A core-shell magnetic layered double hydroxide composite material for the effective decolorization of phenol red

The magnetic composite based on layered double hydroxide (Fe3O4/NiMn-LDH) was prepared by co-precipitation procedure and considered as a material to eliminate phenol red (PR) from aqueous environments. The characterization of Fe3O4/NiMn-LDH were recognized by Fourier transform infrared (FTIR) spectr...

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Main Author: Şakir Yılmaz
Format: Article
Language:English
Published: Kyrgyz Turkish Manas University 2022-06-01
Series:MANAS: Journal of Engineering
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Online Access:https://dergipark.org.tr/en/download/article-file/2294518
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author Şakir Yılmaz
author_facet Şakir Yılmaz
author_sort Şakir Yılmaz
collection DOAJ
description The magnetic composite based on layered double hydroxide (Fe3O4/NiMn-LDH) was prepared by co-precipitation procedure and considered as a material to eliminate phenol red (PR) from aqueous environments. The characterization of Fe3O4/NiMn-LDH were recognized by Fourier transform infrared (FTIR) spectroscopy and scanning electron microscopy (SEM). Box-Behnken design (BBD) under response surface methodology (RSM) were applied to evaluate the effects of the process variables such as pH, adsorbent dosage, and initial PR concentration (Co). The results indicated that a good correlation between the estimated and experimental values was found for the PR decolorization efficiency from aqueous media using Fe3O4/NiMn-LDH (R2 = 0.99). Furthermore, the statistical model obtained from BBD was sufficient to estimate the PR decolorization on Fe3O4/NiMn-LDH (p < 0.0001). The optimal conditions for the PR decolorization efficiency were determined as 5.38, 24.59 mg, and 25.39 mg/L for pH, adsorbent dosage, and Co, respectively which resulted in 86.93% the PR decolorization efficiency. Finally, this work demonstrated that BBD could easefully be utilized for the optimization of the PR decolorization using Fe3O4/NiMn-LDH.
format Article
id doaj-art-ada036d80f5d498b868cd259ea70ab78
institution Kabale University
issn 1694-7398
language English
publishDate 2022-06-01
publisher Kyrgyz Turkish Manas University
record_format Article
series MANAS: Journal of Engineering
spelling doaj-art-ada036d80f5d498b868cd259ea70ab782025-02-03T12:02:41ZengKyrgyz Turkish Manas UniversityMANAS: Journal of Engineering1694-73982022-06-01101889410.51354/mjen.10839831437A core-shell magnetic layered double hydroxide composite material for the effective decolorization of phenol redŞakir Yılmaz0https://orcid.org/0000-0001-9797-0959VAN YÜZÜNCÜ YIL ÜNİVERSİTESİ, MÜHENDİSLİK FAKÜLTESİ, MADEN MÜHENDİSLİĞİ BÖLÜMÜThe magnetic composite based on layered double hydroxide (Fe3O4/NiMn-LDH) was prepared by co-precipitation procedure and considered as a material to eliminate phenol red (PR) from aqueous environments. The characterization of Fe3O4/NiMn-LDH were recognized by Fourier transform infrared (FTIR) spectroscopy and scanning electron microscopy (SEM). Box-Behnken design (BBD) under response surface methodology (RSM) were applied to evaluate the effects of the process variables such as pH, adsorbent dosage, and initial PR concentration (Co). The results indicated that a good correlation between the estimated and experimental values was found for the PR decolorization efficiency from aqueous media using Fe3O4/NiMn-LDH (R2 = 0.99). Furthermore, the statistical model obtained from BBD was sufficient to estimate the PR decolorization on Fe3O4/NiMn-LDH (p < 0.0001). The optimal conditions for the PR decolorization efficiency were determined as 5.38, 24.59 mg, and 25.39 mg/L for pH, adsorbent dosage, and Co, respectively which resulted in 86.93% the PR decolorization efficiency. Finally, this work demonstrated that BBD could easefully be utilized for the optimization of the PR decolorization using Fe3O4/NiMn-LDH.https://dergipark.org.tr/en/download/article-file/2294518decolorizationlayered double hydroxidemagneticoptimizationphenol red
spellingShingle Şakir Yılmaz
A core-shell magnetic layered double hydroxide composite material for the effective decolorization of phenol red
MANAS: Journal of Engineering
decolorization
layered double hydroxide
magnetic
optimization
phenol red
title A core-shell magnetic layered double hydroxide composite material for the effective decolorization of phenol red
title_full A core-shell magnetic layered double hydroxide composite material for the effective decolorization of phenol red
title_fullStr A core-shell magnetic layered double hydroxide composite material for the effective decolorization of phenol red
title_full_unstemmed A core-shell magnetic layered double hydroxide composite material for the effective decolorization of phenol red
title_short A core-shell magnetic layered double hydroxide composite material for the effective decolorization of phenol red
title_sort core shell magnetic layered double hydroxide composite material for the effective decolorization of phenol red
topic decolorization
layered double hydroxide
magnetic
optimization
phenol red
url https://dergipark.org.tr/en/download/article-file/2294518
work_keys_str_mv AT sakiryılmaz acoreshellmagneticlayereddoublehydroxidecompositematerialfortheeffectivedecolorizationofphenolred
AT sakiryılmaz coreshellmagneticlayereddoublehydroxidecompositematerialfortheeffectivedecolorizationofphenolred