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201
Characterization of Key Odorants in Soy Sauce and Their Concentration Changes during Storage
Published 2023-01-01“…To explore the key odorants and their concentration changes in high-salt liquid-state fermentation soy sauce (HLFSS) during storage, solvent extraction coupled with solvent-assisted flavor evaporation was applied to isolate the volatiles in HLFSS, and the volatiles were analyzed by gas chromatograph-mass spectrometry-olfactory and gas chromatograph-flame ionization detector-olfactometry combined with the aroma extract dilution assay. …”
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202
Variations in the concentration of subsoil gases and the atmospheric electric field prior to some earthquakes in Kamchatka
Published 2024-12-01“…The presented data demonstrate the processes of influence of the exhalation of subsoil radon and its daughter products on the ionization balance of the surface layer of the atmosphere. …”
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203
Determination of Urinary Creatinine in Washington State Residents via Liquid Chromatography/Tandem Mass Spectrometry
Published 2014-01-01“…Utilizing electrospray ionization (ESI) in positive mode, the transition ions for creatinine and creatinine-d3 were determined to be 114.0 to 44.1 (quantifier), 114.0 to 86.1 (qualifier), and 117.0 to 47.1 (creatinine-d3). …”
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204
Analysis of 31 Hydrazones of Carbonyl Compounds by RRLC-UV and RRLC-MS(/MS): A Comparison of Methods
Published 2015-01-01“…In this work, the separation of 31 carbonyl compounds (CC) in their 2,4-dinitrophenylhydrazones form was optimized by rapid resolution liquid chromatography in 9 minutes and simultaneously detected by ultraviolet and mass spectrometry with an APCI(−) as ionization source. The mass spectra of hydrazones presented the [M-H]− ions as base peak, but the MS/MS spectra showed fragments related to different structural classes of aldehydes and ketones, representing an important tool to assist structure elucidation of unknown CC in real samples. …”
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205
Liquid Chromatography/Tandem Mass Spectrometry for the Simultaneous Determination of Ursodiol and its Major Metabolites, Tauroursodeoxycholic Acid and Glycoursodeoxycholic Acid in...
Published 2012-01-01“…The mass spectrometer was used in negative ion mode and multiple reactions monitoring using electro spray ionization mode as an interface. The method was fully validated and the calibration curves were linear over the concentration range of 25.9 to 15300.1 ng/mL for ursodiol, 2.7 to 1587.5ng/mLfor tauroursodeoxycholicacid and 25.4 to 15040.9 ng/mL for glycoursodeoxycholic acid. …”
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206
Characterization of Phenolic Constituents from Prunus cerasifera Ldb Leaves
Published 2020-01-01“…The isolated compounds were analyzed by 1H-nuclear magnetic resonance (1H-NMR), 13C-NMR, and electrospray ionization mass spectral (ESI-MS) spectroscopy. Eleven phenolic acids were identified as p-coumaric acid (1), caffeic acid (2), ferulic acid (3), chlorogenic acid (4), 3-O-caffeoylquinic acid (5), 5-O-coumaroylquinic acid (6), 3-O-caffeoylquinic acid methyl ester (7), chlorogenic acid methyl ester (8), 3-O-caffeoyl-5-O-coumaroylquinic acid or 3-O-coumaroyl-5-O-caffeoylquinic acid (9), gallic acid (10), and protocatechuic acid (11). …”
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207
Pharmacokinetic Comparison of Isoalantolactone and Alantolactone in Rats after Administration Separately by Optimization of an UPLC-MS2 Method
Published 2014-01-01“…In this method, an electrospray ionization source was applied and operated in positive ion mode; multiple reaction monitoring (MRM) was selected for quantification using target fragment ions 233.2→187.1 for isoalantolactone (alantolactone) and 245.1→189.1 for internal standard (IS). …”
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208
Deep Electron Density Depletion Near Sunset Terminator on St. Patrick's Day Storm and Its Impacts on Skywave Propagation
Published 2023-03-01“…The controlled SAMI2 (Sami2 is Another Model of the Ionosphere) simulations indicate that a large equatorial vertical drift around sunset terminator can produce such a deep electron density depletion and strong reinforcement of equatorial ionization anomaly. The impacts of these ionospheric density disturbances on the Skywave communication systems have been investigated using an HF propagation simulator that solves the propagation path of radio waves under given background ionospheric conditions. …”
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209
Nontarget Metabolites of Rhizomes of Edible Sacred Lotus Provide New Insights into Rhizome Browning
Published 2022-01-01“…In this study, 48 target metabolites were untargeted and identified in 212 rhizome cultivars (tropical and temperate types) using ultraperformance liquid chromatography-electrospray ionization quadrupole time-of-flight high-resolution mass spectrometry; among these, 32 compounds were newly reported in the rhizome. …”
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210
Multiresidue Pesticides Analysis of Vegetables in Vietnam by Ultrahigh-Performance Liquid Chromatography in Combination with High-Resolution Mass Spectrometry (UPLC-Orbitrap MS)
Published 2019-01-01“…Experimental results demonstrated that the ionization suppression or enhancement was the main contribution on the overall recoveries of target analytes. …”
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211
The Sunburst Arc with JWST. III. An Abundance of Direct Chemical Abundances
Published 2025-01-01“…We detect the temperature-sensitive auroral lines [S ii ] λλ 4070, 4076, [O iii ] λ 4363, [S iii ] λ 6314, [O ii ] λλ 7320, 7330, and [Ne iii ] λ 3343 in a stacked spectrum of five multiple images of the Lyman-continuum emitter (LCE), from which we directly measure the electron temperature in the low-, intermediate-, and high-ionization zones. We also detect the density-sensitive doublets of [O ii ] λλ 3727, 3730, [S ii ] λλ 6718, 6733, and [Ar iv ] λλ 4713, 4741, which constrain the density in both the low- and high-ionization gas. …”
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212
Hydrophilic Interaction Liquid Chromatography-Tandem Mass Spectrometry Analysis of Fosetyl-Aluminum in Airborne Particulate Matter
Published 2018-01-01“…The chromatographic separation was achieved using a polymeric column based on hydrophilic interaction in step elution with water/acetonitrile, whereas the mass spectrometric detection was performed in negative electrospray ionization. The proposed method resulted to be a simple, fast, and suitable method for confirmation purposes.…”
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213
ABIOTIC STRESS RESPONSE-ASSOCIATED PROTEINS IN A SALT TOLERANT STRAIN OF THE CYANOBACTERIUM FREMYELLA DIPLOSIPHON: A POTENTIAL BIOFUEL AGENT
Published 2021-07-01“…In this study, protein expression in wild type and halotolerant mutant F. diplosiphon strains was compared using two-dimensional polyacrylamide gel electrophoresis and matrix-assisted laser desorption/ionization time of flight mass spectrometry. Of the 16 up-regulated proteins identified in the mutant, tripartite ATP-independent periplasmic (TRAP) transporter solute receptor was found to assist in salt-stress response with a significant hit to a corresponding spot with a score of 669 and 21% sequence coverage. …”
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214
Development of a Methodology for the Determination of Pesticide Residues in Cajá-Manga Pulp (Spondias dulcis L.) Using Solid-Liquid Extraction with Low-Temperature Partitioning
Published 2018-01-01“…The quantification was performed by gas chromatography with flame ionization detection which, although it does not present the best detectability for the compounds, is a lower cost instrumentation and is available in several analysis laboratories in Brazil, making the method more accessible to evaluate the pesticide residues in fruit pulp. …”
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215
Comprehensive Studies on Detection of Palm Oil Adulteration in Clarified Milk Fat (Ghee)
Published 2025-01-01“…In chromatographic analytical approaches, triglyceride analysis (S-value) was carried out using gas chromatography with flame ionization detection (GC-FID), and plant sterol detection was done by HPLC, which proved to be the robust method for ascertaining the presence of palm oil in milk fat (ghee) at 5%. …”
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216
Isolation and Identification of Optochin-Resistant Viridans Group Streptococci from the Sputum Samples of Adult Patients in Jakarta, Indonesia
Published 2021-01-01“…Optochin-resistant VGS isolates were identified by matrix-assisted laser desorption ionization time of flight mass spectrometry (MALDI-TOF MS). recA sequencing was used to confirm identified isolates at the genus level by MALDI-TOF MS. …”
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217
An Experimental and Quantum Chemical Calculation Study on the Performance of Different Types of Ester Collectors
Published 2025-01-01“…The electrostatic potential extremum around S atom and the first ionization potential of IPETC and IBALTC are similar and were smaller than IBIBCTC and PXA, which shows that the collecting ability of the former two is similar and stronger than the latter two. …”
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218
Determination of Senegenin and Tenuifolin in Mouse Blood by Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry and Their Pharmacokinetics
Published 2022-01-01“…Quantitative analysis was performed using electrospray ionization (ESI) with multiple reaction monitoring (MRM) in negative ion mode. …”
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219
Similar Strains of Coagulase-Negative Staphylococci Found in the Gastrointestinal Tract and Bloodstream of Bacteremic Neonates
Published 2020-01-01“…CoNS strains isolated from blood cultures and perianal and pharyngeal swab samples of neonates from two neonatal intensive care units were investigated using matrix-assisted laser desorption/ionization time-of-flight mass spectrometry and pulsed-field gel electrophoresis. …”
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220
Detection of n-nitrosamine compounds by gas chromatography in sausages
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