Mesoporous Metal-Containing Carbon Nitrides for Improved Photocatalytic Activities

Graphitic carbon nitrides (g-C3N4) have attracted increasing interest due to their unusual properties and promising applications in water splitting, heterogeneous catalysis, and organic contaminant degradation. In this study, a new method was developed for the synthesis of mesoporous Fe contained g-...

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Main Authors: Jie Luo, Zhao-Jie Cui, Guo-Long Zang
Format: Article
Language:English
Published: Wiley 2013-01-01
Series:Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2013/945348
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author Jie Luo
Zhao-Jie Cui
Guo-Long Zang
author_facet Jie Luo
Zhao-Jie Cui
Guo-Long Zang
author_sort Jie Luo
collection DOAJ
description Graphitic carbon nitrides (g-C3N4) have attracted increasing interest due to their unusual properties and promising applications in water splitting, heterogeneous catalysis, and organic contaminant degradation. In this study, a new method was developed for the synthesis of mesoporous Fe contained g-C3N4 (m-Fe-C3N4) photocatalyst by using SiO2 nanoparticles as hard template and dicyandiamide as precursor. The physicochemical properties of m-Fe-C3N4 were thoroughly investigated. The XRD and XPS results indicated that Fe was strongly coordinated with the g-C3N4 matrix and that the doping and mesoporous structure partially deteriorated its crystalline structure. The UV-visible absorption spectra revealed that m-Fe-C3N4 with a unique electronic structure displays an increased band gap in combination with a slightly reduced absorbance, implying that mesoporous structure modified the electronic properties of g-Fe-C3N4. The photocatalytic activity of m-Fe-C3N4 for photodegradation of Rhodamine B (RhB) was much higher than that of g-Fe-C3N4, clearly demonstrating porous structure positive effect.
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spelling doaj-art-e9e55c8bcdad4f50aa7e674e4fc173632025-08-20T03:20:40ZengWileyJournal of Chemistry2090-90632090-90712013-01-01201310.1155/2013/945348945348Mesoporous Metal-Containing Carbon Nitrides for Improved Photocatalytic ActivitiesJie Luo0Zhao-Jie Cui1Guo-Long Zang2School of Environmental Science and Engineering, Shandong University, Jinan 250100, ChinaSchool of Environmental Science and Engineering, Shandong University, Jinan 250100, ChinaTianjin Renewable Resources Institute, All China Federation of Supply and Marketing Cooperatives, Tianjin 300191, ChinaGraphitic carbon nitrides (g-C3N4) have attracted increasing interest due to their unusual properties and promising applications in water splitting, heterogeneous catalysis, and organic contaminant degradation. In this study, a new method was developed for the synthesis of mesoporous Fe contained g-C3N4 (m-Fe-C3N4) photocatalyst by using SiO2 nanoparticles as hard template and dicyandiamide as precursor. The physicochemical properties of m-Fe-C3N4 were thoroughly investigated. The XRD and XPS results indicated that Fe was strongly coordinated with the g-C3N4 matrix and that the doping and mesoporous structure partially deteriorated its crystalline structure. The UV-visible absorption spectra revealed that m-Fe-C3N4 with a unique electronic structure displays an increased band gap in combination with a slightly reduced absorbance, implying that mesoporous structure modified the electronic properties of g-Fe-C3N4. The photocatalytic activity of m-Fe-C3N4 for photodegradation of Rhodamine B (RhB) was much higher than that of g-Fe-C3N4, clearly demonstrating porous structure positive effect.http://dx.doi.org/10.1155/2013/945348
spellingShingle Jie Luo
Zhao-Jie Cui
Guo-Long Zang
Mesoporous Metal-Containing Carbon Nitrides for Improved Photocatalytic Activities
Journal of Chemistry
title Mesoporous Metal-Containing Carbon Nitrides for Improved Photocatalytic Activities
title_full Mesoporous Metal-Containing Carbon Nitrides for Improved Photocatalytic Activities
title_fullStr Mesoporous Metal-Containing Carbon Nitrides for Improved Photocatalytic Activities
title_full_unstemmed Mesoporous Metal-Containing Carbon Nitrides for Improved Photocatalytic Activities
title_short Mesoporous Metal-Containing Carbon Nitrides for Improved Photocatalytic Activities
title_sort mesoporous metal containing carbon nitrides for improved photocatalytic activities
url http://dx.doi.org/10.1155/2013/945348
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AT zhaojiecui mesoporousmetalcontainingcarbonnitridesforimprovedphotocatalyticactivities
AT guolongzang mesoporousmetalcontainingcarbonnitridesforimprovedphotocatalyticactivities