Photoredox-Catalyzed Radical Cyclization of Unactivated Alkene-Substituted β‑Ketoesters Enabled Asymmetric Total Synthesis of Tricyclic Prostaglandin D2 Metabolite Methyl Ester

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Main Authors: Miao Xiao, Qiaoli Shang, Liuyang Pu, Zheyuan Wang, Lei Zhu, Zhen Yang, Jun Huang
Format: Article
Language:English
Published: American Chemical Society 2025-03-01
Series:JACS Au
Online Access:https://doi.org/10.1021/jacsau.4c01268
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author Miao Xiao
Qiaoli Shang
Liuyang Pu
Zheyuan Wang
Lei Zhu
Zhen Yang
Jun Huang
author_facet Miao Xiao
Qiaoli Shang
Liuyang Pu
Zheyuan Wang
Lei Zhu
Zhen Yang
Jun Huang
author_sort Miao Xiao
collection DOAJ
format Article
id doaj-art-dfbaef36dff048cd97ebb8e76d5ab3ba
institution Kabale University
issn 2691-3704
language English
publishDate 2025-03-01
publisher American Chemical Society
record_format Article
series JACS Au
spelling doaj-art-dfbaef36dff048cd97ebb8e76d5ab3ba2025-08-20T03:40:00ZengAmerican Chemical SocietyJACS Au2691-37042025-03-01531367137510.1021/jacsau.4c01268Photoredox-Catalyzed Radical Cyclization of Unactivated Alkene-Substituted β‑Ketoesters Enabled Asymmetric Total Synthesis of Tricyclic Prostaglandin D2 Metabolite Methyl EsterMiao Xiao0Qiaoli Shang1Liuyang Pu2Zheyuan Wang3Lei Zhu4Zhen Yang5Jun Huang6School of Chemistry and Chemical Engineering, University of South China, Hengyang, ChinaSchool of Chemistry and Chemical Engineering, University of South China, Hengyang, ChinaSchool of Chemistry and Chemical Engineering, University of South China, Hengyang, ChinaState Key Laboratory of Chemical Oncogenomics and Key Laboratory of Chemical Genomics, Peking University Shenzhen Graduate School, Shenzhen, ChinaCollege of Pharmacy, Third Military Medical University, Chongqing, ChinaState Key Laboratory of Chemical Oncogenomics and Key Laboratory of Chemical Genomics, Peking University Shenzhen Graduate School, Shenzhen, ChinaSchool of Chemistry and Chemical Engineering, University of South China, Hengyang, Chinahttps://doi.org/10.1021/jacsau.4c01268
spellingShingle Miao Xiao
Qiaoli Shang
Liuyang Pu
Zheyuan Wang
Lei Zhu
Zhen Yang
Jun Huang
Photoredox-Catalyzed Radical Cyclization of Unactivated Alkene-Substituted β‑Ketoesters Enabled Asymmetric Total Synthesis of Tricyclic Prostaglandin D2 Metabolite Methyl Ester
JACS Au
title Photoredox-Catalyzed Radical Cyclization of Unactivated Alkene-Substituted β‑Ketoesters Enabled Asymmetric Total Synthesis of Tricyclic Prostaglandin D2 Metabolite Methyl Ester
title_full Photoredox-Catalyzed Radical Cyclization of Unactivated Alkene-Substituted β‑Ketoesters Enabled Asymmetric Total Synthesis of Tricyclic Prostaglandin D2 Metabolite Methyl Ester
title_fullStr Photoredox-Catalyzed Radical Cyclization of Unactivated Alkene-Substituted β‑Ketoesters Enabled Asymmetric Total Synthesis of Tricyclic Prostaglandin D2 Metabolite Methyl Ester
title_full_unstemmed Photoredox-Catalyzed Radical Cyclization of Unactivated Alkene-Substituted β‑Ketoesters Enabled Asymmetric Total Synthesis of Tricyclic Prostaglandin D2 Metabolite Methyl Ester
title_short Photoredox-Catalyzed Radical Cyclization of Unactivated Alkene-Substituted β‑Ketoesters Enabled Asymmetric Total Synthesis of Tricyclic Prostaglandin D2 Metabolite Methyl Ester
title_sort photoredox catalyzed radical cyclization of unactivated alkene substituted β ketoesters enabled asymmetric total synthesis of tricyclic prostaglandin d2 metabolite methyl ester
url https://doi.org/10.1021/jacsau.4c01268
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AT zhenyang photoredoxcatalyzedradicalcyclizationofunactivatedalkenesubstitutedbketoestersenabledasymmetrictotalsynthesisoftricyclicprostaglandind2metabolitemethylester
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