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621
Comprehensive metabolite profiling and evaluation of anti-nociceptive and anti-inflammatory potencies of Nypa fruticans (Wurmb.) leaves: Experimental and in-silico approaches
Published 2025-02-01“…High-performance liquid chromatography (HPLC) and gas chromatography-mass spectroscopy (GC-MS) were employed to identify the phytochemicals in EENF. …”
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622
Physical and Chemical Properties of Biodiesel Obtained from Amazon Sailfin Catfish (Pterygoplichthys pardalis) Biomass Oil
Published 2019-01-01“…The physical and chemical properties of biofuel produced were evaluated under the specifications of the European standard EN-14214 by using gas chromatography-mass spectrometry, infrared spectroscopy, and atomic absorption spectrometry analyses. …”
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623
Legacy and emerging organic pollutants in indoor and outdoor environments in Africa: Contamination levels, health risks, and analytical techniques
Published 2025-06-01“…Apart from a few studies for polychlorinated biphenyls (PCBs), most studies reported hazard index (HI) values less than 1 for outdoor air and indoor dust exposure, which suggested negligible non-carcinogenic risks in children and adults. Gas Chromatography and mass spectrometry were the most frequently used analytical techniques for both air and dust probably due to their sensitivity and selectivity in detecting chemical traces at the pg m−3 and ng g−1 levels. …”
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624
Toxicity effect of Ricinus communis methanolic extracts against Bactrocera cucurbitae (Diptera: Tephritidae)
Published 2025-01-01“…The crude extract of R. communis was subjected to fractionating using different organic solvents in an increasing order of polarity, where the fraction indicating maximum activity was then taken for the isolation of the bioactive compounds using various chromatographic and spectroscopic techniques such as column chromatography, thin layer chromatography (TLC), gas chromatography-mass spectrometry (GC-MS). The concentrations of R. communis extracts at 0.5, 1.0, 1.5 and 2% methanol were used. …”
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625
Compositional changes of dissolved organic matter during high flow events in headwater catchments along a gradient of climate and land use
Published 2024-11-01“…The DOM composition was analyzed by thermochemolysis coupled with gas chromatography and mass spectrometry, making it possible to perform a joint analysis of several biomolecule families, monitor the proportion of compounds derived from plant inputs (%VEG) and study the lignin composition through the C/V ratio. …”
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626
Synergistic antimicrobial activity of essential oils mixture of Moringa oleifera, Cinnamomum verum and Nigella sativa against Staphylococcus aureus using L-optimal mixture design
Published 2025-01-01“…Notably, the oil mixture of run 15 demonstrated excellent biocompatibility, maintaining 97.6% viability of normal human skin fibroblasts (HSF) after 24 h exposure to 200 μL EOs of the mixture per mL. Gas chromatography mass spectrometry (GC/MS) identified abundant bioactive phytochemicals like cinnamaldehyde, linoleic acid, and palmitic acid methyl esters underlying the observed antimicrobial effects. …”
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627
Modulation of Caecal Microbiome in Obese Mice Associated with Administration of Amaranth or Soybean Protein Isolates
Published 2018-12-01“…Caecal Short Chain Fatty Acids (SCFAs) were quantified by gas chromatography. The consumption of soybean protein induced the ectopic deposition of fat in the whole intestine while amaranth proteins increased caecal crypt depth and calceiform cells number sustaining its beneficial effect on health. …”
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628
Characteristics and Influencing Factors of Soil CH4 and N2O Fluxes in Typical Broad-leaved Forests in the Yangtze River Delta Region, China
Published 2024-12-01“…[Methods] Taking the typical broad-leaved forest soil in Hangzhou, Zhejiang Province as the research object, soil-air interface CH4 and N2O fluxes were continuously measured from November 2022 to November 2023 by the static chamber-gas chromatography method. [Results] The average annual absorption fluxes of CH4 in the soil without litter (S) and soil with litter (SL) treatments were (47.82±18.54), (36.80±13.55) μg/(m2·h), as well as the average emission fluxes of N2O were (80.74±45.24), (52.70±25.98) μg/(m2·h), respectively. …”
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629
Optimised extraction of antioxidant components from Calophyllum inophyllum L. seeds using response surface methodology
Published 2024-07-01“…Characterisation with gas chromatography-mass spectroscopy revealed ten compounds with major percentage values, among them 2''-(trimethylsilyl)oxy-3,4,4'',5- tetramethoxychalcone (49.70 per cent). …”
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630
Source attribution, health risk analysis, and policy implications of PAHs and NPAHs in PM $$_{10}$$ in Northern Mexico
Published 2024-12-01“…Abstract This research investigates the concentrations, sources, and health risks of polycyclic aromatic hydrocarbons (PAHs) and nitrated PAHs (NPAHs) in particulate matter with an aerodynamic diameter of 10 $$\mu$$ m or less (PM $$_{10}$$ ) from critical urban centers in northern Mexico: Metropolitan Monterrey Area (MMA), Chihuahua (CHI), and Ciudad Juárez (CDJ). Advanced gas chromatography-mass spectrometry (GC-MS and GC-NCI-MS) revealed significant PAHs concentrations, with levels in MMA reaching 108.89 ± 99.90 ng/m $$^3$$ , CHI at 100.69 ± 122.60 ng/m $$^3$$ and CDJ at 73.26 ± 90.85 ng/m $$^3$$ . …”
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631
Microbial community succession characteristics in an anaerobic baffled reactor during phenol gradient acclimation
Published 2025-03-01“…Phenol degradation intermediates were performed using gas chromatography/mass spectrometry (GC–MS), with their quantities measured by high-performance liquid chromatography. …”
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632
Effects of Lactobacillus plantarum on Physicochemical Properties and Volatile Flavor Substances of Blueberry Juice during Fermentation and Storage
Published 2025-01-01“…Moreover, HPLC and headspace solid-phase microextraction gas chromatography (HS-SPME-GC/MS) were used to measure the changes of organic acids and flavor metabolites, finally the quality of flavor was analyzed during fermentation and storage. …”
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633
Bar Adsorptive Microextraction Approach for Trace Determination of Local Anesthetics in Urine Matrices
Published 2024-12-01“…Two extractive preconcentration techniques, solid-phase microextraction (SPME) LC Tips and bar adsorptive microextraction (BAμE), were studied and applied to the four target anesthetics, followed by gas chromatography-mass spectrometry (GC-MS) analysis. Several parameters that could affect microextraction and back-extraction were optimized using two different designs of experiments (Box–Behnken and full-factorial) to maximize extraction efficiency from aqueous media. …”
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634
The effect of endosulfan bioaccumulation on the growth of carp, Cyprinus carpio LINN.
Published 2009-01-01“…Endosulfan residue analysis in the water and the body of the fish was conducted after: 0, 4, 12, 24, 48, 96, 144, 192, 264 of exposure hours by using liquid gas chromatography (LGC). Body weight of fish was measured weekly. …”
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635
Assessment of the essential oil extracted from Citrus aurantifolia leaves using solvent-free microwave extraction technique
Published 2025-03-01“…EO was obtained from C. aurantifolia leaves using solvent-free microwave extraction (SFME). Gas chromatography-mass spectrometry (GC–MS) profiling revealed multiple bioactive components in C. aurantifolia leaves EO, with neral (30.728 %), d-limonene (22.824 %), citral (19.430 %), lemonol (5.060 %), geraniol (3.447 %), geranial (3.079 %), and caryophyllene (3.959 %) being the major components. …”
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636
iMulch: an investigation of the influence of polymers on a terrestrial ecosystem using the example of mulch films used in agriculture
Published 2025-01-01“…The development of a detection methodology using Raman spectroscopy and thermo-extraction desorption gas chromatography mass–spectrometry (TED-GC–MS), the adsorption behaviour, ageing in drainage water and soil, their transport behaviour in lysimeters, ecotoxicity, uptake in plants, a life cycle assessment (LCA) and upcycling were considered. …”
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637
Experimental and Theoretical Study on the False Positive of Monomethyltin Determination in Toys Based on Gastric Juice Migration
Published 2020-01-01“…With metal tin powder as a representative of inorganic tin which existed in real samples, it was treated with artificial gastric juice (0.07 mol/L·HCl), followed by ethyl derivatization using sodium tetraethylborate [NaB(Et)4] and then analyzed by gas chromatography-mass spectrometry (GC-MS) according to the procedure specified in the standard of EN 71-3:2013+A3:2018 issued by the European Committee for Standardization (CEN). …”
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638
Smart packaging tools for selected Indian traditional buffalo milk products: a case for on-package freshness indicators
Published 2023-11-01“…The prerequisites for developing freshness indicators were to identify the critical volatile headspace markers using solid phase microextraction (SPME) coupled with gas chromatography-mass spectrometry (GC-MS) for the respective dairy products, selection of suitable innovative ink components, namely dyes (methyl red, and methyl red sodium salt), plasticizer (glycerol), choose appropriate polymer support (methylcellulose, polyvinyl alcohol or paper), and adopt a suitable production technique such as casting, dipping, or electrospinning. …”
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639
Process Optimization and Antioxidant Activity of Pine Needle Essential Oil Extracted by Microwave-assisted Extraction
Published 2025-01-01“…Methods: Response surface methodology was used to optimize the process of extracting the pine needle essential oil from Pinus tabuliformis by microwave-assisted extraction (MAE), the components of essential oil were identified by gas chromatography-mass spectrometry (GC-MS) and the antioxidant activity was verified by DPPH and ABTS+ free radicals scavenging ability as indicators. …”
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640
Imbalance of Microbacterial Diversity Is Associated with Functional Prognosis of Stroke
Published 2023-01-01“…Twenty stroke patients and twenty healthy controls were enrolled in the current study, and their demographics were matched. Gas chromatography was used to determine the fecal SCFAs, and 16S rRNA gene sequencing was used to evaluate their fecal microbiota. …”
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