Thermal behavior of ground talc mineral

Microstructure development and thermal behavior of ground talc mineral samples (from locality Puebla de Lillo, Spain) was characterized by X-ray diffraction, scanning electron microscopy(SEM),surface area measurements differential thermal analysis, thermogravimetry and emanation thermal analysis (ET...

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Main Authors: Balek V., Šubrt J., Pérez-Maqueda L.A., Beneš M., Bountseva I.M., Beckman I.N., Pérez-Rodríguez J.L.
Format: Article
Language:English
Published: University of Belgrade, Technical Faculty, Bor 2008-01-01
Series:Journal of Mining and Metallurgy. Section B: Metallurgy
Subjects:
Online Access:http://www.doiserbia.nb.rs/img/doi/1450-5339/2008/1450-53390801007B.pdf
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author Balek V.
Šubrt J.
Pérez-Maqueda L.A.
Beneš M.
Bountseva I.M.
Beckman I.N.
Pérez-Rodríguez J.L.
author_facet Balek V.
Šubrt J.
Pérez-Maqueda L.A.
Beneš M.
Bountseva I.M.
Beckman I.N.
Pérez-Rodríguez J.L.
author_sort Balek V.
collection DOAJ
description Microstructure development and thermal behavior of ground talc mineral samples (from locality Puebla de Lillo, Spain) was characterized by X-ray diffraction, scanning electron microscopy(SEM),surface area measurements differential thermal analysis, thermogravimetry and emanation thermal analysis (ETA).A vibratory mill and grinding time 5 min. was used to prepare the ground talc sample. It was found that grinding caused an increase in the surface area of the natural talc from 3 m2g-1 to 110 m2g-1. A decrease of particle size after sample grinding was observed by SEM. The increase of structure disorder of the ground sample and the crystallite size reduction from 40 to 10 nm were determined from the XRD results. ETA results revealed a closing up of surface micro-cracks and healing of microstructure irregularities on heating in the range 200-500ºC of both un-ground and ground talc samples. For the ground talc sample a crystallization of non-crystalline phase into orthorhombic enstatite was characterized as by a decrease of radon mobility in the range 785-825ºC and by a DTA exothermal effect with the maximum at 830ºC. ETA results were used for the assessment of transport properties of the talc samples on heating.
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series Journal of Mining and Metallurgy. Section B: Metallurgy
spelling doaj-art-dd2387e7a4aa4a7185906752d1e022db2025-02-02T05:40:50ZengUniversity of Belgrade, Technical Faculty, BorJournal of Mining and Metallurgy. Section B: Metallurgy1450-53392008-01-0144171710.2298/JMMB0801007BThermal behavior of ground talc mineralBalek V.Šubrt J.Pérez-Maqueda L.A.Beneš M.Bountseva I.M.Beckman I.N.Pérez-Rodríguez J.L.Microstructure development and thermal behavior of ground talc mineral samples (from locality Puebla de Lillo, Spain) was characterized by X-ray diffraction, scanning electron microscopy(SEM),surface area measurements differential thermal analysis, thermogravimetry and emanation thermal analysis (ETA).A vibratory mill and grinding time 5 min. was used to prepare the ground talc sample. It was found that grinding caused an increase in the surface area of the natural talc from 3 m2g-1 to 110 m2g-1. A decrease of particle size after sample grinding was observed by SEM. The increase of structure disorder of the ground sample and the crystallite size reduction from 40 to 10 nm were determined from the XRD results. ETA results revealed a closing up of surface micro-cracks and healing of microstructure irregularities on heating in the range 200-500ºC of both un-ground and ground talc samples. For the ground talc sample a crystallization of non-crystalline phase into orthorhombic enstatite was characterized as by a decrease of radon mobility in the range 785-825ºC and by a DTA exothermal effect with the maximum at 830ºC. ETA results were used for the assessment of transport properties of the talc samples on heating.http://www.doiserbia.nb.rs/img/doi/1450-5339/2008/1450-53390801007B.pdftalcgrindingmicrostructurethermal behaviorradon mobility
spellingShingle Balek V.
Šubrt J.
Pérez-Maqueda L.A.
Beneš M.
Bountseva I.M.
Beckman I.N.
Pérez-Rodríguez J.L.
Thermal behavior of ground talc mineral
Journal of Mining and Metallurgy. Section B: Metallurgy
talc
grinding
microstructure
thermal behavior
radon mobility
title Thermal behavior of ground talc mineral
title_full Thermal behavior of ground talc mineral
title_fullStr Thermal behavior of ground talc mineral
title_full_unstemmed Thermal behavior of ground talc mineral
title_short Thermal behavior of ground talc mineral
title_sort thermal behavior of ground talc mineral
topic talc
grinding
microstructure
thermal behavior
radon mobility
url http://www.doiserbia.nb.rs/img/doi/1450-5339/2008/1450-53390801007B.pdf
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AT benesm thermalbehaviorofgroundtalcmineral
AT bountsevaim thermalbehaviorofgroundtalcmineral
AT beckmanin thermalbehaviorofgroundtalcmineral
AT perezrodriguezjl thermalbehaviorofgroundtalcmineral