Mechanical properties and fracture mechanism of high-strength FGH4097 superalloys prepared by hot oscillatory pressing

A powder metallurgy (PM) nickel-based superalloy of FGH4097 with Φ160mm × 90 mm was prepared by hot oscillatory pressing (HOP) method and heat treatment process. The mechanical properties and fracture mechanism of FGH4097 superalloys at room temperature and 650 °C were studied. The density was 8.36 ...

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Main Authors: Pengfei Li, Hong Huang, Wenzhuo Du, Yan Fan, ruiming Yin, shangdong Hou, Liwen Sheng
Format: Article
Language:English
Published: Elsevier 2025-03-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785425001966
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author Pengfei Li
Hong Huang
Wenzhuo Du
Yan Fan
ruiming Yin
shangdong Hou
Liwen Sheng
author_facet Pengfei Li
Hong Huang
Wenzhuo Du
Yan Fan
ruiming Yin
shangdong Hou
Liwen Sheng
author_sort Pengfei Li
collection DOAJ
description A powder metallurgy (PM) nickel-based superalloy of FGH4097 with Φ160mm × 90 mm was prepared by hot oscillatory pressing (HOP) method and heat treatment process. The mechanical properties and fracture mechanism of FGH4097 superalloys at room temperature and 650 °C were studied. The density was 8.36 g/cm3, and the highest tensile strength and elongation at room temperature reached 1483 MPa and 26%, respectively. At 650 °C, the highest tensile strength and elongation reached 1331 MPa and 28%, respectively. At 650 °C, after 24000 cycles of high cycle fatigue and 100 h of endurance strength, it did not break. The mechanical properties of FGH4097 superalloys prepared by hot oscillating pressing sintering are comparable to those of “plasma rotating electrode processing (PREP) and hot isostatic pressing (HIP)” technology. The fracture surface of FGH4097 superalloys at room temperature and 650 °C exhibits distinct morphological features of fiber zone, radiation zone, and shear lip zone. The average grain size was 48.92 μm, and approximately 320 nm of γ′ phase and (Nb, Ti) C phase were precipitated. The prior particle boundaries (PPBs) effect of primary γ′ phase and carbide phase at the grain boundaries is suppressed. The combined effect of grain boundary strengthening, solid solution strengthening, precipitation strengthening, and stacking fault strengthening enhances the yield strength and ductility. This work not only reduce the production cost and short the manufacturing cycle of powder superalloys, but also promote the application of powder superalloys in high temperature field.
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spelling doaj-art-ca3a58439ac94558a3c487d5773bc5f72025-02-06T05:11:54ZengElsevierJournal of Materials Research and Technology2238-78542025-03-013530083020Mechanical properties and fracture mechanism of high-strength FGH4097 superalloys prepared by hot oscillatory pressingPengfei Li0Hong Huang1Wenzhuo Du2Yan Fan3ruiming Yin4shangdong Hou5Liwen Sheng6National & Local Joint Engineering Research Center for Advanced Packaging Material and Technology, College of Materials and Advanced Manufacturing, Hunan University of Technology, Zhuzhou, 412007, China; Corresponding author.National & Local Joint Engineering Research Center for Advanced Packaging Material and Technology, College of Materials and Advanced Manufacturing, Hunan University of Technology, Zhuzhou, 412007, ChinaNational & Local Joint Engineering Research Center for Advanced Packaging Material and Technology, College of Materials and Advanced Manufacturing, Hunan University of Technology, Zhuzhou, 412007, ChinaAECC Hunan Aviation Powerplant Research Institute, Zhuzhou, 412002, China; Corresponding author.National & Local Joint Engineering Research Center for Advanced Packaging Material and Technology, College of Materials and Advanced Manufacturing, Hunan University of Technology, Zhuzhou, 412007, ChinaZhuzhou Wanrong New Materials Technology Co., Ltd., Zhuzhou, 412007, ChinaZhuzhou Wanrong New Materials Technology Co., Ltd., Zhuzhou, 412007, ChinaA powder metallurgy (PM) nickel-based superalloy of FGH4097 with Φ160mm × 90 mm was prepared by hot oscillatory pressing (HOP) method and heat treatment process. The mechanical properties and fracture mechanism of FGH4097 superalloys at room temperature and 650 °C were studied. The density was 8.36 g/cm3, and the highest tensile strength and elongation at room temperature reached 1483 MPa and 26%, respectively. At 650 °C, the highest tensile strength and elongation reached 1331 MPa and 28%, respectively. At 650 °C, after 24000 cycles of high cycle fatigue and 100 h of endurance strength, it did not break. The mechanical properties of FGH4097 superalloys prepared by hot oscillating pressing sintering are comparable to those of “plasma rotating electrode processing (PREP) and hot isostatic pressing (HIP)” technology. The fracture surface of FGH4097 superalloys at room temperature and 650 °C exhibits distinct morphological features of fiber zone, radiation zone, and shear lip zone. The average grain size was 48.92 μm, and approximately 320 nm of γ′ phase and (Nb, Ti) C phase were precipitated. The prior particle boundaries (PPBs) effect of primary γ′ phase and carbide phase at the grain boundaries is suppressed. The combined effect of grain boundary strengthening, solid solution strengthening, precipitation strengthening, and stacking fault strengthening enhances the yield strength and ductility. This work not only reduce the production cost and short the manufacturing cycle of powder superalloys, but also promote the application of powder superalloys in high temperature field.http://www.sciencedirect.com/science/article/pii/S2238785425001966Hot oscillatory pressingFracture mechanismTensile strengthFGH4097 superalloys
spellingShingle Pengfei Li
Hong Huang
Wenzhuo Du
Yan Fan
ruiming Yin
shangdong Hou
Liwen Sheng
Mechanical properties and fracture mechanism of high-strength FGH4097 superalloys prepared by hot oscillatory pressing
Journal of Materials Research and Technology
Hot oscillatory pressing
Fracture mechanism
Tensile strength
FGH4097 superalloys
title Mechanical properties and fracture mechanism of high-strength FGH4097 superalloys prepared by hot oscillatory pressing
title_full Mechanical properties and fracture mechanism of high-strength FGH4097 superalloys prepared by hot oscillatory pressing
title_fullStr Mechanical properties and fracture mechanism of high-strength FGH4097 superalloys prepared by hot oscillatory pressing
title_full_unstemmed Mechanical properties and fracture mechanism of high-strength FGH4097 superalloys prepared by hot oscillatory pressing
title_short Mechanical properties and fracture mechanism of high-strength FGH4097 superalloys prepared by hot oscillatory pressing
title_sort mechanical properties and fracture mechanism of high strength fgh4097 superalloys prepared by hot oscillatory pressing
topic Hot oscillatory pressing
Fracture mechanism
Tensile strength
FGH4097 superalloys
url http://www.sciencedirect.com/science/article/pii/S2238785425001966
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