Systematic Study of Reaction Conditions for Size-Controlled Synthesis of Silica Nanoparticles

This study presents a reproducible and scalable method for synthesizing silica nanoparticles (SNPs) with controlled sizes below 200 nm, achieved by systematically varying three key reaction parameters: ammonium hydroxide concentration, water concentration, and temperature. SNPs with high monodispers...

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Bibliographic Details
Main Authors: Barbara Vörös-Horváth, Ala’ Salem, Barna Kovács, Aleksandar Széchenyi, Szilárd Pál
Format: Article
Language:English
Published: MDPI AG 2024-09-01
Series:Nanomaterials
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Online Access:https://www.mdpi.com/2079-4991/14/19/1561
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Summary:This study presents a reproducible and scalable method for synthesizing silica nanoparticles (SNPs) with controlled sizes below 200 nm, achieved by systematically varying three key reaction parameters: ammonium hydroxide concentration, water concentration, and temperature. SNPs with high monodispersity and controlled dimensions were produced by optimizing these factors. The results indicated a direct correlation between ammonium hydroxide concentration and particle size, while higher temperatures resulted in smaller particles with increased polydispersity. Water concentration also influenced particle size, with a quadratic relationship observed. This method provides a robust approach for tailoring SNP sizes, with significant implications for biomedical applications, particularly in drug delivery and diagnostics. Using eco-friendly solvents such as ethanol further enhances the sustainability and cost-effectiveness of the process.
ISSN:2079-4991