The influence of morphology and crystal orientation of spangles on hot-dip Zn-0.5Sn alloy coating
The study on the surface morphology and crystal orientation of the Zn-0.5Sn coating could offer some guidance to improve the surface performance of the hot-dip galvanizing coating. In this paper, a scanning electron microscope (SEM) and an energy dispersive spectrometer (EDS) were used to analyze th...
Saved in:
Main Authors: | , , , , , |
---|---|
Format: | Article |
Language: | English |
Published: |
University of Belgrade, Technical Faculty, Bor
2021-01-01
|
Series: | Journal of Mining and Metallurgy. Section B: Metallurgy |
Subjects: | |
Online Access: | http://www.doiserbia.nb.rs/img/doi/1450-5339/2021/1450-53392100004Z.pdf |
Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
_version_ | 1832569409220116480 |
---|---|
author | Zhai L. Peng H -P. Liu Y. Lei Y. Deng S. Su X.-P. |
author_facet | Zhai L. Peng H -P. Liu Y. Lei Y. Deng S. Su X.-P. |
author_sort | Zhai L. |
collection | DOAJ |
description | The study on the surface morphology and crystal orientation of the Zn-0.5Sn coating could offer some guidance to improve the surface performance of the hot-dip galvanizing coating. In this paper, a scanning electron microscope (SEM) and an energy dispersive spectrometer (EDS) were used to analyze the typical morphology and the element distribution of spangles. The surface texture of the coating was analyzed by X-ray diffraction (XRD). Electron backscatter diffraction (EBSD) was used to analyze the crystal orientation of spangles. The results show that Sn segregates among the spangle dendrites while a metastable divorced eutectic structure can be maintained in the tin-rich phase, where the composition tends to be very similar. The crystal orientation of spangles affects their morphology, leading to the formation of feathery, ridged, and orthogonal dendrite arm spangles. When the angle among the <0001> orientation of the spangle crystal and the normal of the steel base surface changes from 0° to 90°, feathery spangles change to orthogonal dendrite arms spangles. The misorientation within a spangle is small while that among spangles is quite large. The orientation changes in the direction of the dendrite arm are relatively smooth and low, while the orientation changes which are perpendicular to the dendrite arm have a saltatory and irregular fluctuation. |
format | Article |
id | doaj-art-a3d3e1561e0a40718d42a9c5e7c475b3 |
institution | Kabale University |
issn | 1450-5339 2217-7175 |
language | English |
publishDate | 2021-01-01 |
publisher | University of Belgrade, Technical Faculty, Bor |
record_format | Article |
series | Journal of Mining and Metallurgy. Section B: Metallurgy |
spelling | doaj-art-a3d3e1561e0a40718d42a9c5e7c475b32025-02-02T21:41:38ZengUniversity of Belgrade, Technical Faculty, BorJournal of Mining and Metallurgy. Section B: Metallurgy1450-53392217-71752021-01-01571637210.2298/JMMB200726004Z1450-53392100004ZThe influence of morphology and crystal orientation of spangles on hot-dip Zn-0.5Sn alloy coatingZhai L.0Peng H -P.1Liu Y.2Lei Y.3Deng S.4Su X.-P.5Jiangsu Key Laboratory of Oil & Gas Storage and Transportation Technology, Changzhou University, Jiangsu, P.R. ChinaJiangsu Key Laboratory of Material surface Science and technology, Changzhou University, Jiangsu, P.R. China + Jiangsu Key Laboratory of Oil & Gas Storage and Transportation Technology, Changzhou University, Jiangsu, P.R. China + Jiangsu Collaborative Innovation Center of Photovoltaic Science and Engineering, Changzhou University, Jiangsu, P.R. ChinaJiangsu Key Laboratory of Material surface Science and technology, Changzhou University, Jiangsu, P.R. China + Jiangsu Collaborative Innovation Center of Photovoltaic Science and Engineering, Changzhou University, Jiangsu, P.R. ChinaJiangsu Key Laboratory of Oil & Gas Storage and Transportation Technology, Changzhou University, Jiangsu, P.R. ChinaJiangsu Key Laboratory of Oil & Gas Storage and Transportation Technology, Changzhou University, Jiangsu, P.R. ChinaJiangsu Key Laboratory of Material surface Science and technology, Changzhou University, Jiangsu, P.R. China + Jiangsu Collaborative Innovation Center of Photovoltaic Science and Engineering, Changzhou University, Jiangsu, P.R. ChinaThe study on the surface morphology and crystal orientation of the Zn-0.5Sn coating could offer some guidance to improve the surface performance of the hot-dip galvanizing coating. In this paper, a scanning electron microscope (SEM) and an energy dispersive spectrometer (EDS) were used to analyze the typical morphology and the element distribution of spangles. The surface texture of the coating was analyzed by X-ray diffraction (XRD). Electron backscatter diffraction (EBSD) was used to analyze the crystal orientation of spangles. The results show that Sn segregates among the spangle dendrites while a metastable divorced eutectic structure can be maintained in the tin-rich phase, where the composition tends to be very similar. The crystal orientation of spangles affects their morphology, leading to the formation of feathery, ridged, and orthogonal dendrite arm spangles. When the angle among the <0001> orientation of the spangle crystal and the normal of the steel base surface changes from 0° to 90°, feathery spangles change to orthogonal dendrite arms spangles. The misorientation within a spangle is small while that among spangles is quite large. The orientation changes in the direction of the dendrite arm are relatively smooth and low, while the orientation changes which are perpendicular to the dendrite arm have a saltatory and irregular fluctuation.http://www.doiserbia.nb.rs/img/doi/1450-5339/2021/1450-53392100004Z.pdfhot-dip galvanizingspanglecrystal orientationbackscattered electron diffraction |
spellingShingle | Zhai L. Peng H -P. Liu Y. Lei Y. Deng S. Su X.-P. The influence of morphology and crystal orientation of spangles on hot-dip Zn-0.5Sn alloy coating Journal of Mining and Metallurgy. Section B: Metallurgy hot-dip galvanizing spangle crystal orientation backscattered electron diffraction |
title | The influence of morphology and crystal orientation of spangles on hot-dip Zn-0.5Sn alloy coating |
title_full | The influence of morphology and crystal orientation of spangles on hot-dip Zn-0.5Sn alloy coating |
title_fullStr | The influence of morphology and crystal orientation of spangles on hot-dip Zn-0.5Sn alloy coating |
title_full_unstemmed | The influence of morphology and crystal orientation of spangles on hot-dip Zn-0.5Sn alloy coating |
title_short | The influence of morphology and crystal orientation of spangles on hot-dip Zn-0.5Sn alloy coating |
title_sort | influence of morphology and crystal orientation of spangles on hot dip zn 0 5sn alloy coating |
topic | hot-dip galvanizing spangle crystal orientation backscattered electron diffraction |
url | http://www.doiserbia.nb.rs/img/doi/1450-5339/2021/1450-53392100004Z.pdf |
work_keys_str_mv | AT zhail theinfluenceofmorphologyandcrystalorientationofspanglesonhotdipzn05snalloycoating AT penghp theinfluenceofmorphologyandcrystalorientationofspanglesonhotdipzn05snalloycoating AT liuy theinfluenceofmorphologyandcrystalorientationofspanglesonhotdipzn05snalloycoating AT leiy theinfluenceofmorphologyandcrystalorientationofspanglesonhotdipzn05snalloycoating AT dengs theinfluenceofmorphologyandcrystalorientationofspanglesonhotdipzn05snalloycoating AT suxp theinfluenceofmorphologyandcrystalorientationofspanglesonhotdipzn05snalloycoating AT zhail influenceofmorphologyandcrystalorientationofspanglesonhotdipzn05snalloycoating AT penghp influenceofmorphologyandcrystalorientationofspanglesonhotdipzn05snalloycoating AT liuy influenceofmorphologyandcrystalorientationofspanglesonhotdipzn05snalloycoating AT leiy influenceofmorphologyandcrystalorientationofspanglesonhotdipzn05snalloycoating AT dengs influenceofmorphologyandcrystalorientationofspanglesonhotdipzn05snalloycoating AT suxp influenceofmorphologyandcrystalorientationofspanglesonhotdipzn05snalloycoating |