Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane
A new compound, 2-dichloromethyl-2-p-nitrophenyl-1,3-dioxane, was synthesized and characterized. The crystal structure of the title compound (C11H11Cl2NO4, Mr=292.11) has been determined by single-crystal X-ray diffraction. The crystal is of monoclinic, space group P21/c with a=11.013(2) Å, b=14.653...
Saved in:
| Main Authors: | , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
Wiley
2013-01-01
|
| Series: | Journal of Chemistry |
| Online Access: | http://dx.doi.org/10.1155/2013/974174 |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| _version_ | 1832556789169651712 |
|---|---|
| author | Fei Ye Chang-Ying Sun Ying Fu |
| author_facet | Fei Ye Chang-Ying Sun Ying Fu |
| author_sort | Fei Ye |
| collection | DOAJ |
| description | A new compound, 2-dichloromethyl-2-p-nitrophenyl-1,3-dioxane, was synthesized and characterized. The crystal structure of the title compound (C11H11Cl2NO4, Mr=292.11) has been determined by single-crystal X-ray diffraction. The crystal is of monoclinic, space group P21/c with a=11.013(2) Å, b=14.653(3) Å, c=7.8693(16) Å, α=90°, β=97.06(3)°, γ=90°, V=1260.3(4) Å3, Z=4, F(000)=600, Dc=1.540 mg/cm3, the final R1=0.0508, and ωR2=0.1072 for observed reflections with I>2σI. A total of 12162 reflections were collected, of which 2867 were unique (Rint=0.06999). |
| format | Article |
| id | doaj-art-f94799a898e64d8f96659cf02e5a01da |
| institution | Kabale University |
| issn | 2090-9063 2090-9071 |
| language | English |
| publishDate | 2013-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | Journal of Chemistry |
| spelling | doaj-art-f94799a898e64d8f96659cf02e5a01da2025-02-03T05:44:33ZengWileyJournal of Chemistry2090-90632090-90712013-01-01201310.1155/2013/974174974174Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxaneFei Ye0Chang-Ying Sun1Ying Fu2College of Science, Northeast Agricultural University, Harbin, Heilongjiang 150030, ChinaCollege of Science, Northeast Agricultural University, Harbin, Heilongjiang 150030, ChinaCollege of Science, Northeast Agricultural University, Harbin, Heilongjiang 150030, ChinaA new compound, 2-dichloromethyl-2-p-nitrophenyl-1,3-dioxane, was synthesized and characterized. The crystal structure of the title compound (C11H11Cl2NO4, Mr=292.11) has been determined by single-crystal X-ray diffraction. The crystal is of monoclinic, space group P21/c with a=11.013(2) Å, b=14.653(3) Å, c=7.8693(16) Å, α=90°, β=97.06(3)°, γ=90°, V=1260.3(4) Å3, Z=4, F(000)=600, Dc=1.540 mg/cm3, the final R1=0.0508, and ωR2=0.1072 for observed reflections with I>2σI. A total of 12162 reflections were collected, of which 2867 were unique (Rint=0.06999).http://dx.doi.org/10.1155/2013/974174 |
| spellingShingle | Fei Ye Chang-Ying Sun Ying Fu Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane Journal of Chemistry |
| title | Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane |
| title_full | Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane |
| title_fullStr | Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane |
| title_full_unstemmed | Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane |
| title_short | Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane |
| title_sort | synthesis and crystal structure of 2 dichloromethyl 2 4 nitrophenyl 1 3 dioxane |
| url | http://dx.doi.org/10.1155/2013/974174 |
| work_keys_str_mv | AT feiye synthesisandcrystalstructureof2dichloromethyl24nitrophenyl13dioxane AT changyingsun synthesisandcrystalstructureof2dichloromethyl24nitrophenyl13dioxane AT yingfu synthesisandcrystalstructureof2dichloromethyl24nitrophenyl13dioxane |