Structural features of near equiatomic FeCo-2V semi-hard magnetic alloy prepared by MIM technology
The structural properties of a magnetically semi-hard near equiatomic FeCo-2wt%V (FeCoV) alloy produced by Powder Injection Moulding (PIM) (option by fine metal powder - Metal Injection Moulding (MIM) technology) were investigated in this paper. Starting granulate was prepared by mixing FeCoV powder...
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International Institute for the Science of Sintering, Beograd
2024-01-01
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Series: | Science of Sintering |
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Online Access: | https://doiserbia.nb.rs/img/doi/0350-820X/2024/0350-820X2300055N.pdf |
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author | Nedeljković Borivoje Pavlović Vladimir B. Obradović Nina Mitrović Nebojša |
author_facet | Nedeljković Borivoje Pavlović Vladimir B. Obradović Nina Mitrović Nebojša |
author_sort | Nedeljković Borivoje |
collection | DOAJ |
description | The structural properties of a magnetically semi-hard near equiatomic FeCo-2wt%V (FeCoV) alloy produced by Powder Injection Moulding (PIM) (option by fine metal powder - Metal Injection Moulding (MIM) technology) were investigated in this paper. Starting granulate was prepared by mixing FeCoV powder with a low-viscosity binder. After injection, the green samples were first treated with a solvent and then thermally with the same aim of removing the binder. MIM technology was completed by high-temperature sintering for 3.5 hours at temperatures from 1370 to 1460°C in a hydrogen atmosphere, which provides the necessary magnetic and mechanical characteristics. The influence of sintering temperature was investigated concerning the aspects of the processes of structural transformation by the methods of X-ray diffraction (XRD) and scanning electron microscopy (SEM). The appearance of an intense diffraction peak of the α'- FeCo phase (crystal structure type B2) was registered for all investigated samples. Structural parameters particle size Dmax, Feret X, and Feret Y exhibit constant increase with increase of sintering temperature. |
format | Article |
id | doaj-art-f0462adf5f844c50a78421f302a19855 |
institution | Kabale University |
issn | 0350-820X 1820-7413 |
language | English |
publishDate | 2024-01-01 |
publisher | International Institute for the Science of Sintering, Beograd |
record_format | Article |
series | Science of Sintering |
spelling | doaj-art-f0462adf5f844c50a78421f302a198552025-01-30T06:46:26ZengInternational Institute for the Science of Sintering, BeogradScience of Sintering0350-820X1820-74132024-01-0156443344410.2298/SOS231024055N0350-820X2300055NStructural features of near equiatomic FeCo-2V semi-hard magnetic alloy prepared by MIM technologyNedeljković Borivoje0https://orcid.org/0000-0003-4923-3174Pavlović Vladimir B.1https://orcid.org/0000-0002-1138-0331Obradović Nina2https://orcid.org/0000-0002-7993-293XMitrović Nebojša3https://orcid.org/0000-0002-7971-6321Faculty of Technical Sciences, University of Kragujevac, Čačak, SerbiaUniversity of Belgrade, Faculty of Agriculture, Belgrade, SerbiaInstitute of Technical Sciences of SASA, Belgrade, SerbiaFaculty of Technical Sciences, University of Kragujevac, Čačak, SerbiaThe structural properties of a magnetically semi-hard near equiatomic FeCo-2wt%V (FeCoV) alloy produced by Powder Injection Moulding (PIM) (option by fine metal powder - Metal Injection Moulding (MIM) technology) were investigated in this paper. Starting granulate was prepared by mixing FeCoV powder with a low-viscosity binder. After injection, the green samples were first treated with a solvent and then thermally with the same aim of removing the binder. MIM technology was completed by high-temperature sintering for 3.5 hours at temperatures from 1370 to 1460°C in a hydrogen atmosphere, which provides the necessary magnetic and mechanical characteristics. The influence of sintering temperature was investigated concerning the aspects of the processes of structural transformation by the methods of X-ray diffraction (XRD) and scanning electron microscopy (SEM). The appearance of an intense diffraction peak of the α'- FeCo phase (crystal structure type B2) was registered for all investigated samples. Structural parameters particle size Dmax, Feret X, and Feret Y exhibit constant increase with increase of sintering temperature.https://doiserbia.nb.rs/img/doi/0350-820X/2024/0350-820X2300055N.pdffecov alloymim technologystructural propertiesparticle size dmaxferet x |
spellingShingle | Nedeljković Borivoje Pavlović Vladimir B. Obradović Nina Mitrović Nebojša Structural features of near equiatomic FeCo-2V semi-hard magnetic alloy prepared by MIM technology Science of Sintering fecov alloy mim technology structural properties particle size dmax feret x |
title | Structural features of near equiatomic FeCo-2V semi-hard magnetic alloy prepared by MIM technology |
title_full | Structural features of near equiatomic FeCo-2V semi-hard magnetic alloy prepared by MIM technology |
title_fullStr | Structural features of near equiatomic FeCo-2V semi-hard magnetic alloy prepared by MIM technology |
title_full_unstemmed | Structural features of near equiatomic FeCo-2V semi-hard magnetic alloy prepared by MIM technology |
title_short | Structural features of near equiatomic FeCo-2V semi-hard magnetic alloy prepared by MIM technology |
title_sort | structural features of near equiatomic feco 2v semi hard magnetic alloy prepared by mim technology |
topic | fecov alloy mim technology structural properties particle size dmax feret x |
url | https://doiserbia.nb.rs/img/doi/0350-820X/2024/0350-820X2300055N.pdf |
work_keys_str_mv | AT nedeljkovicborivoje structuralfeaturesofnearequiatomicfeco2vsemihardmagneticalloypreparedbymimtechnology AT pavlovicvladimirb structuralfeaturesofnearequiatomicfeco2vsemihardmagneticalloypreparedbymimtechnology AT obradovicnina structuralfeaturesofnearequiatomicfeco2vsemihardmagneticalloypreparedbymimtechnology AT mitrovicnebojsa structuralfeaturesofnearequiatomicfeco2vsemihardmagneticalloypreparedbymimtechnology |