-
1021
Electrochemical preparation of polypyrrole-molybdenum disulfide-graphene nanocomposite coating for the determination of phenols
Published 2025-08-01“…The resulting coating was applied to extract five phenolic compounds, and combined with gas chromatography-mass spectrometry (GC–MS) to establish an analytical method for the determination of 3‑chloro-4-fluorophenol, 2‑chloro-4-methoxyphenol, 2,6-dimethoxyphenol, 2,4,6-trichlorophenol, and 2,6-dichloro-4-nitrophenol in environmental samples. …”
Get full text
Article -
1022
From contamination to detection: The growing threat of heavy metals
Published 2025-01-01“…Although more sensitive, the high cost of inductively coupled plasma mass spectrometry (ICP-MS) may limit laboratory accessibility. …”
Get full text
Article -
1023
Effects of Volatile Components on Mixing State and Size Distribution of Individual Black Carbon Aerosols
Published 2022-03-01“…Abstract In this study, the effects of different volatile components on the mixing state and size distribution of ambient individual black carbon (BC) aerosols were measured using thermo-denudation with single-particle soot photometry and single-particle aerosol mass spectrometry from September 9 to September 27, 2018, in Shanghai, China. …”
Get full text
Article -
1024
Infections Caused by Actinomyces neuii: A Case Series and Review of an Unusual Bacterium
Published 2016-01-01“…Isolates’ identities were confirmed by matrix-assisted laser desorption ionization time-of-flight mass spectrometry microbial identification system (MALDI-TOF MS MIS; bioMérieux) and/or DNA sequencing. …”
Get full text
Article -
1025
Detection of chimeric alpha-defensin transcripts and peptides in mouse Paneth cells
Published 2025-02-01“…Despite their low abundance (less than 0.3%), mass spectrometry confirmed the presence of chimeric peptides. …”
Get full text
Article -
1026
Proteomic Analysis Reveals the Vital Role of Synaptic Plasticity in the Pathogenesis of Temporal Lobe Epilepsy
Published 2022-01-01“…Isobaric tag for relative and absolute quantization (iTRAQ) coupled with liquid chromatography-tandem mass spectrometry (LC–MS/MS) technique was applied for proteomic analysis of hippocampus. …”
Get full text
Article -
1027
Analysis of the changes of volatile flavor compounds in a traditional Chinese shrimp paste during fermentation based on electronic nose, SPME-GC-MS and HS-GC-IMS
Published 2023-01-01“…A total of 106 volatile flavor compounds in the shrimp paste samples at different fermentation stages were identified by solid-phase microextraction-gas chromatography-mass spectrometry (SPME-GC-MS) and headspace-gas chromatography-ion mobility spectrometry (HS-GC-IMS). …”
Get full text
Article -
1028
Rapid detection of Tulipalin A with SESI-Orbitrap MS: an exploration across spring flowers
Published 2025-02-01“…Results Here, we demonstrated the secondary electrospray ionization coupled Orbitrap mass spectrometry (SESI-Orbitrap MS) methodology for quantifying tulipalin A release from plants upon injury. …”
Get full text
Article -
1029
N-acetylated sugars in clownfish and damselfish skin mucus as messengers involved in chemical recognition by anemone host
Published 2025-01-01“…The free and total sialic acid content, including its conjugated form, and three other intermediates of this pathway were quantified using a stable isotope dilution mass spectrometry approach. We found significantly higher levels of sialic acid and its precursor in the non-symbiotic damselfishes. …”
Get full text
Article -
1030
RETRACTED ARTICLE: Clinical and immuno-proteomic approach on Lantana camara pollen allergy—a major health hazard
Published 2016-07-01“…Total proteome was profiled in SDS–PAGE, 2D PAGE and immunoblotted to detect IgE binding proteins which were further identified using mass spectrometry. Results Lantana camara pollen emerged as a significant contributor from the correlation study with hospital admission of the respiratory allergy sufferers and its extract demonstrated an elevated IgE response in ELISA and histamine release assay tests. …”
Get full text
Article -
1031
Development and Validation of a GC-MS Method for the Detection and Quantification of Clotiapine in Blood and Urine Specimens and Application to a Postmortem Case
Published 2015-01-01“…The aim of the present study is the development and validation of a method that allows the detection and quantification of clotiapine in blood and urine specimens by gas chromatography-mass spectrometry (GC-MS). Methods. Validation was performed working on spiked postmortem blood and urine samples. …”
Get full text
Article -
1032
Chemical Composition and Antioxidant Activity of Aloe vera from the Pica Oasis (Tarapacá, Chile) by UHPLC-Q/Orbitrap/MS/MS
Published 2018-01-01“…The chemical characterization was performed using liquid chromatography (UHPLC) coupled to PDA and high-resolution mass spectrometry (HESI-Q-Orbitrap®-MS) in four different plant parts of Aloe (peel, flowers, gel, and roots). …”
Get full text
Article -
1033
Differentially expressed whey proteins of donkey and bovine colostrum revealed with a label-free proteomics approach
Published 2023-07-01“…This study aimed to analyze and compare the differentially expressed whey proteins (DEWPs) of donkey and bovine colostrum using high-performance liquid chromatography with tandem mass spectrometry-based proteomics. A total of 620 and 696 whey proteins were characterized in the donkey and bovine colostrum, respectively, including 383 common whey proteins. …”
Get full text
Article -
1034
Decoding CKD-induced muscle atrophy through the critical role of lncRNA GAS5 and pyroptosis
Published 2025-03-01“…Furthermore, we pinpointed an interaction between GAS5 and the mitochondrial translation elongation factor (TUFM) through RNA pull-down and mass spectrometry. This interaction amplified NLRP3 activity, contributing to pyroptosis and muscle atrophy. …”
Get full text
Article -
1035
Polyhydroxyalkanoates Biopolymer Production by Moderately Halophilic Paracoccus onubensis Strain E3: Extraction, Characterization and Synergistic Activity with Sorafenib Drug again...
Published 2025-01-01“…PHAs were extracted and then subjected to Fourier transform infrared spectroscopy (FT-IR), where the spectrum showed a strong band at 1649.72 cm−1 for the carbon (C=O) stretching of the ester group, which is a common feature in PHAs structures, and Gas chromatography–mass spectrometry (GC-MS) analyses. The GC-MS identified twelve different biodegradable PHA compounds, including hexadecenoic acid and octadecanoic acid. …”
Get full text
Article -
1036
Health risks evaluation of mycotoxins in plant-based supplements marketed in Malaysia
Published 2025-01-01“…Contamination levels of AFB1, AFB2, and OTA were quantified in 14 PBS samples using Liquid Chromatography-Mass Spectrometry. All samples tested positive for AFB2, while 28.57% and 42.86% tested positive for AFB1 and OTA, respectively with some levels exceeding the regulatory limits set by the Malaysian Food Act 1983 and European regulations. …”
Get full text
Article -
1037
Gestational stress disrupts dopamine and oxytocin signaling in the postpartum reward system of rats: implications for mood, motivation and mothering
Published 2025-01-01“…A reduction in accumbal DA content as determined by liquid chromatography-mass spectrometry was also observed in gestationally-stressed dams. …”
Get full text
Article -
1038
Identification of defensive antimicrobial compounds from environmental Serratia marcescens SNB-CN88 strain associated with macro-holobiont (termite nest) using a molecular network...
Published 2024-02-01“…An integrated approach combining reversed-phase high-performance liquid chromatography and high-resolution tandem mass spectrometry with the use of molecular networks was applied to annotate novel chemical structures with potential antimicrobial activities. …”
Get full text
Article -
1039
Sulfone-modified chitosan as selective adsorbent for the extraction of toxic Hg(II) metal ions
Published 2019-03-01“…The β-ketosulfone derivative, namely 1–(4-bromophenyl)-2-(phenylsulfonyl)ethanone, was first prepared by treatment of the corresponding phenacyl bromide with a sufficient amount of sodium benzene sulfinate; its chemical structure was confirmed by spectral analyses, including Fourier transform infrared spectroscopy, 1 H-NMR, 13 C-NMR, and mass spectrometry. Then, sulfone-modified chitosan/5–20 derivatives were synthesized by the interaction of chitosan with a freshly prepared p-bromo-β-ketosulfone derivative in a mildly acidic aqueous solution using the solution-blending technique. …”
Get full text
Article -
1040
SOLARIS project: a portable 3D-printed bioaerosol sampler for environmental bacterial collection
Published 2025-02-01“…Collected samples were found suitable for downstream analysis methods such as culturing, mass spectrometry, molecular detection and electron microscopy. …”
Get full text
Article