Synthesis and Characterization of Tetrakis(4-oxo-piperidinium ethylene acetal) Bis Sulfate Hexahydrate
Chemical preparation, x-ray characterization, IR spectroscopy and thermal analysis of a new sulfate (C7H12O2NH2)4(SO4)2.6H2O, are reported. The atomic arrangement can be described by layers formed by sulfate anions (SO -24) and water molecules connected by hydrogen bonds O-H…O. These inorganic layer...
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| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
| Published: |
Wiley
2011-01-01
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| Series: | E-Journal of Chemistry |
| Online Access: | http://dx.doi.org/10.1155/2011/572080 |
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| Summary: | Chemical preparation, x-ray characterization, IR spectroscopy and thermal analysis of a new sulfate (C7H12O2NH2)4(SO4)2.6H2O, are reported. The atomic arrangement can be described by layers formed by sulfate anions (SO -24) and water molecules connected by hydrogen bonds O-H…O. These inorganic layers are developed around ab planes at z = 0 and z = 1/2 and are interconnected by the H-bonds created by organic groups. All the hydrogen bonds, the Van der waals contacts and electrostatic interactions between the different entities give rise to a three-dimensional network in the structure and add stability to this compound. The thermal behaviour and the IR spectroscopic studies of this new sulfate are discussed. |
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| ISSN: | 0973-4945 2090-9810 |