Quantitative Characterization of Full-Spectrum Pore Size and Connectivity for Shale with Different Sedimentary Facies from the Dongying Depression, Bohai Bay Basin, East China

Working with shales in the fourth member of Shahejie Formation in the Dongying Depression in Bohai Bay Basin of East China, this study examines the facies classification, petrological characteristics, pore size distribution, and pore connectivity of oil-producing shale. The studied shales could be c...

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Main Authors: Yushan Du, Na Yin, Qinhong Hu, Mianmo Meng, Xiuchuan Zhu, Jing Chao, Cunfei Ma
Format: Article
Language:English
Published: Wiley 2022-01-01
Series:Geofluids
Online Access:http://dx.doi.org/10.1155/2022/9744086
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author Yushan Du
Na Yin
Qinhong Hu
Mianmo Meng
Xiuchuan Zhu
Jing Chao
Cunfei Ma
author_facet Yushan Du
Na Yin
Qinhong Hu
Mianmo Meng
Xiuchuan Zhu
Jing Chao
Cunfei Ma
author_sort Yushan Du
collection DOAJ
description Working with shales in the fourth member of Shahejie Formation in the Dongying Depression in Bohai Bay Basin of East China, this study examines the facies classification, petrological characteristics, pore size distribution, and pore connectivity of oil-producing shale. The studied shales could be classified into five sedimentary facies according to a three-step classification criterion that consists of total organic carbon (TOC), sedimentary structure, and mineral composition. Among them, the “low TOC massive siliceous mudstone” and “low TOC layered clayey mudstone” facies have similar distributions from low-pressure N2 physisorption, and the incremental volume within the 3-30 nm pore size range is much higher than the “high TOC laminated clayey marlstone” and “low TOC layered siliceous marlstone” facies. The T2 spectra of nuclear magnetic resonance tests for the “high TOC laminated clayey marlstone” facies which contains abundant calcite laminae and organic matter-hosted pores commonly show three peaks, with a dominant peak at less than 300 nm in diameter and good pore connectivity. The T2 spectra of three other facies are both characterized by two peaks, and the main peak of the “low TOC layered siliceous marlstone” and “low TOC layered clayey mudstone” facies has a similar range at 2-500 nm, in contrast with 1-17 nm for the “low TOC massive siliceous mudstone” facies. Pores in these four facies are mainly at nanoscales with predominant pore-throat diameters at less than 50 nm; however, the “high TOC laminated clayey marlstone” facies has the largest peak in the range of >1 μm, possibly because of its interlaminar structure and microcracks. The spontaneous imbibition experiments using two distinct fluids indicated that all of four facies have a much better pore connectivity towards the hydrophilic fluid than these experienced by the hydrophobic fluid.
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issn 1468-8123
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spelling doaj-art-e77f00507aa641dda6b604a3d44550b92025-02-03T05:53:28ZengWileyGeofluids1468-81232022-01-01202210.1155/2022/9744086Quantitative Characterization of Full-Spectrum Pore Size and Connectivity for Shale with Different Sedimentary Facies from the Dongying Depression, Bohai Bay Basin, East ChinaYushan Du0Na Yin1Qinhong Hu2Mianmo Meng3Xiuchuan Zhu4Jing Chao5Cunfei Ma6Exploration and Production Research Institute of Shengli Oilfield CompanyShandong Provincial Key Laboratory of Deep Oil and GasDepartment of Earth and Environmental SciencesHubei Key Laboratory of Marine Geological ResourcesShandong Provincial Key Laboratory of Deep Oil and GasExploration and Production Research Institute of Shengli Oilfield CompanyShandong Provincial Key Laboratory of Deep Oil and GasWorking with shales in the fourth member of Shahejie Formation in the Dongying Depression in Bohai Bay Basin of East China, this study examines the facies classification, petrological characteristics, pore size distribution, and pore connectivity of oil-producing shale. The studied shales could be classified into five sedimentary facies according to a three-step classification criterion that consists of total organic carbon (TOC), sedimentary structure, and mineral composition. Among them, the “low TOC massive siliceous mudstone” and “low TOC layered clayey mudstone” facies have similar distributions from low-pressure N2 physisorption, and the incremental volume within the 3-30 nm pore size range is much higher than the “high TOC laminated clayey marlstone” and “low TOC layered siliceous marlstone” facies. The T2 spectra of nuclear magnetic resonance tests for the “high TOC laminated clayey marlstone” facies which contains abundant calcite laminae and organic matter-hosted pores commonly show three peaks, with a dominant peak at less than 300 nm in diameter and good pore connectivity. The T2 spectra of three other facies are both characterized by two peaks, and the main peak of the “low TOC layered siliceous marlstone” and “low TOC layered clayey mudstone” facies has a similar range at 2-500 nm, in contrast with 1-17 nm for the “low TOC massive siliceous mudstone” facies. Pores in these four facies are mainly at nanoscales with predominant pore-throat diameters at less than 50 nm; however, the “high TOC laminated clayey marlstone” facies has the largest peak in the range of >1 μm, possibly because of its interlaminar structure and microcracks. The spontaneous imbibition experiments using two distinct fluids indicated that all of four facies have a much better pore connectivity towards the hydrophilic fluid than these experienced by the hydrophobic fluid.http://dx.doi.org/10.1155/2022/9744086
spellingShingle Yushan Du
Na Yin
Qinhong Hu
Mianmo Meng
Xiuchuan Zhu
Jing Chao
Cunfei Ma
Quantitative Characterization of Full-Spectrum Pore Size and Connectivity for Shale with Different Sedimentary Facies from the Dongying Depression, Bohai Bay Basin, East China
Geofluids
title Quantitative Characterization of Full-Spectrum Pore Size and Connectivity for Shale with Different Sedimentary Facies from the Dongying Depression, Bohai Bay Basin, East China
title_full Quantitative Characterization of Full-Spectrum Pore Size and Connectivity for Shale with Different Sedimentary Facies from the Dongying Depression, Bohai Bay Basin, East China
title_fullStr Quantitative Characterization of Full-Spectrum Pore Size and Connectivity for Shale with Different Sedimentary Facies from the Dongying Depression, Bohai Bay Basin, East China
title_full_unstemmed Quantitative Characterization of Full-Spectrum Pore Size and Connectivity for Shale with Different Sedimentary Facies from the Dongying Depression, Bohai Bay Basin, East China
title_short Quantitative Characterization of Full-Spectrum Pore Size and Connectivity for Shale with Different Sedimentary Facies from the Dongying Depression, Bohai Bay Basin, East China
title_sort quantitative characterization of full spectrum pore size and connectivity for shale with different sedimentary facies from the dongying depression bohai bay basin east china
url http://dx.doi.org/10.1155/2022/9744086
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