Photosensitized degradation of dinitrosalicylic acid by uranyl ions

The photodegradation of dinitrosalicylic acid (DNS) by photoexcited uranyl ion was studied in aqueous solutions. The failure of DNS to degrade directly with light highlights the importance of the photoexcited uranyl ion in controlling the photochemical processes. Fluorescence quenching studies showe...

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Main Authors: A. A. I. Essawy, M. S. A. Abdel-Mottaleb
Format: Article
Language:English
Published: Wiley 2003-01-01
Series:International Journal of Photoenergy
Online Access:http://dx.doi.org/10.1155/S1110662X03000357
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author A. A. I. Essawy
M. S. A. Abdel-Mottaleb
author_facet A. A. I. Essawy
M. S. A. Abdel-Mottaleb
author_sort A. A. I. Essawy
collection DOAJ
description The photodegradation of dinitrosalicylic acid (DNS) by photoexcited uranyl ion was studied in aqueous solutions. The failure of DNS to degrade directly with light highlights the importance of the photoexcited uranyl ion in controlling the photochemical processes. Fluorescence quenching studies showed that an electron-transfer process from the DNS to the excited uranyl ion is involved leading to the formation of UO2+/DNS•+ radical pair complex as an initial step. Illumination of the UO22+/DNS solution in presence of oxygen results in mineralization of DNS. The results are explained on the basis of a catalytic cycle involving UO22+ ion and molecular oxygen that generates reactive superoxide O2•− anion and its conjugate acid HO2•. The efficiency of the photocatalytic cycle is enhanced markedly by addition of dilute NaOH solution.
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spelling doaj-art-d24c7c9ef30b46a6bf3313af51b6e1f32025-08-20T02:19:43ZengWileyInternational Journal of Photoenergy1110-662X2003-01-015421922110.1155/S1110662X03000357Photosensitized degradation of dinitrosalicylic acid by uranyl ionsA. A. I. Essawy0M. S. A. Abdel-Mottaleb1Dept. Chem., Faculty of Science, Cairo University, Fayoum Branch, EgyptPhotoenergy Center, Faculty of Science, Ain Shams University, Abbassia, Cairo, EgyptThe photodegradation of dinitrosalicylic acid (DNS) by photoexcited uranyl ion was studied in aqueous solutions. The failure of DNS to degrade directly with light highlights the importance of the photoexcited uranyl ion in controlling the photochemical processes. Fluorescence quenching studies showed that an electron-transfer process from the DNS to the excited uranyl ion is involved leading to the formation of UO2+/DNS•+ radical pair complex as an initial step. Illumination of the UO22+/DNS solution in presence of oxygen results in mineralization of DNS. The results are explained on the basis of a catalytic cycle involving UO22+ ion and molecular oxygen that generates reactive superoxide O2•− anion and its conjugate acid HO2•. The efficiency of the photocatalytic cycle is enhanced markedly by addition of dilute NaOH solution.http://dx.doi.org/10.1155/S1110662X03000357
spellingShingle A. A. I. Essawy
M. S. A. Abdel-Mottaleb
Photosensitized degradation of dinitrosalicylic acid by uranyl ions
International Journal of Photoenergy
title Photosensitized degradation of dinitrosalicylic acid by uranyl ions
title_full Photosensitized degradation of dinitrosalicylic acid by uranyl ions
title_fullStr Photosensitized degradation of dinitrosalicylic acid by uranyl ions
title_full_unstemmed Photosensitized degradation of dinitrosalicylic acid by uranyl ions
title_short Photosensitized degradation of dinitrosalicylic acid by uranyl ions
title_sort photosensitized degradation of dinitrosalicylic acid by uranyl ions
url http://dx.doi.org/10.1155/S1110662X03000357
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