Dynamic Mechanical, Dielectrical, and Rheological Analysis of Polyethylene Terephthalate/Carbon Nanotube Nanocomposites Prepared by Melt Processing
The polyethylene terephthalate/carbon nanotube (PET/CNT) nanocomposites were prepared by melt mixing using a twin screw extruder. CNT content was varied up to 5 wt. %. Morphology as well as dynamic mechanical, calorimetric, and rheological properties of the PET/CNT nanocomposites was investigated. M...
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Format: | Article |
Language: | English |
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Wiley
2020-01-01
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Series: | International Journal of Polymer Science |
Online Access: | http://dx.doi.org/10.1155/2020/5715463 |
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author | Juris Bitenieks Remo Merijs Meri Janis Zicans Krisjanis Buks |
author_facet | Juris Bitenieks Remo Merijs Meri Janis Zicans Krisjanis Buks |
author_sort | Juris Bitenieks |
collection | DOAJ |
description | The polyethylene terephthalate/carbon nanotube (PET/CNT) nanocomposites were prepared by melt mixing using a twin screw extruder. CNT content was varied up to 5 wt. %. Morphology as well as dynamic mechanical, calorimetric, and rheological properties of the PET/CNT nanocomposites was investigated. Morphological studies indicated that CNT bundles are regularly distributed within the polymer matrix creating a connected network structure which significantly affects the nanocomposite properties. Dynamic mechanical thermal analysis revealed increase in storage and loss modules of the investigated PET nanocomposites by increasing the content of CNTs. Differential scanning calorimetry results demonstrated increase in crystallinity of the investigated PET nanocomposites upon addition of the nanofiller. Rheological studies demonstrated that CNT addition up to 5 wt. % caused increment in complex viscosity and storage modulus. Rheological percolation threshold was observed to be 0.83 wt. % of CNT concentration, respectively. |
format | Article |
id | doaj-art-e72e415a3aaa49a0a89b5a62ee41010e |
institution | Kabale University |
issn | 1687-9422 1687-9430 |
language | English |
publishDate | 2020-01-01 |
publisher | Wiley |
record_format | Article |
series | International Journal of Polymer Science |
spelling | doaj-art-e72e415a3aaa49a0a89b5a62ee41010e2025-02-03T05:52:29ZengWileyInternational Journal of Polymer Science1687-94221687-94302020-01-01202010.1155/2020/57154635715463Dynamic Mechanical, Dielectrical, and Rheological Analysis of Polyethylene Terephthalate/Carbon Nanotube Nanocomposites Prepared by Melt ProcessingJuris Bitenieks0Remo Merijs Meri1Janis Zicans2Krisjanis Buks3Institute of Polymer Materials, Faculty of Materials Science and Applied Chemistry, Riga Technical University, LatviaInstitute of Polymer Materials, Faculty of Materials Science and Applied Chemistry, Riga Technical University, LatviaInstitute of Polymer Materials, Faculty of Materials Science and Applied Chemistry, Riga Technical University, LatviaInstitute of Chemical Physics, University of Latvia, LatviaThe polyethylene terephthalate/carbon nanotube (PET/CNT) nanocomposites were prepared by melt mixing using a twin screw extruder. CNT content was varied up to 5 wt. %. Morphology as well as dynamic mechanical, calorimetric, and rheological properties of the PET/CNT nanocomposites was investigated. Morphological studies indicated that CNT bundles are regularly distributed within the polymer matrix creating a connected network structure which significantly affects the nanocomposite properties. Dynamic mechanical thermal analysis revealed increase in storage and loss modules of the investigated PET nanocomposites by increasing the content of CNTs. Differential scanning calorimetry results demonstrated increase in crystallinity of the investigated PET nanocomposites upon addition of the nanofiller. Rheological studies demonstrated that CNT addition up to 5 wt. % caused increment in complex viscosity and storage modulus. Rheological percolation threshold was observed to be 0.83 wt. % of CNT concentration, respectively.http://dx.doi.org/10.1155/2020/5715463 |
spellingShingle | Juris Bitenieks Remo Merijs Meri Janis Zicans Krisjanis Buks Dynamic Mechanical, Dielectrical, and Rheological Analysis of Polyethylene Terephthalate/Carbon Nanotube Nanocomposites Prepared by Melt Processing International Journal of Polymer Science |
title | Dynamic Mechanical, Dielectrical, and Rheological Analysis of Polyethylene Terephthalate/Carbon Nanotube Nanocomposites Prepared by Melt Processing |
title_full | Dynamic Mechanical, Dielectrical, and Rheological Analysis of Polyethylene Terephthalate/Carbon Nanotube Nanocomposites Prepared by Melt Processing |
title_fullStr | Dynamic Mechanical, Dielectrical, and Rheological Analysis of Polyethylene Terephthalate/Carbon Nanotube Nanocomposites Prepared by Melt Processing |
title_full_unstemmed | Dynamic Mechanical, Dielectrical, and Rheological Analysis of Polyethylene Terephthalate/Carbon Nanotube Nanocomposites Prepared by Melt Processing |
title_short | Dynamic Mechanical, Dielectrical, and Rheological Analysis of Polyethylene Terephthalate/Carbon Nanotube Nanocomposites Prepared by Melt Processing |
title_sort | dynamic mechanical dielectrical and rheological analysis of polyethylene terephthalate carbon nanotube nanocomposites prepared by melt processing |
url | http://dx.doi.org/10.1155/2020/5715463 |
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