Mechanical properties of modern restorative “bioactive” dental materials - an in vitro study

Abstract This study aimed at assessing the mechanical properties and degradation of commercial bioactive materials. The bioactive materials (Activa Bioactive Restorative, Beautifil Flow Plus F00, F03, Predicta Bulk Bioactive) and composite resin Filtek Supreme Flow were submitted to flexural and dia...

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Main Authors: Mateusz Radwanski, Ewa Zmyslowska-Polakowska, Karolina Osica, Michal Krasowski, Salvatore Sauro, Louis Hardan, Monika Lukomska-Szymanska
Format: Article
Language:English
Published: Nature Portfolio 2025-01-01
Series:Scientific Reports
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Online Access:https://doi.org/10.1038/s41598-025-86595-7
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author Mateusz Radwanski
Ewa Zmyslowska-Polakowska
Karolina Osica
Michal Krasowski
Salvatore Sauro
Louis Hardan
Monika Lukomska-Szymanska
author_facet Mateusz Radwanski
Ewa Zmyslowska-Polakowska
Karolina Osica
Michal Krasowski
Salvatore Sauro
Louis Hardan
Monika Lukomska-Szymanska
author_sort Mateusz Radwanski
collection DOAJ
description Abstract This study aimed at assessing the mechanical properties and degradation of commercial bioactive materials. The bioactive materials (Activa Bioactive Restorative, Beautifil Flow Plus F00, F03, Predicta Bulk Bioactive) and composite resin Filtek Supreme Flow were submitted to flexural and diametral tensile strength tests (FS, DTS), modulus of elasticity (ME) evaluation, and analysis of aging in 70% ethanol and saliva on their hardness and sorption. The results for DTS ranged from 33.16 MPa (Beautifil Flow Plus F03) to 47.74 MPa (Filtek Supreme Flow). The highest FS was 120.40 MPa (Predicta Bulk Bioactive), while the lowest values were 86.55 MPa (Activa Bioactive Restorative). Activa Bioactive Restorative showed the lowest ME, as well as the highest water sorption both in alcohol and artificial saliva. Moreover, aging in saliva induced a significant decrease in hardness for Activa Restorative (p < .01). Alcohol storage caused a significant decrease in hardness for all materials (p < .0001). All tested materials met the basic requirements for light-curing materials in terms of DTS and FS. However, all materials showed higher sorption in alcohol than in saliva, while hardness decreased significantly after 30 days. Predicta Bulk Bioactive presented the highest mechanical parameters, initial hardness, and the lowest sorption of alcohol and saliva.
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spelling doaj-art-a72bc444692c4e7b9aa7196c7a7e674a2025-02-02T12:17:56ZengNature PortfolioScientific Reports2045-23222025-01-0115111310.1038/s41598-025-86595-7Mechanical properties of modern restorative “bioactive” dental materials - an in vitro studyMateusz Radwanski0Ewa Zmyslowska-Polakowska1Karolina Osica2Michal Krasowski3Salvatore Sauro4Louis Hardan5Monika Lukomska-Szymanska6Department of Endodontics, Medical University of LodzDepartment of Endodontics, Medical University of LodzDepartment of General Dentistry, Medical University of LodzMaterial Science Laboratory, Medical University of LodzDental Biomaterials and Minimally Invasive Dentistry, Departamento de Odontología, Facultad de Ciencias de la Salud, Universidad CEU-Cardenal HerreraDepartment of Restorative Dentistry, School of Dentistry, Saint-Joseph UniversityDepartment of General Dentistry, Medical University of LodzAbstract This study aimed at assessing the mechanical properties and degradation of commercial bioactive materials. The bioactive materials (Activa Bioactive Restorative, Beautifil Flow Plus F00, F03, Predicta Bulk Bioactive) and composite resin Filtek Supreme Flow were submitted to flexural and diametral tensile strength tests (FS, DTS), modulus of elasticity (ME) evaluation, and analysis of aging in 70% ethanol and saliva on their hardness and sorption. The results for DTS ranged from 33.16 MPa (Beautifil Flow Plus F03) to 47.74 MPa (Filtek Supreme Flow). The highest FS was 120.40 MPa (Predicta Bulk Bioactive), while the lowest values were 86.55 MPa (Activa Bioactive Restorative). Activa Bioactive Restorative showed the lowest ME, as well as the highest water sorption both in alcohol and artificial saliva. Moreover, aging in saliva induced a significant decrease in hardness for Activa Restorative (p < .01). Alcohol storage caused a significant decrease in hardness for all materials (p < .0001). All tested materials met the basic requirements for light-curing materials in terms of DTS and FS. However, all materials showed higher sorption in alcohol than in saliva, while hardness decreased significantly after 30 days. Predicta Bulk Bioactive presented the highest mechanical parameters, initial hardness, and the lowest sorption of alcohol and saliva.https://doi.org/10.1038/s41598-025-86595-7Bioactive materialsFlexural strengthHardnessMechanical propertiesModulus of elasticitySorption
spellingShingle Mateusz Radwanski
Ewa Zmyslowska-Polakowska
Karolina Osica
Michal Krasowski
Salvatore Sauro
Louis Hardan
Monika Lukomska-Szymanska
Mechanical properties of modern restorative “bioactive” dental materials - an in vitro study
Scientific Reports
Bioactive materials
Flexural strength
Hardness
Mechanical properties
Modulus of elasticity
Sorption
title Mechanical properties of modern restorative “bioactive” dental materials - an in vitro study
title_full Mechanical properties of modern restorative “bioactive” dental materials - an in vitro study
title_fullStr Mechanical properties of modern restorative “bioactive” dental materials - an in vitro study
title_full_unstemmed Mechanical properties of modern restorative “bioactive” dental materials - an in vitro study
title_short Mechanical properties of modern restorative “bioactive” dental materials - an in vitro study
title_sort mechanical properties of modern restorative bioactive dental materials an in vitro study
topic Bioactive materials
Flexural strength
Hardness
Mechanical properties
Modulus of elasticity
Sorption
url https://doi.org/10.1038/s41598-025-86595-7
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