Rapid Synthesis of Dittmarite by Microwave-Assisted Hydrothermal Method
Dittmarite was obtained using MgO and (NH4)2HPO4 as raw materials via microwave-assisted hydrothermal method for 3 min at 120°C. The resulting samples were investigated by X-ray powder diffraction, scanning electron microscopy, Fourier transform infrared spectroscopy, and thermogravimetry-differenti...
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| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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Wiley
2012-01-01
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| Series: | Advances in Materials Science and Engineering |
| Online Access: | http://dx.doi.org/10.1155/2012/968396 |
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| _version_ | 1832552591740895232 |
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| author | Lai zhenyu Qian Jueshi Lu Zhongyuan Li Qian Zou Qiulin |
| author_facet | Lai zhenyu Qian Jueshi Lu Zhongyuan Li Qian Zou Qiulin |
| author_sort | Lai zhenyu |
| collection | DOAJ |
| description | Dittmarite was obtained using MgO and (NH4)2HPO4 as raw materials via microwave-assisted hydrothermal method for 3 min at 120°C. The resulting samples were investigated by X-ray powder diffraction, scanning electron microscopy, Fourier transform infrared spectroscopy, and thermogravimetry-differential thermal analysis. The results indicate that dittmarite can be rapidly synthesized by microwave-assisted hydrothermal method. With higher temperature and longer reaction time, highly crystallized dittmarite can be obtained. Pure dittmarite can be synthesized for 3 min at 120°C, which is faster than with the use of any other reported methods. |
| format | Article |
| id | doaj-art-c447068e55a947bd97a1eb6613fd9b58 |
| institution | Kabale University |
| issn | 1687-8434 1687-8442 |
| language | English |
| publishDate | 2012-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | Advances in Materials Science and Engineering |
| spelling | doaj-art-c447068e55a947bd97a1eb6613fd9b582025-02-03T05:58:19ZengWileyAdvances in Materials Science and Engineering1687-84341687-84422012-01-01201210.1155/2012/968396968396Rapid Synthesis of Dittmarite by Microwave-Assisted Hydrothermal MethodLai zhenyu0Qian Jueshi1Lu Zhongyuan2Li Qian3Zou Qiulin4School of Materials Science and Engineering, Southwest University of Science and Technology, Sichuan, Mianyang 621010, ChinaSchool of Materials Science and Engineering, Chongqing University, Chongqing 400030, ChinaSchool of Materials Science and Engineering, Southwest University of Science and Technology, Sichuan, Mianyang 621010, ChinaSchool of Materials Science and Engineering, Southwest University of Science and Technology, Sichuan, Mianyang 621010, ChinaSchool of Materials Science and Engineering, Southwest University of Science and Technology, Sichuan, Mianyang 621010, ChinaDittmarite was obtained using MgO and (NH4)2HPO4 as raw materials via microwave-assisted hydrothermal method for 3 min at 120°C. The resulting samples were investigated by X-ray powder diffraction, scanning electron microscopy, Fourier transform infrared spectroscopy, and thermogravimetry-differential thermal analysis. The results indicate that dittmarite can be rapidly synthesized by microwave-assisted hydrothermal method. With higher temperature and longer reaction time, highly crystallized dittmarite can be obtained. Pure dittmarite can be synthesized for 3 min at 120°C, which is faster than with the use of any other reported methods.http://dx.doi.org/10.1155/2012/968396 |
| spellingShingle | Lai zhenyu Qian Jueshi Lu Zhongyuan Li Qian Zou Qiulin Rapid Synthesis of Dittmarite by Microwave-Assisted Hydrothermal Method Advances in Materials Science and Engineering |
| title | Rapid Synthesis of Dittmarite by Microwave-Assisted Hydrothermal Method |
| title_full | Rapid Synthesis of Dittmarite by Microwave-Assisted Hydrothermal Method |
| title_fullStr | Rapid Synthesis of Dittmarite by Microwave-Assisted Hydrothermal Method |
| title_full_unstemmed | Rapid Synthesis of Dittmarite by Microwave-Assisted Hydrothermal Method |
| title_short | Rapid Synthesis of Dittmarite by Microwave-Assisted Hydrothermal Method |
| title_sort | rapid synthesis of dittmarite by microwave assisted hydrothermal method |
| url | http://dx.doi.org/10.1155/2012/968396 |
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