SPE cartridge and determined on a Waters CORTECTS C18 column (4.6 mm × 150 mm, 2.7 μm) by gradient elution using 0.01% acetic acid aqueous solution and acetonitrile. …”
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887
Qualitative and Quantitative Characterization of Monosaccharide Components of Salvia miltiorrhiza, Liguspyragine Hydrochloride, and Glucose Injection
Published 2017-01-01“…Separation was performed on a Phenomenex Luna C18 analytical column (250 mm × 4.6 mm i.d., 5 μm, AccuStandard Inc., USA) at 30°C. …”
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888
Coupling Solvent Extraction Units to Cyclic Adsorption Units
Published 2018-01-01“…When extracting the acid with methanol in a spray column, feed = 4 L min−1, solvent = 80 L min−1, feed impurity level 140 mmol L−1, and extract concentration 7.6 mmol L−1, the raffinate reaches a purity of 1.2 mmol L−1, the solvent being regenerated cyclically in the adsorber (364 kg) to an average of 0.7 mmol L−1. …”
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889
Optimizing Extraction, Evaluating Antioxidant Activity, and Analyzing Bioactive Compounds in Trikaysornmas Formula
Published 2024-01-01“…For the analysis of active constituents in the formula, gallic acid, kaempferol-3-o-glucoside, imperatorin, vitexin, and scopoletin, a validated reversed-phase column high-performance liquid chromatography (HPLC) method was developed. …”
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890
Behavior and Distribution of Heavy Metals Including Rare Earth Elements, Thorium, and Uranium in Sludge from Industry Water Treatment Plant and Recovery Method of Metals by Biosurf...
Published 2012-01-01“…In addition, the removal/recovery process of heavy metals (Pb, Cr, and Ni) from the polluted sludge was studied with biosurfactant (saponin and sophorolipid) elution by batch and column experiments to evaluate the efficiency of biosurfactant for the removal of heavy metals. …”
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891
Preliminary Assessment of Methane Concentration Variation Observed by GOSAT in China
Published 2015-01-01“…Atmospheric column-averaged methane (XCH4) observations from GOSAT are analyzed to study the spatiotemporal variation of XCH4 in China. …”
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892
Charge heterogeneity of therapeutic monoclonal antibodies by different cIEF systems: views on the current situation
Published 2024-12-01“…Here, we discuss the results of an analysis of a panel of antibody products by conventional and whole-column imaging cIEF systems performed as part of European Pharmacopoeia activities related to development of “horizontal standards” for the quality control of monoclonal antibodies (mAbs). …”
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893
Shield Cutting Pile-Group Implementation Effects on the Superstructure
Published 2022-01-01“…At the same time, because of the low angle between the longitudinal axis of the masonry structure and the tunnel axis (22°) and the positive effect of the ring beam and column of the structure in the building, it is clear that the construction of this project has little effect on the upper building, thus showing improved control.…”
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894
Thiazolidinone Steroids Impregnated Polyurethane Foams as a Solid Phase Extractant for the Extraction and Preconcentration of Cadmium(II) from Industrial Wastewater
Published 2011-01-01“…Compound II treated PUFs sorbent was successfully packed in glass column for complete extraction and / or determination of trace concentrations of cadmium(II) in wastewater samples with satisfactory recovery (95±2.6). …”
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895
Simultaneous Determination of Five Chromones of Radix Saposhnikoviae Extract in Rat Plasma by UPLC-MS/MS: Application to a Comparative Pharmacokinetic Study in Normal and Febrile R...
Published 2019-01-01“…The Waters Acquity UPLC BEH C18 (50 mm × 2.1 mm, 1.7 μm) was used as the chromatographic column, 0.1% formic acid water and 0.1% formic acid acetonitrile comprised the mobile phases, and all samples were determined under positive ion mode. …”
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896
Ultrasonic-Assisted Thymol and Carvacrol Extraction from Za’atar Leaves Using Cold-Pressed Sesame Oil
Published 2021-01-01“…In addition, a high-performance liquid chromatography (HPLC) analytical method was developed by using a C8 column and 0.05% trifluoroacetic acid as a buffering agent. …”
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897
Development and Validation of UPLC-MS/MS Method for Determination of Enasidenib in Rat Plasma and Its Pharmacokinetic Application
Published 2020-01-01“…We used the Acquity UPLC BEH C18 column to separate enasidenib and IS. Under the positive ion electrospray ionization (ESI) source conditions, the mass transfer pairs of enasidenib were monitored by multiple reaction monitoring (MRM) to be m/z 474.2 ⟶ 456.1 and m/z 474.2 ⟶ 267.0, and the IS mass transfer pairs were m/z 285.0 ⟶ 154.0. …”
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898
Research on the Characteristics of Coal Bump and Monitoring and Early Warning in Hujiahe Coal Mine
Published 2022-01-01“…The bearing capacity of the coal sample decreases rapidly during the accelerated development period. (2) According to the simulation and field monitoring, it is known that 0~100 m in front of the coal mining face belongs to the key monitoring area. (3) With the advancement of the working face, different coal pillar widths have obvious effects on the vertical stress, and stress increase and decrease zones appear on both sides of the coal column, and the peak stress shows the characteristics of increasing first and then decreasing with the advancement of the working face. …”
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899
NEWS You Can Use— Helping Older Adults Make Informed Food Choices
Published 2024-12-01“…Descriptive statistics and chi-square tests were employed for sociodemographic analysis, while z-tests with Bonferroni correction compared column proportions. Respondents were primarily female (64.5%), aged 60-69 (52.1%). …”
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900
A High-Throughput Size Exclusion Chromatography Method to Determine the Molecular Size Distribution of Meningococcal Polysaccharide Vaccine
Published 2016-01-01“…The analyses were performed on a XK16/70 column packed with sepharose CL-4B with six different batches of Ingovax® ACWY, a meningococcal polysaccharide vaccine produced by Incepta Vaccine Ltd., Bangladesh. …”
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