RSM-, ANN-, and GA-Based Process Optimization for Acid Centrifugation Treatment of Cane Molasses Toward Mitigating Calcium Oxide Fouling in Ethanol Plant Heat Exchanger

In the present investigation, process parameters were optimized in order to enhance the reduction of calcium oxide (CaO) from sugarcane molasses using acid centrifugation treatment. To predict the effects of process factors on CaO reduction efficiency, a response surface approach with a central comp...

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Main Authors: Lata Deso Abo, Sintayehu Mekuria Hailegiorgis, Mani Jayakumar, Sundramurthy Venkatesa Prabhu, Gadissa Tokuma Gindaba, Abas Siraj Hamda, B. S. Naveen Prasad
Format: Article
Language:English
Published: Wiley 2024-01-01
Series:International Journal of Chemical Engineering
Online Access:http://dx.doi.org/10.1155/2024/2744213
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author Lata Deso Abo
Sintayehu Mekuria Hailegiorgis
Mani Jayakumar
Sundramurthy Venkatesa Prabhu
Gadissa Tokuma Gindaba
Abas Siraj Hamda
B. S. Naveen Prasad
author_facet Lata Deso Abo
Sintayehu Mekuria Hailegiorgis
Mani Jayakumar
Sundramurthy Venkatesa Prabhu
Gadissa Tokuma Gindaba
Abas Siraj Hamda
B. S. Naveen Prasad
author_sort Lata Deso Abo
collection DOAJ
description In the present investigation, process parameters were optimized in order to enhance the reduction of calcium oxide (CaO) from sugarcane molasses using acid centrifugation treatment. To predict the effects of process factors on CaO reduction efficiency, a response surface approach with a central composite design was selected. The polynomial quadratic equation was used to predict CaO removal efficiency, and the analysis of variance (ANOVA) test was utilized to assess the relevance of process factors. The appropriateness of the developed model was determined by regression analysis, which yielded a higher R-squared value of 0.99334 ± 0.01. At the optimum process parameters of 100°C temperature, 50°Bx, and 3.50 pH, the CaO clarification efficacy of 66.17 wt.% was achieved. The experimental results indicated that for acidic centrifugation treatment, the experimentally observed CaO reduction of 65.94 wt% is in close agreement with the model equation’s predicted maximum CaO reduction of 66.17 wt% with a t-test value of 0.497726. Under such conditions, 0.982 wt.% CaO sugarcane molasses was obtained, which is low when compared to the world average of 1.5% CaO content of sugarcane molasses. Furthermore, the implementation of an artificial neural network (ANN) provided a better prediction model for CaO reduction, with a substantial R-squared value of 0.99866. However, the genetic algorithm (GA) optimization resulted in an actual CaO reduction of 66.21 wt.% with a t-test value of 0.497726.
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spelling doaj-art-a7ae1a7025d74c01893de56d4d7d052d2025-02-03T06:10:21ZengWileyInternational Journal of Chemical Engineering1687-80782024-01-01202410.1155/2024/2744213RSM-, ANN-, and GA-Based Process Optimization for Acid Centrifugation Treatment of Cane Molasses Toward Mitigating Calcium Oxide Fouling in Ethanol Plant Heat ExchangerLata Deso Abo0Sintayehu Mekuria Hailegiorgis1Mani Jayakumar2Sundramurthy Venkatesa Prabhu3Gadissa Tokuma Gindaba4Abas Siraj Hamda5B. S. Naveen Prasad6Department of Chemical EngineeringDepartment of Chemical EngineeringDepartment of Chemical EngineeringCentre for Natural Products and Functional FoodsDepartment of Chemical EngineeringDepartment of Chemical EngineeringChemical Engineering Section, Engineering DepartmentIn the present investigation, process parameters were optimized in order to enhance the reduction of calcium oxide (CaO) from sugarcane molasses using acid centrifugation treatment. To predict the effects of process factors on CaO reduction efficiency, a response surface approach with a central composite design was selected. The polynomial quadratic equation was used to predict CaO removal efficiency, and the analysis of variance (ANOVA) test was utilized to assess the relevance of process factors. The appropriateness of the developed model was determined by regression analysis, which yielded a higher R-squared value of 0.99334 ± 0.01. At the optimum process parameters of 100°C temperature, 50°Bx, and 3.50 pH, the CaO clarification efficacy of 66.17 wt.% was achieved. The experimental results indicated that for acidic centrifugation treatment, the experimentally observed CaO reduction of 65.94 wt% is in close agreement with the model equation’s predicted maximum CaO reduction of 66.17 wt% with a t-test value of 0.497726. Under such conditions, 0.982 wt.% CaO sugarcane molasses was obtained, which is low when compared to the world average of 1.5% CaO content of sugarcane molasses. Furthermore, the implementation of an artificial neural network (ANN) provided a better prediction model for CaO reduction, with a substantial R-squared value of 0.99866. However, the genetic algorithm (GA) optimization resulted in an actual CaO reduction of 66.21 wt.% with a t-test value of 0.497726.http://dx.doi.org/10.1155/2024/2744213
spellingShingle Lata Deso Abo
Sintayehu Mekuria Hailegiorgis
Mani Jayakumar
Sundramurthy Venkatesa Prabhu
Gadissa Tokuma Gindaba
Abas Siraj Hamda
B. S. Naveen Prasad
RSM-, ANN-, and GA-Based Process Optimization for Acid Centrifugation Treatment of Cane Molasses Toward Mitigating Calcium Oxide Fouling in Ethanol Plant Heat Exchanger
International Journal of Chemical Engineering
title RSM-, ANN-, and GA-Based Process Optimization for Acid Centrifugation Treatment of Cane Molasses Toward Mitigating Calcium Oxide Fouling in Ethanol Plant Heat Exchanger
title_full RSM-, ANN-, and GA-Based Process Optimization for Acid Centrifugation Treatment of Cane Molasses Toward Mitigating Calcium Oxide Fouling in Ethanol Plant Heat Exchanger
title_fullStr RSM-, ANN-, and GA-Based Process Optimization for Acid Centrifugation Treatment of Cane Molasses Toward Mitigating Calcium Oxide Fouling in Ethanol Plant Heat Exchanger
title_full_unstemmed RSM-, ANN-, and GA-Based Process Optimization for Acid Centrifugation Treatment of Cane Molasses Toward Mitigating Calcium Oxide Fouling in Ethanol Plant Heat Exchanger
title_short RSM-, ANN-, and GA-Based Process Optimization for Acid Centrifugation Treatment of Cane Molasses Toward Mitigating Calcium Oxide Fouling in Ethanol Plant Heat Exchanger
title_sort rsm ann and ga based process optimization for acid centrifugation treatment of cane molasses toward mitigating calcium oxide fouling in ethanol plant heat exchanger
url http://dx.doi.org/10.1155/2024/2744213
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