EXPERIMENTAL TESTING OF AN IN VIVO METHOD OF PHOTOTOXICITY EVALUATION

At present all new medicinal products and cosmetics that absorb medium-wavelength UVB, long-wavelength UVA, or visible light in the range 290–700 nm need to be tested for potential phototoxicity. phototoxicity is evaluated by both in vitro and in vivo methods. There are guidelines for in vitro photo...

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Main Authors: V. А. Vavilova, E. V. Shekunova, V. A. Kashkin, M. N. Makarova, V. G. Makarov, A. Ya. Khaymenov
Format: Article
Language:Russian
Published: Federal State Budgetary Institution ‘Scientific Centre for Expert Evaluation of Medicinal Products’ of the Ministry of Health of the Russian Federation (FSBI ‘SCEEMP’) 2018-06-01
Series:Регуляторные исследования и экспертиза лекарственных средств
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Online Access:https://www.vedomostincesmp.ru/jour/article/view/182
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author V. А. Vavilova
E. V. Shekunova
V. A. Kashkin
M. N. Makarova
V. G. Makarov
A. Ya. Khaymenov
author_facet V. А. Vavilova
E. V. Shekunova
V. A. Kashkin
M. N. Makarova
V. G. Makarov
A. Ya. Khaymenov
author_sort V. А. Vavilova
collection DOAJ
description At present all new medicinal products and cosmetics that absorb medium-wavelength UVB, long-wavelength UVA, or visible light in the range 290–700 nm need to be tested for potential phototoxicity. phototoxicity is evaluated by both in vitro and in vivo methods. There are guidelines for in vitro phototoxicity evaluation, however, there are no formally validated protocols for in vivo phototoxicity evaluation. The purpose of this study was to test an economically viable and informative method for in vivo evaluation of tetracycline and ketorolac phototoxicity using outbred rats. Two medicinal products potentially capable of causing clinically established phototoxic reactions were used in this study: tetracycline (tablets, 200 mg/kg and 300 mg/kg) and ketorolac (gel, 13.4 mg/kg, 26.8 mg/kg and 40.3 mg/kg). The medicines were administered in both single and multiple doses. Ultraviolet irradiator OUFK-03 (OOO «Solnyshko», Russia) was used as a light source. The UV exposure (5 J/cm2 and 15 J/cm2) was performed once 1 h after medicine administration. The skin reaction was evaluated 30 minutes and 24 hours after irradiation and then daily for 2 weeks. As a result, the following optimal parameters were determined for in vivo evaluation of phototoxic reactions caused by the medicines: radiation intensity — 15 J/cm2 for single systemic administration and 5 J/cm2 for single topical (dermal) administration; recommended period of skin reaction evaluation for outbred rats is not less than 7 days.
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institution Kabale University
issn 3034-3062
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language Russian
publishDate 2018-06-01
publisher Federal State Budgetary Institution ‘Scientific Centre for Expert Evaluation of Medicinal Products’ of the Ministry of Health of the Russian Federation (FSBI ‘SCEEMP’)
record_format Article
series Регуляторные исследования и экспертиза лекарственных средств
spelling doaj-art-fb366da38b5341d0822ff26491663d072025-08-20T03:40:14ZrusFederal State Budgetary Institution ‘Scientific Centre for Expert Evaluation of Medicinal Products’ of the Ministry of Health of the Russian Federation (FSBI ‘SCEEMP’)Регуляторные исследования и экспертиза лекарственных средств3034-30623034-34532018-06-018211512210.30895/1991-2919-2018-8-2-115-122163EXPERIMENTAL TESTING OF AN IN VIVO METHOD OF PHOTOTOXICITY EVALUATIONV. А. Vavilova0E. V. Shekunova1V. A. Kashkin2M. N. Makarova3V. G. Makarov4A. Ya. Khaymenov5JSC Scientific-Production Association «HOME OF PHARMACY»JSC Scientific-Production Association «HOME OF PHARMACY»JSC Scientific-Production Association «HOME OF PHARMACY»JSC Scientific-Production Association «HOME OF PHARMACY»JSC Scientific-Production Association «HOME OF PHARMACY»Russian office of Dr. Reddy’s Laboratories Ltd.At present all new medicinal products and cosmetics that absorb medium-wavelength UVB, long-wavelength UVA, or visible light in the range 290–700 nm need to be tested for potential phototoxicity. phototoxicity is evaluated by both in vitro and in vivo methods. There are guidelines for in vitro phototoxicity evaluation, however, there are no formally validated protocols for in vivo phototoxicity evaluation. The purpose of this study was to test an economically viable and informative method for in vivo evaluation of tetracycline and ketorolac phototoxicity using outbred rats. Two medicinal products potentially capable of causing clinically established phototoxic reactions were used in this study: tetracycline (tablets, 200 mg/kg and 300 mg/kg) and ketorolac (gel, 13.4 mg/kg, 26.8 mg/kg and 40.3 mg/kg). The medicines were administered in both single and multiple doses. Ultraviolet irradiator OUFK-03 (OOO «Solnyshko», Russia) was used as a light source. The UV exposure (5 J/cm2 and 15 J/cm2) was performed once 1 h after medicine administration. The skin reaction was evaluated 30 minutes and 24 hours after irradiation and then daily for 2 weeks. As a result, the following optimal parameters were determined for in vivo evaluation of phototoxic reactions caused by the medicines: radiation intensity — 15 J/cm2 for single systemic administration and 5 J/cm2 for single topical (dermal) administration; recommended period of skin reaction evaluation for outbred rats is not less than 7 days.https://www.vedomostincesmp.ru/jour/article/view/182phototoxicityphototoxic reactionsuv radiationtetracyclineketorolacoutbred rats
spellingShingle V. А. Vavilova
E. V. Shekunova
V. A. Kashkin
M. N. Makarova
V. G. Makarov
A. Ya. Khaymenov
EXPERIMENTAL TESTING OF AN IN VIVO METHOD OF PHOTOTOXICITY EVALUATION
Регуляторные исследования и экспертиза лекарственных средств
phototoxicity
phototoxic reactions
uv radiation
tetracycline
ketorolac
outbred rats
title EXPERIMENTAL TESTING OF AN IN VIVO METHOD OF PHOTOTOXICITY EVALUATION
title_full EXPERIMENTAL TESTING OF AN IN VIVO METHOD OF PHOTOTOXICITY EVALUATION
title_fullStr EXPERIMENTAL TESTING OF AN IN VIVO METHOD OF PHOTOTOXICITY EVALUATION
title_full_unstemmed EXPERIMENTAL TESTING OF AN IN VIVO METHOD OF PHOTOTOXICITY EVALUATION
title_short EXPERIMENTAL TESTING OF AN IN VIVO METHOD OF PHOTOTOXICITY EVALUATION
title_sort experimental testing of an in vivo method of phototoxicity evaluation
topic phototoxicity
phototoxic reactions
uv radiation
tetracycline
ketorolac
outbred rats
url https://www.vedomostincesmp.ru/jour/article/view/182
work_keys_str_mv AT vavavilova experimentaltestingofaninvivomethodofphototoxicityevaluation
AT evshekunova experimentaltestingofaninvivomethodofphototoxicityevaluation
AT vakashkin experimentaltestingofaninvivomethodofphototoxicityevaluation
AT mnmakarova experimentaltestingofaninvivomethodofphototoxicityevaluation
AT vgmakarov experimentaltestingofaninvivomethodofphototoxicityevaluation
AT ayakhaymenov experimentaltestingofaninvivomethodofphototoxicityevaluation