LEWIS-BASE ADDUCTS OF LEAD(II) COMPOUNDS VI.* SYNTHESIS AND STRUCTURAL CHARACTERIZATION OF MONONUCLEAR (DIACETATO-0,O ')(1, 10-PHENANTHROLINE)
The synthesis and single-crystal X-ray structure determination of the title compound (phen)Pb(02CMe) is described. The complex crystallizes in the monoclinic space group P2 /c, a = 7.823(3), b = 12.421(4), c = 9.262(2) ?, ? = 79.92(3)", Z = 4, yielding R 0.048 for 3210 independent reflections....
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| Format: | Article |
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| Language: | English |
| Published: |
University of Tehran
1996-06-01
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| Series: | Journal of Sciences, Islamic Republic of Iran |
| Online Access: | https://jsciences.ut.ac.ir/article_31103_5a9e9fd2355d0fc06ee5356415ffbd3b.pdf |
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| Summary: | The synthesis and single-crystal X-ray structure determination of the title
compound (phen)Pb(02CMe) is described. The complex crystallizes in the
monoclinic space group P2 /c, a = 7.823(3), b = 12.421(4), c = 9.262(2) ?, ? =
79.92(3)", Z = 4, yielding R 0.048 for 3210 independent reflections. The
coordination number around the lead atom is six. [Pb-N 2.54(2), 2.56(4)],[Pb-0,
2.19-2.22] |
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| ISSN: | 1016-1104 2345-6914 |