Synthesis and Characterization of Dodecylbenzene Sulfonic Acid doped Tetraaniline via Emulsion Polymerization
In this work, we report preparation and characterization of dodecylbenzene sulfonic acid (DBSA) doped tetraaniline via micelles assisted method using ammonium per sulphate (APS) as an oxidant. Here, DBSA act as dopant as well as template for tetraaniline nanostructures. The synthesized DBSA doped te...
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| Format: | Article |
| Language: | English |
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Wiley
2012-01-01
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| Series: | E-Journal of Chemistry |
| Online Access: | http://dx.doi.org/10.1155/2012/692853 |
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| author | K. Basavaiah K. Tirumala Rao A. V. Prasada Rao |
| author_facet | K. Basavaiah K. Tirumala Rao A. V. Prasada Rao |
| author_sort | K. Basavaiah |
| collection | DOAJ |
| description | In this work, we report preparation and characterization of dodecylbenzene sulfonic acid (DBSA) doped tetraaniline via micelles assisted method using ammonium per sulphate (APS) as an oxidant. Here, DBSA act as dopant as well as template for tetraaniline nanostructures. The synthesized DBSA doped tetraaniline have been well characterized by X-ray diffraction patterns, Fourier transform infrared spectroscopy, UV-Visible spectroscopy, Scanning electron microscopy and thermogravimetry. The morphologies of tetraaniline were found to be dependent on molar ratios of N-phenyl-1, 4-phenylenediamine to DBSA. The spectroscopic data indicated that DBSA doped tetraaniline. Thermogravimetry studies revealed that the DBSA doping improved the thermal stability of tetraaniline. |
| format | Article |
| id | doaj-art-e98e4e63763b4d0299956f177de0ccbc |
| institution | Kabale University |
| issn | 0973-4945 2090-9810 |
| language | English |
| publishDate | 2012-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | E-Journal of Chemistry |
| spelling | doaj-art-e98e4e63763b4d0299956f177de0ccbc2025-02-03T01:32:04ZengWileyE-Journal of Chemistry0973-49452090-98102012-01-01931342134610.1155/2012/692853Synthesis and Characterization of Dodecylbenzene Sulfonic Acid doped Tetraaniline via Emulsion PolymerizationK. Basavaiah0K. Tirumala Rao1A. V. Prasada Rao2Department of Inorganic and Analytical Chemistry, Andhra University, Visakhapatnam -530003, IndiaDepartment of Inorganic and Analytical Chemistry, Andhra University, Visakhapatnam -530003, IndiaDepartment of Inorganic and Analytical Chemistry, Andhra University, Visakhapatnam -530003, IndiaIn this work, we report preparation and characterization of dodecylbenzene sulfonic acid (DBSA) doped tetraaniline via micelles assisted method using ammonium per sulphate (APS) as an oxidant. Here, DBSA act as dopant as well as template for tetraaniline nanostructures. The synthesized DBSA doped tetraaniline have been well characterized by X-ray diffraction patterns, Fourier transform infrared spectroscopy, UV-Visible spectroscopy, Scanning electron microscopy and thermogravimetry. The morphologies of tetraaniline were found to be dependent on molar ratios of N-phenyl-1, 4-phenylenediamine to DBSA. The spectroscopic data indicated that DBSA doped tetraaniline. Thermogravimetry studies revealed that the DBSA doping improved the thermal stability of tetraaniline.http://dx.doi.org/10.1155/2012/692853 |
| spellingShingle | K. Basavaiah K. Tirumala Rao A. V. Prasada Rao Synthesis and Characterization of Dodecylbenzene Sulfonic Acid doped Tetraaniline via Emulsion Polymerization E-Journal of Chemistry |
| title | Synthesis and Characterization of Dodecylbenzene Sulfonic Acid doped Tetraaniline via Emulsion Polymerization |
| title_full | Synthesis and Characterization of Dodecylbenzene Sulfonic Acid doped Tetraaniline via Emulsion Polymerization |
| title_fullStr | Synthesis and Characterization of Dodecylbenzene Sulfonic Acid doped Tetraaniline via Emulsion Polymerization |
| title_full_unstemmed | Synthesis and Characterization of Dodecylbenzene Sulfonic Acid doped Tetraaniline via Emulsion Polymerization |
| title_short | Synthesis and Characterization of Dodecylbenzene Sulfonic Acid doped Tetraaniline via Emulsion Polymerization |
| title_sort | synthesis and characterization of dodecylbenzene sulfonic acid doped tetraaniline via emulsion polymerization |
| url | http://dx.doi.org/10.1155/2012/692853 |
| work_keys_str_mv | AT kbasavaiah synthesisandcharacterizationofdodecylbenzenesulfonicaciddopedtetraanilineviaemulsionpolymerization AT ktirumalarao synthesisandcharacterizationofdodecylbenzenesulfonicaciddopedtetraanilineviaemulsionpolymerization AT avprasadarao synthesisandcharacterizationofdodecylbenzenesulfonicaciddopedtetraanilineviaemulsionpolymerization |