Enhancing biocomposite critical quality indicators (CQIs): the impact of biochar content in additive manufacturing

Abstract Biocomposite filaments for material extrusion (MEX) additive manufacturing, particularly those derived from agricultural biomass, have attracted significant research and industrial interest. Biochar is a well-documented reinforcement agent that is used in several polymeric matrices. However...

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Main Authors: Nectarios Vidakis, Markos Petousis, Dimitrios Sagris, Constantine David, Nikolaos Mountakis, Mariza Spiridaki, Emmanuel Maravelakis, Costas Charitidis, Emmanuel Stratakis
Format: Article
Language:English
Published: Springer 2025-01-01
Series:Biochar
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Online Access:https://doi.org/10.1007/s42773-024-00400-8
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author Nectarios Vidakis
Markos Petousis
Dimitrios Sagris
Constantine David
Nikolaos Mountakis
Mariza Spiridaki
Emmanuel Maravelakis
Costas Charitidis
Emmanuel Stratakis
author_facet Nectarios Vidakis
Markos Petousis
Dimitrios Sagris
Constantine David
Nikolaos Mountakis
Mariza Spiridaki
Emmanuel Maravelakis
Costas Charitidis
Emmanuel Stratakis
author_sort Nectarios Vidakis
collection DOAJ
description Abstract Biocomposite filaments for material extrusion (MEX) additive manufacturing, particularly those derived from agricultural biomass, have attracted significant research and industrial interest. Biochar is a well-documented reinforcement agent that is used in several polymeric matrices. However, systematic research efforts regarding the quality scores of parts built with MEX 3D printing with biochar-based filaments are marginal. Herein, the impact of biochar loading on the quality metrics of the five most popular polymers for MEX 3D printing (ABS, HDPE, PETG, PP, and PLA) is quantitatively examined in depth. Sophisticated and massive Non-Destructive Tests (NDTs) were conducted, and the impact of biochar loading on the critical quality indicators (CQIs), including porosity, dimensional conformity, and surface roughness, was documented. The quality scores for the biochar filler loading, also five in total, were statistically correlated with the corresponding reinforcement metrics for the five polymeric matrices. A statistically significant antagonistic interaction between the tensile strength course and porosity/dimensional deviation metrics, particularly for PETG, was observed. It can be concluded that the lowest porosity and dimensional deviation are associated with the highest strength. The 4 wt% biocomposite exhibited optimal quality performance in most polymers studied. Graphical abstract
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spelling doaj-art-ad247cc1bc8844bca88ae989f7f55f1c2025-01-26T12:46:12ZengSpringerBiochar2524-78672025-01-017111810.1007/s42773-024-00400-8Enhancing biocomposite critical quality indicators (CQIs): the impact of biochar content in additive manufacturingNectarios Vidakis0Markos Petousis1Dimitrios Sagris2Constantine David3Nikolaos Mountakis4Mariza Spiridaki5Emmanuel Maravelakis6Costas Charitidis7Emmanuel Stratakis8Department of Mechanical Engineering, Hellenic Mediterranean UniversityDepartment of Mechanical Engineering, Hellenic Mediterranean UniversityDepartment of Mechanical Engineering, International Hellenic UniversityDepartment of Mechanical Engineering, International Hellenic UniversityDepartment of Mechanical Engineering, Hellenic Mediterranean UniversityDepartment of Mechanical Engineering, Hellenic Mediterranean UniversityDepartment of Electronic Engineering, Hellenic Mediterranean UniversityDepartment of Materials Science and Engineering, School of Chemical Engineering NTUA, National Technical UniversityFoundation for Research and Technology-Hellas (FO.R.T.H)Abstract Biocomposite filaments for material extrusion (MEX) additive manufacturing, particularly those derived from agricultural biomass, have attracted significant research and industrial interest. Biochar is a well-documented reinforcement agent that is used in several polymeric matrices. However, systematic research efforts regarding the quality scores of parts built with MEX 3D printing with biochar-based filaments are marginal. Herein, the impact of biochar loading on the quality metrics of the five most popular polymers for MEX 3D printing (ABS, HDPE, PETG, PP, and PLA) is quantitatively examined in depth. Sophisticated and massive Non-Destructive Tests (NDTs) were conducted, and the impact of biochar loading on the critical quality indicators (CQIs), including porosity, dimensional conformity, and surface roughness, was documented. The quality scores for the biochar filler loading, also five in total, were statistically correlated with the corresponding reinforcement metrics for the five polymeric matrices. A statistically significant antagonistic interaction between the tensile strength course and porosity/dimensional deviation metrics, particularly for PETG, was observed. It can be concluded that the lowest porosity and dimensional deviation are associated with the highest strength. The 4 wt% biocomposite exhibited optimal quality performance in most polymers studied. Graphical abstracthttps://doi.org/10.1007/s42773-024-00400-83D printingBiocharPolymersMaterial extrusion (MEX)Micro-computed tomography (µ-CT)Atomic force microscopy (AFM)
spellingShingle Nectarios Vidakis
Markos Petousis
Dimitrios Sagris
Constantine David
Nikolaos Mountakis
Mariza Spiridaki
Emmanuel Maravelakis
Costas Charitidis
Emmanuel Stratakis
Enhancing biocomposite critical quality indicators (CQIs): the impact of biochar content in additive manufacturing
Biochar
3D printing
Biochar
Polymers
Material extrusion (MEX)
Micro-computed tomography (µ-CT)
Atomic force microscopy (AFM)
title Enhancing biocomposite critical quality indicators (CQIs): the impact of biochar content in additive manufacturing
title_full Enhancing biocomposite critical quality indicators (CQIs): the impact of biochar content in additive manufacturing
title_fullStr Enhancing biocomposite critical quality indicators (CQIs): the impact of biochar content in additive manufacturing
title_full_unstemmed Enhancing biocomposite critical quality indicators (CQIs): the impact of biochar content in additive manufacturing
title_short Enhancing biocomposite critical quality indicators (CQIs): the impact of biochar content in additive manufacturing
title_sort enhancing biocomposite critical quality indicators cqis the impact of biochar content in additive manufacturing
topic 3D printing
Biochar
Polymers
Material extrusion (MEX)
Micro-computed tomography (µ-CT)
Atomic force microscopy (AFM)
url https://doi.org/10.1007/s42773-024-00400-8
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