Phase diagram prediction and particle characterization of Sn-Ag nano alloy for low melting point lead-free solders

SnAg nanoparticles (SnAg NPs) were prepared by wet synthesis. The chemical composition of the SnAg NPs was obtained by inductively coupled plasma - mass spectrometry. The prepared fine powder samples were characterized by electron microscopic technique (SEM) and thermal analysis (DSC). The nanopa...

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Main Authors: Sopousek J., Vrestal J., Zemanova A., Bursi J.
Format: Article
Language:English
Published: University of Belgrade, Technical Faculty, Bor 2012-01-01
Series:Journal of Mining and Metallurgy. Section B: Metallurgy
Online Access:http://www.doiserbia.nb.rs/img/doi/1450-5339/2012/1450-53391200032S.pdf
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author Sopousek J.
Vrestal J.
Zemanova A.
Bursi J.
author_facet Sopousek J.
Vrestal J.
Zemanova A.
Bursi J.
author_sort Sopousek J.
collection DOAJ
description SnAg nanoparticles (SnAg NPs) were prepared by wet synthesis. The chemical composition of the SnAg NPs was obtained by inductively coupled plasma - mass spectrometry. The prepared fine powder samples were characterized by electron microscopic technique (SEM) and thermal analysis (DSC). The nanoparticles with different size were obtained. The size dependent melting point depression (MPD) of the SnAg NPs was determined experimentally. The size dependent phase diagram of the SnAg alloy was also calculated using CALPHAD method, which has been extended to describe the surface energy of SnAg nanoparticles. The same approach was used for SnAg eutectic MPD calculations. The own experimental and theoretical results were compared with the data of the other authors. The satisfactory agreement was found.
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institution Kabale University
issn 1450-5339
language English
publishDate 2012-01-01
publisher University of Belgrade, Technical Faculty, Bor
record_format Article
series Journal of Mining and Metallurgy. Section B: Metallurgy
spelling doaj-art-b09c30e3c0044b168ceeabcff3038a3b2025-02-02T01:06:16ZengUniversity of Belgrade, Technical Faculty, BorJournal of Mining and Metallurgy. Section B: Metallurgy1450-53392012-01-0148341942510.2298/JMMB120121032SPhase diagram prediction and particle characterization of Sn-Ag nano alloy for low melting point lead-free soldersSopousek J.Vrestal J.Zemanova A.Bursi J.SnAg nanoparticles (SnAg NPs) were prepared by wet synthesis. The chemical composition of the SnAg NPs was obtained by inductively coupled plasma - mass spectrometry. The prepared fine powder samples were characterized by electron microscopic technique (SEM) and thermal analysis (DSC). The nanoparticles with different size were obtained. The size dependent melting point depression (MPD) of the SnAg NPs was determined experimentally. The size dependent phase diagram of the SnAg alloy was also calculated using CALPHAD method, which has been extended to describe the surface energy of SnAg nanoparticles. The same approach was used for SnAg eutectic MPD calculations. The own experimental and theoretical results were compared with the data of the other authors. The satisfactory agreement was found.http://www.doiserbia.nb.rs/img/doi/1450-5339/2012/1450-53391200032S.pdf
spellingShingle Sopousek J.
Vrestal J.
Zemanova A.
Bursi J.
Phase diagram prediction and particle characterization of Sn-Ag nano alloy for low melting point lead-free solders
Journal of Mining and Metallurgy. Section B: Metallurgy
title Phase diagram prediction and particle characterization of Sn-Ag nano alloy for low melting point lead-free solders
title_full Phase diagram prediction and particle characterization of Sn-Ag nano alloy for low melting point lead-free solders
title_fullStr Phase diagram prediction and particle characterization of Sn-Ag nano alloy for low melting point lead-free solders
title_full_unstemmed Phase diagram prediction and particle characterization of Sn-Ag nano alloy for low melting point lead-free solders
title_short Phase diagram prediction and particle characterization of Sn-Ag nano alloy for low melting point lead-free solders
title_sort phase diagram prediction and particle characterization of sn ag nano alloy for low melting point lead free solders
url http://www.doiserbia.nb.rs/img/doi/1450-5339/2012/1450-53391200032S.pdf
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AT vrestalj phasediagrampredictionandparticlecharacterizationofsnagnanoalloyforlowmeltingpointleadfreesolders
AT zemanovaa phasediagrampredictionandparticlecharacterizationofsnagnanoalloyforlowmeltingpointleadfreesolders
AT bursij phasediagrampredictionandparticlecharacterizationofsnagnanoalloyforlowmeltingpointleadfreesolders