-
1261
Accumulation and distribution of cadmium at organic-mineral micro-interfaces across soil aggregates
Published 2025-01-01“…Pot experiments were conducted to assess the impacts of mineral, organic, and microbial amendments on the Cd distribution in soil aggregates using synchrotron radiation-based Fourier transform infrared (SR-FTIR) spectroscopy and nano-scale secondary ion mass spectrometry (NanoSIMS). Our results revealed that different soil amendments exerted varying effects on Cd accumulation in soil aggregates. …”
Get full text
Article -
1262
Rapid Determination of Pemetrexed Concentration and Distribution in Human Breast Cancer Cells (McF-7) Based on UHPLC-MS/MS
Published 2021-01-01“…An ultra high-performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) method was developed for rapid quantification of pemetrexed concentration in human breast cancer cells (MCF-7). …”
Get full text
Article -
1263
Gender-Specific Independent and Combined Effects of the Cortisol-to-Cortisone Ratio and 11-Deoxycortisol on Prediabetes and Type 2 Diabetes Mellitus: From the Henan Rural Cohort St...
Published 2019-01-01“…Liquid chromatography-tandem mass spectrometry was used to assess serum cortisol, cortisone, and 11-deoxycortisol. …”
Get full text
Article -
1264
Selective solvothermal extraction of tetrabromobisphenol A to promote plastic recycling
Published 2025-03-01“…Removal of total elemental bromine was analyzed with X-ray fluorescence (XRF), whereas the removal of TBBPA and other plastic additives was evaluated with direct insertion probe mass spectrometry (DIP-MS). IPA/NaOH extraction provided efficient bromine removal, but it also extracted plenty of other plastic additives, including phenolic stabilizers Irganox 1076 and Cyasorb UV-2908. …”
Get full text
Article -
1265
Increased Duodenal Iron Absorption through Upregulation of Ferroportin 1 due to the Decrement in Serum Hepcidin in Patients with Chronic Hepatitis C
Published 2018-01-01“…Serum level of hepcidin-25 was measured by liquid chromatography-tandem mass spectrometry. Ferroportin 1 (FPN) mRNA was measured by RT-PCR and FPN protein was analyzed by western blot. …”
Get full text
Article -
1266
Oleanolic Acid Cubic Liquid Crystal Nanoparticle-Based Thermosensitive Gel Attenuates Depression Symptoms in Chronic Unpredictable Mild Stress Rats
Published 2025-02-01“…The pharmacokinetics of OANG was studied in rats, and OA content was determined using liquid chromatography-mass spectrometry (LC-MS). The pharmacological effects of OANG on depression were evaluated in chronic unpredictable mild stress (CUMS) model rats.Results: The phase transition temperature of the gel was 34°C, and the release of OA from OANG was slow according to the Higuchi kinetic equation. …”
Get full text
Article -
1267
Assessment of the essential oil extracted from Citrus aurantifolia leaves using solvent-free microwave extraction technique
Published 2025-03-01“…Gas chromatography-mass spectrometry (GC–MS) profiling revealed multiple bioactive components in C. aurantifolia leaves EO, with neral (30.728 %), d-limonene (22.824 %), citral (19.430 %), lemonol (5.060 %), geraniol (3.447 %), geranial (3.079 %), and caryophyllene (3.959 %) being the major components. …”
Get full text
Article -
1268
iMulch: an investigation of the influence of polymers on a terrestrial ecosystem using the example of mulch films used in agriculture
Published 2025-01-01“…The development of a detection methodology using Raman spectroscopy and thermo-extraction desorption gas chromatography mass–spectrometry (TED-GC–MS), the adsorption behaviour, ageing in drainage water and soil, their transport behaviour in lysimeters, ecotoxicity, uptake in plants, a life cycle assessment (LCA) and upcycling were considered. …”
Get full text
Article -
1269
Experimental and Theoretical Study on the False Positive of Monomethyltin Determination in Toys Based on Gastric Juice Migration
Published 2020-01-01“…With metal tin powder as a representative of inorganic tin which existed in real samples, it was treated with artificial gastric juice (0.07 mol/L·HCl), followed by ethyl derivatization using sodium tetraethylborate [NaB(Et)4] and then analyzed by gas chromatography-mass spectrometry (GC-MS) according to the procedure specified in the standard of EN 71-3:2013+A3:2018 issued by the European Committee for Standardization (CEN). …”
Get full text
Article -
1270
Smart packaging tools for selected Indian traditional buffalo milk products: a case for on-package freshness indicators
Published 2023-11-01“…The prerequisites for developing freshness indicators were to identify the critical volatile headspace markers using solid phase microextraction (SPME) coupled with gas chromatography-mass spectrometry (GC-MS) for the respective dairy products, selection of suitable innovative ink components, namely dyes (methyl red, and methyl red sodium salt), plasticizer (glycerol), choose appropriate polymer support (methylcellulose, polyvinyl alcohol or paper), and adopt a suitable production technique such as casting, dipping, or electrospinning. …”
Get full text
Article -
1271
Tracing the change of the volatile compounds of soy sauce at different fermentation times by PTR-TOF-MS, E-nose and GC–MS
Published 2025-01-01“…Proton-transfer reaction time-of-flight mass spectrometry (PTR-TOF-MS), combined with electronic nose (E-nose), was first used to track the change of volatile organic compounds (VOCs) in soy sauce in this study. …”
Get full text
Article -
1272
Chemical Composition and Antioxidant and Antimicrobial Activities of Wormwood (Artemisia absinthium L.) Essential Oils and Phenolics
Published 2015-01-01“…The essential oil composition variability of A. absinthium L. aerial parts collected from four different Tunisian regions was assessed by gas chromatography (GC/FID) and by gas chromatography mass spectrometry (GC/MS). In addition, total polyphenols, flavonoids, and condensed tannins as well as antioxidant, antibacterial, and antifungal activities of methanolic extract and essential oils were undertaken. …”
Get full text
Article -
1273
Biocontrol of gray spot disease on Polygonatum cyrtonema Hua by Bacillus velezensis GX1
Published 2025-02-01“…Liquid chromatography-tandem mass spectrometry (LC-MS/MS) analysis revealed that strain GX1 produced significantly higher levels of surfactin A, surfactin B and plipastatin, relative to strain GX8, an ineffective strain. …”
Get full text
Article -
1274
Development of Ketoprofen Impurity A (1-(3-Benzoylphenyl)ethanone) as a Certified Reference Material for Pharmaceutical Quality Control
Published 2025-01-01“…The obtained product was purified using preparative chromatography and characterised by infrared spectroscopy (IR), 1H and 13C nuclear magnetic resonance (NMR), and mass spectrometry. The structure was verified using primary research methods to confirm its identity as the target product. …”
Get full text
Article -
1275
Relationship between prenatal metals exposure and neurodevelopment in one-year-old infants in the CLIMB study
Published 2025-02-01“…The concentrations of 21 metallic elements and 2 metalloids in umbilical cord blood (UCB) serum were measured using inductively coupled plasma mass spectrometry (ICP-MS). Neurodevelopment was measured using Chinese version of Bayley Scales of Infant Development (BSID) for the Psychomotor Development Index (PDI) and the Mental Development Index (MDI). …”
Get full text
Article -
1276
Quantitative proteomics and targeted metabolomics reveal the role of Cassia siamea L. extract in the response to high-fat diet-induced obesity in Drosophila
Published 2025-02-01“…Methods: CSE was obtained via extraction from C. siamea wood with 70 % ethanol and its phytochemical content was analyzed by gas chromatography–mass spectrometry (GC‒MS) and high-performance liquid chromatography (HPLC). …”
Get full text
Article -
1277
Robust collection and processing for label-free single voxel proteomics
Published 2025-01-01“…Abstract With advanced mass spectrometry (MS)-based proteomics, genome-scale proteome coverage can be achieved from bulk tissues. …”
Get full text
Article -
1278
The effects of age and sex on reference intervals for cobalamin, homocysteine, and serum and urinary methylmalonic acid in healthy adult dogs
Published 2025-01-01“…Cobalamin and markersB12met were determined using chemiluminescence immunoassay (cobalamin) and liquid chromatography/tandem mass spectrometry (homocysteine, sMMA, uMMA:crea). In dogs with outlying data, changes in health, markersB12met, and onset of gastrointestinal signs were reevaluated after 9‐15 months. …”
Get full text
Article -
1279
Adipocyte-specific Steap4 deficiency reduced thermogenesis and energy expenditure in mice
Published 2025-02-01“…Adipocyte-specific Steap4-deficient mice exhibited increased fat mass and severe insulin resistance in our high-fat diet model. Mass spectrometry identified two classes of Steap4 interactomes: mitochondrial proteins and proteins involved in splicing. …”
Get full text
Article -
1280
Interaction Between Malat1 and miR-499-5p Regulates Meis1 Expression and Function with a Net Impact on Cell Proliferation
Published 2025-01-01“…Enrichment analyses on proteins identified via mass spectrometry after manipulating Malat1, miR-499-5p, or Meis1 revealed a multitude of differentially expressed proteins related to cell cycle, cell division, and key pathways like Wnt and mTOR, essential for cell proliferation. …”
Get full text
Article