Effect of Flaxseed Gum on the Microstructure and Physicochemical Properties of Starch in Frozen Dough
This study investigated the effects of adding different amounts of flaxseed gum (0%, 0.2%, 0.4%, 0.6% and 0.8%) on the microstructure and physicochemical properties of starch in frozen dough using scanning electron microscopy (SEM), solid-state nuclear magnetic resonance (SSNMR) spectroscopy, X-ray...
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China Food Publishing Company
2025-01-01
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Online Access: | https://www.spkx.net.cn/fileup/1002-6630/PDF/2025-46-2-008.pdf |
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author | WANG Hongwei, LI Xiangjie, QIAO Jingyue, SHEN Huishan, ZHANG Yanyan, LIU Xingli, ZHAO Xuewei, ZHANG Hua |
author_facet | WANG Hongwei, LI Xiangjie, QIAO Jingyue, SHEN Huishan, ZHANG Yanyan, LIU Xingli, ZHAO Xuewei, ZHANG Hua |
author_sort | WANG Hongwei, LI Xiangjie, QIAO Jingyue, SHEN Huishan, ZHANG Yanyan, LIU Xingli, ZHAO Xuewei, ZHANG Hua |
collection | DOAJ |
description | This study investigated the effects of adding different amounts of flaxseed gum (0%, 0.2%, 0.4%, 0.6% and 0.8%) on the microstructure and physicochemical properties of starch in frozen dough using scanning electron microscopy (SEM), solid-state nuclear magnetic resonance (SSNMR) spectroscopy, X-ray diffraction (XRD), and rapid visco analysis (RVA). The aim was to reveal the potential mechanism underlying the effect of flaxseed gum on the quality improvement of frozen dough from the perspective of changes in starch characteristics of frozen dough. The results showed that after repeated freeze-thaw cycles, the surface of starch particles appeared sunken, the relative crystallinity of starch decreased, the double helix structure of starch molecules was destroyed, and consequently water molecules were more likely to enter starch particles, thus resulting in an increase in peak viscosity and final viscosity. The addition of flaxseed gum inhibited the formation of ice crystals in frozen dough and delayed the unwinding of the double helix structure of starch molecules, and the hydrogen bond interaction between flaxseed gum and starch molecules increased the relative crystallinity of starch (22.2%–23.8%). As a result, the peak viscosity of starch decreased from 2 409.5 mPa⋅s to 2 247.2–2 288.5 mPa⋅s, and the gelatinization temperature gradually increased. In conclusion, flaxseed gum delayed the damage of starch in dough caused by repeated freeze-thaw cycles, thereby protecting frozen dough. |
format | Article |
id | doaj-art-9fa59000a96240f2ac30390e88c61008 |
institution | Kabale University |
issn | 1002-6630 |
language | English |
publishDate | 2025-01-01 |
publisher | China Food Publishing Company |
record_format | Article |
series | Shipin Kexue |
spelling | doaj-art-9fa59000a96240f2ac30390e88c610082025-02-05T09:08:22ZengChina Food Publishing CompanyShipin Kexue1002-66302025-01-01462657110.7506/spkx1002-6630-20240527-219Effect of Flaxseed Gum on the Microstructure and Physicochemical Properties of Starch in Frozen DoughWANG Hongwei, LI Xiangjie, QIAO Jingyue, SHEN Huishan, ZHANG Yanyan, LIU Xingli, ZHAO Xuewei, ZHANG Hua0(1. College of Food and Bioengineering, Zhengzhou University of Light Industry, Zhengzhou 450002, China; 2. Key Laboratory of Cold Chain Food Processing and Safety Control, Ministry of Education, Zhengzhou 450002, China; 3. Food Laboratory of Zhongyuan, Luohe 462300, China; 4. National &Local Joint Engineering Research Center of Cereal-Based Foods (Henan), Zhengzhou 450002, China)This study investigated the effects of adding different amounts of flaxseed gum (0%, 0.2%, 0.4%, 0.6% and 0.8%) on the microstructure and physicochemical properties of starch in frozen dough using scanning electron microscopy (SEM), solid-state nuclear magnetic resonance (SSNMR) spectroscopy, X-ray diffraction (XRD), and rapid visco analysis (RVA). The aim was to reveal the potential mechanism underlying the effect of flaxseed gum on the quality improvement of frozen dough from the perspective of changes in starch characteristics of frozen dough. The results showed that after repeated freeze-thaw cycles, the surface of starch particles appeared sunken, the relative crystallinity of starch decreased, the double helix structure of starch molecules was destroyed, and consequently water molecules were more likely to enter starch particles, thus resulting in an increase in peak viscosity and final viscosity. The addition of flaxseed gum inhibited the formation of ice crystals in frozen dough and delayed the unwinding of the double helix structure of starch molecules, and the hydrogen bond interaction between flaxseed gum and starch molecules increased the relative crystallinity of starch (22.2%–23.8%). As a result, the peak viscosity of starch decreased from 2 409.5 mPa⋅s to 2 247.2–2 288.5 mPa⋅s, and the gelatinization temperature gradually increased. In conclusion, flaxseed gum delayed the damage of starch in dough caused by repeated freeze-thaw cycles, thereby protecting frozen dough.https://www.spkx.net.cn/fileup/1002-6630/PDF/2025-46-2-008.pdfrepeated freeze-thaw cycles; starch; flaxseed gum; microstructure; physicochemical properties |
spellingShingle | WANG Hongwei, LI Xiangjie, QIAO Jingyue, SHEN Huishan, ZHANG Yanyan, LIU Xingli, ZHAO Xuewei, ZHANG Hua Effect of Flaxseed Gum on the Microstructure and Physicochemical Properties of Starch in Frozen Dough Shipin Kexue repeated freeze-thaw cycles; starch; flaxseed gum; microstructure; physicochemical properties |
title | Effect of Flaxseed Gum on the Microstructure and Physicochemical Properties of Starch in Frozen Dough |
title_full | Effect of Flaxseed Gum on the Microstructure and Physicochemical Properties of Starch in Frozen Dough |
title_fullStr | Effect of Flaxseed Gum on the Microstructure and Physicochemical Properties of Starch in Frozen Dough |
title_full_unstemmed | Effect of Flaxseed Gum on the Microstructure and Physicochemical Properties of Starch in Frozen Dough |
title_short | Effect of Flaxseed Gum on the Microstructure and Physicochemical Properties of Starch in Frozen Dough |
title_sort | effect of flaxseed gum on the microstructure and physicochemical properties of starch in frozen dough |
topic | repeated freeze-thaw cycles; starch; flaxseed gum; microstructure; physicochemical properties |
url | https://www.spkx.net.cn/fileup/1002-6630/PDF/2025-46-2-008.pdf |
work_keys_str_mv | AT wanghongweilixiangjieqiaojingyueshenhuishanzhangyanyanliuxinglizhaoxueweizhanghua effectofflaxseedgumonthemicrostructureandphysicochemicalpropertiesofstarchinfrozendough |