Ultrasonic Assisted Environmentally Friendly Extraction of Natural Dyes From Beta vulgaris for the Coloration of Silk Fabric Using Different Mordants
ABSTRACT Considering the indispensability of environmental protection, the utilization of natural ingredients as sustainable and eco‐friendly alternatives to synthetic dyes in fabric dyeing is of great significance. Betacyanins are naturally sourced pigments of red‐violet color that have the propens...
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2025-01-01
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| Online Access: | https://doi.org/10.1002/ese3.2001 |
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| author | Rony Mia Tafsir Uddin A. Z. M. Mofasser Nadim Ibn Sayed Al Mojnun Shamim Sanjida Islam Khandaker Akil Mahadi Ohi Moonis Ali Khan Burhan Uddin Banna |
| author_facet | Rony Mia Tafsir Uddin A. Z. M. Mofasser Nadim Ibn Sayed Al Mojnun Shamim Sanjida Islam Khandaker Akil Mahadi Ohi Moonis Ali Khan Burhan Uddin Banna |
| author_sort | Rony Mia |
| collection | DOAJ |
| description | ABSTRACT Considering the indispensability of environmental protection, the utilization of natural ingredients as sustainable and eco‐friendly alternatives to synthetic dyes in fabric dyeing is of great significance. Betacyanins are naturally sourced pigments of red‐violet color that have the propensity to be fixed to mordanted substrates with reasonable permanency. In this study, the betacyanins sourced from beetroot (Beta vulgaris) were used to dye pre‐mordanted silk fabrics employing ultrasonication. In addition, a comparative analysis of the effects of five different mordants such as orange‐peel extracts, lemon peel extracts, tannic acid, ferrous sulfate, and alum on the color strength and fastness of beetroot‐dyed silk fabrics was presented in this research. For the characterization of the extracted dye, undyed, dyed, and mordanted silk fabric, infrared spectroscopy was performed. To observe the interaction of extracted dye and silk fabric, scanning electron microscopy was also accomplished. The outcomes of the characterization validated the successful extraction of dyes from beetroot and dyeing silk fabric with it. The values of color intensity (K/S), CIE L* a* b*, and CIE L* c* h* were measured using a reflectance spectrophotometer. At the same time, dry and wet rubbing and lightfastness ratings of dyed silk fabrics were determined according to the ISO standards. When 5% (o.w.f.) ferrous sulfate was used in pre‐mordanting, the ratings of colorfastness to wash, rub, and light ranged from 4 to 4/5, and the K/S value of the final sample was 4.88, which is higher than the K/S values of any other dyed samples. In contrast, the performance of 5% (o.w.f.) lemon peel extracts as a mordant was remarkably higher than orange peel extracts and even better than alum and tannic acid to some extent. The beetroot‐dyed silk fabric pre‐mordanted with 5% lemon peel exhibited a K/S value of 4.32, and the overall colorfastness rating ranged from 3/4 to 4/5. In conclusion, beetroot extracts hold the promise of being utilized as a sustainable replacement for environmentally harmful synthetic dyestuff in silk dyeing. Furthermore, in silk dyeing with beetroot extract, lemon peel extract is a potent alternative to ferrous sulfate as a mordant. |
| format | Article |
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| institution | Kabale University |
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| spelling | doaj-art-da674a029dcf4ec583bcb7d39f2cdf472025-01-21T11:38:24ZengWileyEnergy Science & Engineering2050-05052025-01-0113132333410.1002/ese3.2001Ultrasonic Assisted Environmentally Friendly Extraction of Natural Dyes From Beta vulgaris for the Coloration of Silk Fabric Using Different MordantsRony Mia0Tafsir Uddin1A. Z. M. Mofasser2Nadim Ibn Sayed3Al Mojnun Shamim4Sanjida Islam5Khandaker Akil Mahadi Ohi6Moonis Ali Khan7Burhan Uddin Banna8Department of Medical Biotechnology, Center for Global Health Research Saveetha Medical College and Hospital, Saveetha Institute of Medical and Technical Sciences (SIMATS) Chennai IndiaDepartment of Textile Engineering, National Institute of Textile Engineering and Research University of Dhaka Dhaka BangladeshDepartment of Textile Engineering European University of Bangladesh Dhaka BangladeshDepartment of Textile Engineering European University of Bangladesh Dhaka BangladeshDepartment of Information Technology (Data Management and Analytics) Washington University of Science and Technology (WUST) Alexandria Virginia USADepartment of Textile Engineering, National Institute of Textile Engineering and Research University of Dhaka Dhaka BangladeshDepartment of Textile Engineering, National Institute of Textile Engineering and Research University of Dhaka Dhaka BangladeshDepartment of Chemistry, College of Science King Saud University Riyadh Saudi ArabiaDepartment of Textile Engineering, National Institute of Textile Engineering and Research University of Dhaka Dhaka BangladeshABSTRACT Considering the indispensability of environmental protection, the utilization of natural ingredients as sustainable and eco‐friendly alternatives to synthetic dyes in fabric dyeing is of great significance. Betacyanins are naturally sourced pigments of red‐violet color that have the propensity to be fixed to mordanted substrates with reasonable permanency. In this study, the betacyanins sourced from beetroot (Beta vulgaris) were used to dye pre‐mordanted silk fabrics employing ultrasonication. In addition, a comparative analysis of the effects of five different mordants such as orange‐peel extracts, lemon peel extracts, tannic acid, ferrous sulfate, and alum on the color strength and fastness of beetroot‐dyed silk fabrics was presented in this research. For the characterization of the extracted dye, undyed, dyed, and mordanted silk fabric, infrared spectroscopy was performed. To observe the interaction of extracted dye and silk fabric, scanning electron microscopy was also accomplished. The outcomes of the characterization validated the successful extraction of dyes from beetroot and dyeing silk fabric with it. The values of color intensity (K/S), CIE L* a* b*, and CIE L* c* h* were measured using a reflectance spectrophotometer. At the same time, dry and wet rubbing and lightfastness ratings of dyed silk fabrics were determined according to the ISO standards. When 5% (o.w.f.) ferrous sulfate was used in pre‐mordanting, the ratings of colorfastness to wash, rub, and light ranged from 4 to 4/5, and the K/S value of the final sample was 4.88, which is higher than the K/S values of any other dyed samples. In contrast, the performance of 5% (o.w.f.) lemon peel extracts as a mordant was remarkably higher than orange peel extracts and even better than alum and tannic acid to some extent. The beetroot‐dyed silk fabric pre‐mordanted with 5% lemon peel exhibited a K/S value of 4.32, and the overall colorfastness rating ranged from 3/4 to 4/5. In conclusion, beetroot extracts hold the promise of being utilized as a sustainable replacement for environmentally harmful synthetic dyestuff in silk dyeing. Furthermore, in silk dyeing with beetroot extract, lemon peel extract is a potent alternative to ferrous sulfate as a mordant.https://doi.org/10.1002/ese3.2001beetrootbio‐mordantingsilk fabricsustainabilityultrasonication |
| spellingShingle | Rony Mia Tafsir Uddin A. Z. M. Mofasser Nadim Ibn Sayed Al Mojnun Shamim Sanjida Islam Khandaker Akil Mahadi Ohi Moonis Ali Khan Burhan Uddin Banna Ultrasonic Assisted Environmentally Friendly Extraction of Natural Dyes From Beta vulgaris for the Coloration of Silk Fabric Using Different Mordants Energy Science & Engineering beetroot bio‐mordanting silk fabric sustainability ultrasonication |
| title | Ultrasonic Assisted Environmentally Friendly Extraction of Natural Dyes From Beta vulgaris for the Coloration of Silk Fabric Using Different Mordants |
| title_full | Ultrasonic Assisted Environmentally Friendly Extraction of Natural Dyes From Beta vulgaris for the Coloration of Silk Fabric Using Different Mordants |
| title_fullStr | Ultrasonic Assisted Environmentally Friendly Extraction of Natural Dyes From Beta vulgaris for the Coloration of Silk Fabric Using Different Mordants |
| title_full_unstemmed | Ultrasonic Assisted Environmentally Friendly Extraction of Natural Dyes From Beta vulgaris for the Coloration of Silk Fabric Using Different Mordants |
| title_short | Ultrasonic Assisted Environmentally Friendly Extraction of Natural Dyes From Beta vulgaris for the Coloration of Silk Fabric Using Different Mordants |
| title_sort | ultrasonic assisted environmentally friendly extraction of natural dyes from beta vulgaris for the coloration of silk fabric using different mordants |
| topic | beetroot bio‐mordanting silk fabric sustainability ultrasonication |
| url | https://doi.org/10.1002/ese3.2001 |
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