New Method for <i>Lawsonia intracelullaris</i> Quantification Based on Optical Density by Spectrophotometry

Studies investigating the pathogenesis of <i>Lawsonia intracellularis</i> often require bacterial quantification in suspension. However, due to the organism’s fastidious growth requirements—being both intracellular and microaerophilic—traditional quantification methods, such as colony-fo...

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Main Authors: Mirtha E. Suarez-Duarte, Ricardo P. Laub, Renato L. Santos, Carlos E. R. Pereira, Talita P. Resende, Matheus D. Araujo, Paula A. Correia, Jessica C. R. Barbosa, Roberto M. C. Guedes
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Language:English
Published: MDPI AG 2025-03-01
Series:Microorganisms
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Online Access:https://www.mdpi.com/2076-2607/13/3/568
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author Mirtha E. Suarez-Duarte
Ricardo P. Laub
Renato L. Santos
Carlos E. R. Pereira
Talita P. Resende
Matheus D. Araujo
Paula A. Correia
Jessica C. R. Barbosa
Roberto M. C. Guedes
author_facet Mirtha E. Suarez-Duarte
Ricardo P. Laub
Renato L. Santos
Carlos E. R. Pereira
Talita P. Resende
Matheus D. Araujo
Paula A. Correia
Jessica C. R. Barbosa
Roberto M. C. Guedes
author_sort Mirtha E. Suarez-Duarte
collection DOAJ
description Studies investigating the pathogenesis of <i>Lawsonia intracellularis</i> often require bacterial quantification in suspension. However, due to the organism’s fastidious growth requirements—being both intracellular and microaerophilic—traditional quantification methods, such as colony-forming unit counting, are not feasible. Currently, the only widely available method for quantifying <i>L. intracellularis</i> is real-time quantitative PCR (RT-qPCR). Unfortunately, the time required to perform RT-qPCR is incompatible with the bacterium’s limited survival outside its intracellular and microaerophilic environment. As a result, bacterial suspensions are typically quantified subjectively, based on the researcher’s experience for immediate use, with RT-qPCR conducted afterward. Optical density (OD) spectrophotometry is a rapid, although indirect, method of estimating bacterial concentrations in suspension, and it has been applied successfully to fast-growing prokaryotic species. Therefore, the objective of this study was to determine the correlation between RT-qPCR results and the optical density of <i>L. intracellularis</i> suspensions, with the goal of enabling the use of spectrophotometry for immediate bacterial quantification in experimental settings. Optical densities (ODs) were measured at 405 nm and 450 nm, using either a cuvette or microplate, while RT-qPCR was employed to establish a standard curve from samples of known concentration and to quantify the concentration of <i>L. intracellularis</i> in the test suspensions. Four comparison variations between OD and RT-qPCR were evaluated: (1) spectrophotometry at 405 nm using a cuvette vs. RT-qPCR; (2) spectrophotometry at 405 nm using a microplate vs. RT-qPCR; (3) spectrophotometry at 450 nm using a cuvette vs. RT-qPCR; and (4) spectrophotometry at 450 nm using a microplate vs. RT-qPCR. The tests were conducted in two independent replications, with each sample analyzed in duplicate. In all variations, the correlation between the bacterial concentrations determined by RT-qPCR and those estimated by OD was greater than 80%, with a statistical significance of <i>p</i> < 0.05. The following OD conversion equations for determining the number of microorganisms/mL were obtained: (1) f(x) = −7.438 × 10<sup>8</sup> + 1.797 × 10<sup>10</sup>. x; (2) f(x) = 3.255 × 10<sup>8</sup> + 3.003 × 10<sup>9</sup>. x; (3) f(x) = −8.006 × 10<sup>8</sup> + 2.169 × 10<sup>10</sup>. x; (4) f(x) = 3.107 × 10<sup>8</sup> + 3.758 × 10<sup>9</sup>. x. Here, “X” is the Ct value obtained by RT-qPCR. These findings enable researchers to improve the accuracy of their <i>L. intracellularis</i> experiments by utilizing optical spectrometry—a straightforward method that provides immediate results for determining bacterial concentration in suspensions.
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spelling doaj-art-eabf316728d249658d4c8da91c8bc4ba2025-08-20T03:43:10ZengMDPI AGMicroorganisms2076-26072025-03-0113356810.3390/microorganisms13030568New Method for <i>Lawsonia intracelullaris</i> Quantification Based on Optical Density by SpectrophotometryMirtha E. Suarez-Duarte0Ricardo P. Laub1Renato L. Santos2Carlos E. R. Pereira3Talita P. Resende4Matheus D. Araujo5Paula A. Correia6Jessica C. R. Barbosa7Roberto M. C. Guedes8Department of Clinic and Surgery, Veterinary School, Universidade Federal de Minas Gerais, Belo Horizonte 31270, Minas Gerais, BrazilDepartment of Clinic and Surgery, Veterinary School, Universidade Federal de Minas Gerais, Belo Horizonte 31270, Minas Gerais, BrazilDepartment of Clinic and Surgery, Veterinary School, Universidade Federal de Minas Gerais, Belo Horizonte 31270, Minas Gerais, BrazilDepartment of Veterinary, Universidade Federal de Viçosa, Belo Horizonte 31270, Minas Gerais, BrazilDepartment of Animal Science, College of Food, Agriculture and Environmental Sciences, Ohio State University, Columbus, OH 43210, USADepartment of Clinic and Surgery, Veterinary School, Universidade Federal de Minas Gerais, Belo Horizonte 31270, Minas Gerais, BrazilDepartment of Clinic and Surgery, Veterinary School, Universidade Federal de Minas Gerais, Belo Horizonte 31270, Minas Gerais, BrazilDepartment of Clinic and Surgery, Veterinary School, Universidade Federal de Minas Gerais, Belo Horizonte 31270, Minas Gerais, BrazilDepartment of Clinic and Surgery, Veterinary School, Universidade Federal de Minas Gerais, Belo Horizonte 31270, Minas Gerais, BrazilStudies investigating the pathogenesis of <i>Lawsonia intracellularis</i> often require bacterial quantification in suspension. However, due to the organism’s fastidious growth requirements—being both intracellular and microaerophilic—traditional quantification methods, such as colony-forming unit counting, are not feasible. Currently, the only widely available method for quantifying <i>L. intracellularis</i> is real-time quantitative PCR (RT-qPCR). Unfortunately, the time required to perform RT-qPCR is incompatible with the bacterium’s limited survival outside its intracellular and microaerophilic environment. As a result, bacterial suspensions are typically quantified subjectively, based on the researcher’s experience for immediate use, with RT-qPCR conducted afterward. Optical density (OD) spectrophotometry is a rapid, although indirect, method of estimating bacterial concentrations in suspension, and it has been applied successfully to fast-growing prokaryotic species. Therefore, the objective of this study was to determine the correlation between RT-qPCR results and the optical density of <i>L. intracellularis</i> suspensions, with the goal of enabling the use of spectrophotometry for immediate bacterial quantification in experimental settings. Optical densities (ODs) were measured at 405 nm and 450 nm, using either a cuvette or microplate, while RT-qPCR was employed to establish a standard curve from samples of known concentration and to quantify the concentration of <i>L. intracellularis</i> in the test suspensions. Four comparison variations between OD and RT-qPCR were evaluated: (1) spectrophotometry at 405 nm using a cuvette vs. RT-qPCR; (2) spectrophotometry at 405 nm using a microplate vs. RT-qPCR; (3) spectrophotometry at 450 nm using a cuvette vs. RT-qPCR; and (4) spectrophotometry at 450 nm using a microplate vs. RT-qPCR. The tests were conducted in two independent replications, with each sample analyzed in duplicate. In all variations, the correlation between the bacterial concentrations determined by RT-qPCR and those estimated by OD was greater than 80%, with a statistical significance of <i>p</i> < 0.05. The following OD conversion equations for determining the number of microorganisms/mL were obtained: (1) f(x) = −7.438 × 10<sup>8</sup> + 1.797 × 10<sup>10</sup>. x; (2) f(x) = 3.255 × 10<sup>8</sup> + 3.003 × 10<sup>9</sup>. x; (3) f(x) = −8.006 × 10<sup>8</sup> + 2.169 × 10<sup>10</sup>. x; (4) f(x) = 3.107 × 10<sup>8</sup> + 3.758 × 10<sup>9</sup>. x. Here, “X” is the Ct value obtained by RT-qPCR. These findings enable researchers to improve the accuracy of their <i>L. intracellularis</i> experiments by utilizing optical spectrometry—a straightforward method that provides immediate results for determining bacterial concentration in suspensions.https://www.mdpi.com/2076-2607/13/3/568optical densityproliferative enteropathyindirect countingRT-qPCRspectrophotometer
spellingShingle Mirtha E. Suarez-Duarte
Ricardo P. Laub
Renato L. Santos
Carlos E. R. Pereira
Talita P. Resende
Matheus D. Araujo
Paula A. Correia
Jessica C. R. Barbosa
Roberto M. C. Guedes
New Method for <i>Lawsonia intracelullaris</i> Quantification Based on Optical Density by Spectrophotometry
Microorganisms
optical density
proliferative enteropathy
indirect counting
RT-qPCR
spectrophotometer
title New Method for <i>Lawsonia intracelullaris</i> Quantification Based on Optical Density by Spectrophotometry
title_full New Method for <i>Lawsonia intracelullaris</i> Quantification Based on Optical Density by Spectrophotometry
title_fullStr New Method for <i>Lawsonia intracelullaris</i> Quantification Based on Optical Density by Spectrophotometry
title_full_unstemmed New Method for <i>Lawsonia intracelullaris</i> Quantification Based on Optical Density by Spectrophotometry
title_short New Method for <i>Lawsonia intracelullaris</i> Quantification Based on Optical Density by Spectrophotometry
title_sort new method for i lawsonia intracelullaris i quantification based on optical density by spectrophotometry
topic optical density
proliferative enteropathy
indirect counting
RT-qPCR
spectrophotometer
url https://www.mdpi.com/2076-2607/13/3/568
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