An Efficient One-Pot Synthesis of 1,8-Dioxodecahydroacridines Using Silica-Supported Polyphosphoric Acid (PPA-SiO2) under Solvent-Free Conditions

Silica gel–supported polyphosphoric acid (PPA-SiO2) was found to be an efficient catalyst for the synthesis of 1,8-dioxodecahydroacridines via one-pot three-component condensation of aryl aldehydes, dimedone, and ammonium acetate or 4-methyl aniline in high yields, easy workup procedure and short pe...

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Main Authors: Farid Moeinpour, Amir Khojastehnezhad
Format: Article
Language:English
Published: Wiley 2012-01-01
Series:E-Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2012/214231
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author Farid Moeinpour
Amir Khojastehnezhad
author_facet Farid Moeinpour
Amir Khojastehnezhad
author_sort Farid Moeinpour
collection DOAJ
description Silica gel–supported polyphosphoric acid (PPA-SiO2) was found to be an efficient catalyst for the synthesis of 1,8-dioxodecahydroacridines via one-pot three-component condensation of aryl aldehydes, dimedone, and ammonium acetate or 4-methyl aniline in high yields, easy workup procedure and short period of times. The catalyst was separated by simple filtration and used in the reaction three times without any significant loss of its activity.
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spelling doaj-art-bfc23d70813d4667887f1d4485c6cbaa2025-02-03T01:11:10ZengWileyE-Journal of Chemistry0973-49452090-98102012-01-019250450910.1155/2012/214231An Efficient One-Pot Synthesis of 1,8-Dioxodecahydroacridines Using Silica-Supported Polyphosphoric Acid (PPA-SiO2) under Solvent-Free ConditionsFarid Moeinpour0Amir Khojastehnezhad1Department of Chemistry, Islamic Azad University - Bandar Abbas Branch, Bandar Abbas 7915893144, IranDepartment of Chemistry, Islamic Azad University - Mashhad Branch, Mashhad, IranSilica gel–supported polyphosphoric acid (PPA-SiO2) was found to be an efficient catalyst for the synthesis of 1,8-dioxodecahydroacridines via one-pot three-component condensation of aryl aldehydes, dimedone, and ammonium acetate or 4-methyl aniline in high yields, easy workup procedure and short period of times. The catalyst was separated by simple filtration and used in the reaction three times without any significant loss of its activity.http://dx.doi.org/10.1155/2012/214231
spellingShingle Farid Moeinpour
Amir Khojastehnezhad
An Efficient One-Pot Synthesis of 1,8-Dioxodecahydroacridines Using Silica-Supported Polyphosphoric Acid (PPA-SiO2) under Solvent-Free Conditions
E-Journal of Chemistry
title An Efficient One-Pot Synthesis of 1,8-Dioxodecahydroacridines Using Silica-Supported Polyphosphoric Acid (PPA-SiO2) under Solvent-Free Conditions
title_full An Efficient One-Pot Synthesis of 1,8-Dioxodecahydroacridines Using Silica-Supported Polyphosphoric Acid (PPA-SiO2) under Solvent-Free Conditions
title_fullStr An Efficient One-Pot Synthesis of 1,8-Dioxodecahydroacridines Using Silica-Supported Polyphosphoric Acid (PPA-SiO2) under Solvent-Free Conditions
title_full_unstemmed An Efficient One-Pot Synthesis of 1,8-Dioxodecahydroacridines Using Silica-Supported Polyphosphoric Acid (PPA-SiO2) under Solvent-Free Conditions
title_short An Efficient One-Pot Synthesis of 1,8-Dioxodecahydroacridines Using Silica-Supported Polyphosphoric Acid (PPA-SiO2) under Solvent-Free Conditions
title_sort efficient one pot synthesis of 1 8 dioxodecahydroacridines using silica supported polyphosphoric acid ppa sio2 under solvent free conditions
url http://dx.doi.org/10.1155/2012/214231
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