Matrix stiffness-dependent PD-L2 deficiency improves SMYD3/xCT-mediated ferroptosis and the efficacy of anti-PD-1 in HCC

Introduction: Heterogeneous tissue stiffening promotes tumor progression and resistance, and predicts a poor clinical outcome in patients with hepatocellular carcinoma (HCC). Ferroptosis, a congenital tumor suppressive mechanism, mediates the anticancer activity of various tumor suppressors, includi...

Full description

Saved in:
Bibliographic Details
Main Authors: Shunxi Wang, Xiaoxue Yuan, Zetao Yang, Xuan Zhang, Zhiling Xu, Li Yang, Xian Yang, Wei Zhou, Wanqian Liu
Format: Article
Language:English
Published: Elsevier 2025-07-01
Series:Journal of Advanced Research
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2090123224003631
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849329442341519360
author Shunxi Wang
Xiaoxue Yuan
Zetao Yang
Xuan Zhang
Zhiling Xu
Li Yang
Xian Yang
Wei Zhou
Wanqian Liu
author_facet Shunxi Wang
Xiaoxue Yuan
Zetao Yang
Xuan Zhang
Zhiling Xu
Li Yang
Xian Yang
Wei Zhou
Wanqian Liu
author_sort Shunxi Wang
collection DOAJ
description Introduction: Heterogeneous tissue stiffening promotes tumor progression and resistance, and predicts a poor clinical outcome in patients with hepatocellular carcinoma (HCC). Ferroptosis, a congenital tumor suppressive mechanism, mediates the anticancer activity of various tumor suppressors, including immune checkpoint inhibitors, and its induction is currently considered a promising treatment strategy. However, the role of extracellular matrix (ECM) stiffness in regulating ferroptosis and ferroptosis-targeted resistance in HCC remains unclear. Objectives: This research aimed to explore how extracellular matrix stiffness affects ferroptosis and its treatment efficacy in HCC. Methods: Ferroptosis analysis was confirmed via cell activity, intracellular ferrous irons, and mitochondrial pathology assays. Baseline PD-L2, SMYD3, and SLC7A11 (xCT) were evaluated in 67 sorafenib-treated patients with HCC (46 for non-responder and 21 for responder) from public data. The combined efficacy of shPD-L2, sorafenib, and anti-PD-1 antibody in HCC was investigated in vivo. Results: Here, we revealed that matrix stiffness-induced PD-L2 functions as a suppressor of xCT-mediated ferroptosis to promote cancer growth and sorafenib resistance in patients with HCC. Mechanically, matrix stiffening induced the expression of PD-L2 by activating SMYD3/H3K4me3, which acts as an RNA binding protein to enhance the mRNA stability of FTL and elevate its protein level. Knockdown of PD-L2 significantly promoted xCT-mediated ferroptosis induced by RSL3 or sorafenib on stiff substrate via FTL, whereas its overexpression abolished these upward trends. Notably, PD-L2 deletion in combination with sorafenib and anti-PD-1 antibody significantly sensitized HCC cells and blunted cancer growth in vivo. Additionally, we found the ferroptosis- and immune checkpoint-related prognostic genes that combined PD-L2, SLC7A11 and SYMD3 well predict the clinical efficacy of sorafenib in patients with HCC. Conclusion: These findings expand our understanding of the mechanics-dependent PD-L2 role in ferroptosis, cancer progression and resistance, providing a basis for the clinical translation of PD-L2 as a therapeutic target or diagnostic biomarker.
format Article
id doaj-art-e66559312ebb4e0d8f05945e65dce14c
institution Kabale University
issn 2090-1232
language English
publishDate 2025-07-01
publisher Elsevier
record_format Article
series Journal of Advanced Research
spelling doaj-art-e66559312ebb4e0d8f05945e65dce14c2025-08-20T03:47:16ZengElsevierJournal of Advanced Research2090-12322025-07-017326528210.1016/j.jare.2024.08.021Matrix stiffness-dependent PD-L2 deficiency improves SMYD3/xCT-mediated ferroptosis and the efficacy of anti-PD-1 in HCCShunxi Wang0Xiaoxue Yuan1Zetao Yang2Xuan Zhang3Zhiling Xu4Li Yang5Xian Yang6Wei Zhou7Wanqian Liu8Key Laboratory of Biorheological Science and Technology, Ministry of Education& 111 Project Laboratory of Biomechanics and Tissue Repair, Bioengineering College, Chongqing University, Chongqing 400044, ChinaKey Laboratory of Biorheological Science and Technology, Ministry of Education& 111 Project Laboratory of Biomechanics and Tissue Repair, Bioengineering College, Chongqing University, Chongqing 400044, ChinaKey Laboratory of Biorheological Science and Technology, Ministry of Education& 111 Project Laboratory of Biomechanics and Tissue Repair, Bioengineering College, Chongqing University, Chongqing 400044, ChinaKey Laboratory of Biorheological Science and Technology, Ministry of Education& 111 Project Laboratory of Biomechanics and Tissue Repair, Bioengineering College, Chongqing University, Chongqing 400044, ChinaKey Laboratory of Biorheological Science and Technology, Ministry of Education& 111 Project Laboratory of Biomechanics and Tissue Repair, Bioengineering College, Chongqing University, Chongqing 400044, ChinaKey Laboratory of Biorheological Science and Technology, Ministry of Education& 111 Project Laboratory of Biomechanics and Tissue Repair, Bioengineering College, Chongqing University, Chongqing 400044, ChinaKey Laboratory of Biorheological Science and Technology, Ministry of Education& 111 Project Laboratory of Biomechanics and Tissue Repair, Bioengineering College, Chongqing University, Chongqing 400044, ChinaChongqing Key Laboratory of Translational Research for Cancer Metastasis and Individualized Treatment, Chongqing University Cancer Hospital, Chongqing 400030, China; Department of Radiation Oncology, Chongqing University Cancer Hospital, Chongqing, China; Corresponding author at: Chongqing Key Laboratory of Translational Research for Cancer Metastasis and Individualized Treatment, Chongqing University Cancer Hospital, Chongqing 400030, China.Key Laboratory of Biorheological Science and Technology, Ministry of Education& 111 Project Laboratory of Biomechanics and Tissue Repair, Bioengineering College, Chongqing University, Chongqing 400044, China; Corresponding author at: Bioengineering Institute of Chongqing University, 174 Shazheng Street, Chongqing 400044, China.Introduction: Heterogeneous tissue stiffening promotes tumor progression and resistance, and predicts a poor clinical outcome in patients with hepatocellular carcinoma (HCC). Ferroptosis, a congenital tumor suppressive mechanism, mediates the anticancer activity of various tumor suppressors, including immune checkpoint inhibitors, and its induction is currently considered a promising treatment strategy. However, the role of extracellular matrix (ECM) stiffness in regulating ferroptosis and ferroptosis-targeted resistance in HCC remains unclear. Objectives: This research aimed to explore how extracellular matrix stiffness affects ferroptosis and its treatment efficacy in HCC. Methods: Ferroptosis analysis was confirmed via cell activity, intracellular ferrous irons, and mitochondrial pathology assays. Baseline PD-L2, SMYD3, and SLC7A11 (xCT) were evaluated in 67 sorafenib-treated patients with HCC (46 for non-responder and 21 for responder) from public data. The combined efficacy of shPD-L2, sorafenib, and anti-PD-1 antibody in HCC was investigated in vivo. Results: Here, we revealed that matrix stiffness-induced PD-L2 functions as a suppressor of xCT-mediated ferroptosis to promote cancer growth and sorafenib resistance in patients with HCC. Mechanically, matrix stiffening induced the expression of PD-L2 by activating SMYD3/H3K4me3, which acts as an RNA binding protein to enhance the mRNA stability of FTL and elevate its protein level. Knockdown of PD-L2 significantly promoted xCT-mediated ferroptosis induced by RSL3 or sorafenib on stiff substrate via FTL, whereas its overexpression abolished these upward trends. Notably, PD-L2 deletion in combination with sorafenib and anti-PD-1 antibody significantly sensitized HCC cells and blunted cancer growth in vivo. Additionally, we found the ferroptosis- and immune checkpoint-related prognostic genes that combined PD-L2, SLC7A11 and SYMD3 well predict the clinical efficacy of sorafenib in patients with HCC. Conclusion: These findings expand our understanding of the mechanics-dependent PD-L2 role in ferroptosis, cancer progression and resistance, providing a basis for the clinical translation of PD-L2 as a therapeutic target or diagnostic biomarker.http://www.sciencedirect.com/science/article/pii/S2090123224003631Matrix stiffnessPD-L2FerroptosisSorafenib resistanceImmunotherapyHepatocellular carcinoma
spellingShingle Shunxi Wang
Xiaoxue Yuan
Zetao Yang
Xuan Zhang
Zhiling Xu
Li Yang
Xian Yang
Wei Zhou
Wanqian Liu
Matrix stiffness-dependent PD-L2 deficiency improves SMYD3/xCT-mediated ferroptosis and the efficacy of anti-PD-1 in HCC
Journal of Advanced Research
Matrix stiffness
PD-L2
Ferroptosis
Sorafenib resistance
Immunotherapy
Hepatocellular carcinoma
title Matrix stiffness-dependent PD-L2 deficiency improves SMYD3/xCT-mediated ferroptosis and the efficacy of anti-PD-1 in HCC
title_full Matrix stiffness-dependent PD-L2 deficiency improves SMYD3/xCT-mediated ferroptosis and the efficacy of anti-PD-1 in HCC
title_fullStr Matrix stiffness-dependent PD-L2 deficiency improves SMYD3/xCT-mediated ferroptosis and the efficacy of anti-PD-1 in HCC
title_full_unstemmed Matrix stiffness-dependent PD-L2 deficiency improves SMYD3/xCT-mediated ferroptosis and the efficacy of anti-PD-1 in HCC
title_short Matrix stiffness-dependent PD-L2 deficiency improves SMYD3/xCT-mediated ferroptosis and the efficacy of anti-PD-1 in HCC
title_sort matrix stiffness dependent pd l2 deficiency improves smyd3 xct mediated ferroptosis and the efficacy of anti pd 1 in hcc
topic Matrix stiffness
PD-L2
Ferroptosis
Sorafenib resistance
Immunotherapy
Hepatocellular carcinoma
url http://www.sciencedirect.com/science/article/pii/S2090123224003631
work_keys_str_mv AT shunxiwang matrixstiffnessdependentpdl2deficiencyimprovessmyd3xctmediatedferroptosisandtheefficacyofantipd1inhcc
AT xiaoxueyuan matrixstiffnessdependentpdl2deficiencyimprovessmyd3xctmediatedferroptosisandtheefficacyofantipd1inhcc
AT zetaoyang matrixstiffnessdependentpdl2deficiencyimprovessmyd3xctmediatedferroptosisandtheefficacyofantipd1inhcc
AT xuanzhang matrixstiffnessdependentpdl2deficiencyimprovessmyd3xctmediatedferroptosisandtheefficacyofantipd1inhcc
AT zhilingxu matrixstiffnessdependentpdl2deficiencyimprovessmyd3xctmediatedferroptosisandtheefficacyofantipd1inhcc
AT liyang matrixstiffnessdependentpdl2deficiencyimprovessmyd3xctmediatedferroptosisandtheefficacyofantipd1inhcc
AT xianyang matrixstiffnessdependentpdl2deficiencyimprovessmyd3xctmediatedferroptosisandtheefficacyofantipd1inhcc
AT weizhou matrixstiffnessdependentpdl2deficiencyimprovessmyd3xctmediatedferroptosisandtheefficacyofantipd1inhcc
AT wanqianliu matrixstiffnessdependentpdl2deficiencyimprovessmyd3xctmediatedferroptosisandtheefficacyofantipd1inhcc