XPS, FTIR, EDX, and XRD Analysis of Al2O3 Scales Grown on PM2000 Alloy
This work is an original example to compare the results obtained after calcination of Al2O3 hydroxides and oxidation of alumino-formers alloys. FTIR and XPS signatures were obtained for various oxidation temperatures and compared with those known from the literature about calcination of Al2O3 precu...
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| Format: | Article |
| Language: | English |
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Wiley
2015-01-01
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| Series: | Journal of Spectroscopy |
| Online Access: | http://dx.doi.org/10.1155/2015/868109 |
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| author | K. Djebaili Z. Mekhalif A. Boumaza A. Djelloul |
| author_facet | K. Djebaili Z. Mekhalif A. Boumaza A. Djelloul |
| author_sort | K. Djebaili |
| collection | DOAJ |
| description | This work is an original example to compare the results obtained after calcination of Al2O3 hydroxides and oxidation of alumino-formers alloys. FTIR and XPS signatures were obtained for various oxidation temperatures and compared with those known from the literature about calcination of Al2O3 precursors. The aim of this work is to evaluate the use of IR spectroscopy and XPS analysis to probe the structural varieties of Al2O3. For this objective, a study of the PM2000 oxidation at various temperatures was conducted by means of XRD, IR spectroscopy, XPS analysis, EDX analysis, and SEM observations. This allowed us to clearly differentiate the transition Al2O3 from the α-Al2O3 and, amongst the transition Al2O3, to differentiate the characteristic of the IR spectrum of γ-δ phases from that of the θ phase. |
| format | Article |
| id | doaj-art-d493e01a454f419a8d971c9c2da7977a |
| institution | Kabale University |
| issn | 2314-4920 2314-4939 |
| language | English |
| publishDate | 2015-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | Journal of Spectroscopy |
| spelling | doaj-art-d493e01a454f419a8d971c9c2da7977a2025-02-03T01:28:02ZengWileyJournal of Spectroscopy2314-49202314-49392015-01-01201510.1155/2015/868109868109XPS, FTIR, EDX, and XRD Analysis of Al2O3 Scales Grown on PM2000 AlloyK. Djebaili0Z. Mekhalif1A. Boumaza2A. Djelloul3Structures, Properties and InterAtomic Interactions Laboratory (LASPI2A), Faculty of Science and Technology, University of Abbès Laghrour, 40000 Khenchela, AlgeriaChemistry and Electrochemistry Surfaces Laboratory (LCES), Notre-Dame de la Paix Faculty, Road of Bruxelles 61, 5000 Namur, BelgiumStructures, Properties and InterAtomic Interactions Laboratory (LASPI2A), Faculty of Science and Technology, University of Abbès Laghrour, 40000 Khenchela, AlgeriaStructures, Properties and InterAtomic Interactions Laboratory (LASPI2A), Faculty of Science and Technology, University of Abbès Laghrour, 40000 Khenchela, AlgeriaThis work is an original example to compare the results obtained after calcination of Al2O3 hydroxides and oxidation of alumino-formers alloys. FTIR and XPS signatures were obtained for various oxidation temperatures and compared with those known from the literature about calcination of Al2O3 precursors. The aim of this work is to evaluate the use of IR spectroscopy and XPS analysis to probe the structural varieties of Al2O3. For this objective, a study of the PM2000 oxidation at various temperatures was conducted by means of XRD, IR spectroscopy, XPS analysis, EDX analysis, and SEM observations. This allowed us to clearly differentiate the transition Al2O3 from the α-Al2O3 and, amongst the transition Al2O3, to differentiate the characteristic of the IR spectrum of γ-δ phases from that of the θ phase.http://dx.doi.org/10.1155/2015/868109 |
| spellingShingle | K. Djebaili Z. Mekhalif A. Boumaza A. Djelloul XPS, FTIR, EDX, and XRD Analysis of Al2O3 Scales Grown on PM2000 Alloy Journal of Spectroscopy |
| title | XPS, FTIR, EDX, and XRD Analysis of Al2O3 Scales Grown on PM2000 Alloy |
| title_full | XPS, FTIR, EDX, and XRD Analysis of Al2O3 Scales Grown on PM2000 Alloy |
| title_fullStr | XPS, FTIR, EDX, and XRD Analysis of Al2O3 Scales Grown on PM2000 Alloy |
| title_full_unstemmed | XPS, FTIR, EDX, and XRD Analysis of Al2O3 Scales Grown on PM2000 Alloy |
| title_short | XPS, FTIR, EDX, and XRD Analysis of Al2O3 Scales Grown on PM2000 Alloy |
| title_sort | xps ftir edx and xrd analysis of al2o3 scales grown on pm2000 alloy |
| url | http://dx.doi.org/10.1155/2015/868109 |
| work_keys_str_mv | AT kdjebaili xpsftiredxandxrdanalysisofal2o3scalesgrownonpm2000alloy AT zmekhalif xpsftiredxandxrdanalysisofal2o3scalesgrownonpm2000alloy AT aboumaza xpsftiredxandxrdanalysisofal2o3scalesgrownonpm2000alloy AT adjelloul xpsftiredxandxrdanalysisofal2o3scalesgrownonpm2000alloy |