Image registration for accurate electrode deformation analysis in operando microscopy of battery materials

Operando imaging techniques have become increasingly valuable in both battery research and manufacturing. However, the reliability of these methods can be compromised by instabilities in the imaging setup and operando cells, particularly when utilizing high-resolution imaging systems. The acquired i...

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Main Authors: Tianxiao Sun, Robert Peng, Wenlong Li, Yijin Liu
Format: Article
Language:English
Published: International Union of Crystallography 2025-03-01
Series:Journal of Synchrotron Radiation
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Online Access:https://journals.iucr.org/paper?S1600577524012293
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author Tianxiao Sun
Robert Peng
Wenlong Li
Yijin Liu
author_facet Tianxiao Sun
Robert Peng
Wenlong Li
Yijin Liu
author_sort Tianxiao Sun
collection DOAJ
description Operando imaging techniques have become increasingly valuable in both battery research and manufacturing. However, the reliability of these methods can be compromised by instabilities in the imaging setup and operando cells, particularly when utilizing high-resolution imaging systems. The acquired imaging data often include features arising from both undesirable system vibrations and drift, as well as the scientifically relevant deformations occurring in the battery sample during cell operation. For meaningful analysis, it is crucial to distinguish and separately evaluate these two factors. To address these challenges, we employ a suite of advanced image-processing techniques. These include fast Fourier transform analysis in the frequency domain, power spectrum-based assessments for image quality, as well as rigid and non-rigid image-registration methods. These techniques allow us to identify and exclude blurred images, correct for displacements caused by motor vibrations and sample holder drift and, thus, prevent unwanted image artifacts from affecting subsequent analyses and interpretations. Additionally, we apply optical flow analysis to track the dynamic deformation of battery electrode materials during electrochemical cycling. This enables us to observe and quantify the evolving mechanical responses of the electrodes, offering deeper insights into battery degradation. Together, these methods ensure more accurate image analysis and enhance our understanding of the chemomechanical interplay in battery performance and longevity.
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spelling doaj-art-b99cd3e9c9b74e1a91fbfef1cb5d5a302025-08-20T02:46:08ZengInternational Union of CrystallographyJournal of Synchrotron Radiation1600-57752025-03-0132241742310.1107/S1600577524012293gy5070Image registration for accurate electrode deformation analysis in operando microscopy of battery materialsTianxiao Sun0Robert Peng1Wenlong Li2Yijin Liu3Walker Department of Mechanical Engineering, The University of Texas at Austin, Austin, TX 78712, USAMcNeil High School, Austin, TX 78729, USAWalker Department of Mechanical Engineering, The University of Texas at Austin, Austin, TX 78712, USAWalker Department of Mechanical Engineering, The University of Texas at Austin, Austin, TX 78712, USAOperando imaging techniques have become increasingly valuable in both battery research and manufacturing. However, the reliability of these methods can be compromised by instabilities in the imaging setup and operando cells, particularly when utilizing high-resolution imaging systems. The acquired imaging data often include features arising from both undesirable system vibrations and drift, as well as the scientifically relevant deformations occurring in the battery sample during cell operation. For meaningful analysis, it is crucial to distinguish and separately evaluate these two factors. To address these challenges, we employ a suite of advanced image-processing techniques. These include fast Fourier transform analysis in the frequency domain, power spectrum-based assessments for image quality, as well as rigid and non-rigid image-registration methods. These techniques allow us to identify and exclude blurred images, correct for displacements caused by motor vibrations and sample holder drift and, thus, prevent unwanted image artifacts from affecting subsequent analyses and interpretations. Additionally, we apply optical flow analysis to track the dynamic deformation of battery electrode materials during electrochemical cycling. This enables us to observe and quantify the evolving mechanical responses of the electrodes, offering deeper insights into battery degradation. Together, these methods ensure more accurate image analysis and enhance our understanding of the chemomechanical interplay in battery performance and longevity.https://journals.iucr.org/paper?S1600577524012293operando imagingbattery degradationimage registrationoptical flow analysischemomechanical coupling
spellingShingle Tianxiao Sun
Robert Peng
Wenlong Li
Yijin Liu
Image registration for accurate electrode deformation analysis in operando microscopy of battery materials
Journal of Synchrotron Radiation
operando imaging
battery degradation
image registration
optical flow analysis
chemomechanical coupling
title Image registration for accurate electrode deformation analysis in operando microscopy of battery materials
title_full Image registration for accurate electrode deformation analysis in operando microscopy of battery materials
title_fullStr Image registration for accurate electrode deformation analysis in operando microscopy of battery materials
title_full_unstemmed Image registration for accurate electrode deformation analysis in operando microscopy of battery materials
title_short Image registration for accurate electrode deformation analysis in operando microscopy of battery materials
title_sort image registration for accurate electrode deformation analysis in operando microscopy of battery materials
topic operando imaging
battery degradation
image registration
optical flow analysis
chemomechanical coupling
url https://journals.iucr.org/paper?S1600577524012293
work_keys_str_mv AT tianxiaosun imageregistrationforaccurateelectrodedeformationanalysisinoperandomicroscopyofbatterymaterials
AT robertpeng imageregistrationforaccurateelectrodedeformationanalysisinoperandomicroscopyofbatterymaterials
AT wenlongli imageregistrationforaccurateelectrodedeformationanalysisinoperandomicroscopyofbatterymaterials
AT yijinliu imageregistrationforaccurateelectrodedeformationanalysisinoperandomicroscopyofbatterymaterials