Determination of microstructural changes by severely plastically deformed copper-aluminum alloy: Optical study

Our work deals with the problem of producing a complex metal-ceramic composite using the processes of internal oxidation (IO) and severe plastic deformation. For this purpose, Cu-Al alloy with 0.4wt.% of Al was used. IO of sample serves in the first step of the processing as a means for att...

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Main Authors: Romčević N., Gilić M., Anžel I., Rudolf R., Mitrić M., Romčević M., Hadžić B., Joksimović D., Petrović-Damjanović M., Kos M.
Format: Article
Language:English
Published: University of Belgrade, Technical Faculty, Bor 2014-01-01
Series:Journal of Mining and Metallurgy. Section B: Metallurgy
Subjects:
Online Access:http://www.doiserbia.nb.rs/img/doi/1450-5339/2014/1450-53391400007R.pdf
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author Romčević N.
Gilić M.
Anžel I.
Rudolf R.
Mitrić M.
Romčević M.
Hadžić B.
Joksimović D.
Petrović-Damjanović M.
Kos M.
author_facet Romčević N.
Gilić M.
Anžel I.
Rudolf R.
Mitrić M.
Romčević M.
Hadžić B.
Joksimović D.
Petrović-Damjanović M.
Kos M.
author_sort Romčević N.
collection DOAJ
description Our work deals with the problem of producing a complex metal-ceramic composite using the processes of internal oxidation (IO) and severe plastic deformation. For this purpose, Cu-Al alloy with 0.4wt.% of Al was used. IO of sample serves in the first step of the processing as a means for attaining a fine dispersion of nanosized oxide particles in the metal matrix. Production technology continues with repeated application of severe plastic deformation (SPD) of the resulting metalmatrix composite to produce the bulk nanoscaled structural material. SPD was carried out with equal channel angular pressing (ECAP), which allowed that the material could be subjected to an intense plastic strain through simple shear. Microstructural characteristics of one phase and multiphase material was studied on internally oxidized Cu with 0.4wt.% of Al sample composed of one phase copper-aluminum solid solution in the core and fine dispersed oxide particles in the same matrix in the mantle region. In this manner AFM, X-ray diffraction and Raman spectroscopy were used. Local structures in plastically deformed samples reflect presence of Cu, CuO, Cu2O, Cu4O3 or Al2O3 structural characteristics, depending on type of sample. [Projekat Ministarstva nauke Republike Srbije, br. III45003]
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institution Kabale University
issn 1450-5339
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publishDate 2014-01-01
publisher University of Belgrade, Technical Faculty, Bor
record_format Article
series Journal of Mining and Metallurgy. Section B: Metallurgy
spelling doaj-art-9dfc1fd4763542c1be9809bfe03582212025-02-02T01:07:39ZengUniversity of Belgrade, Technical Faculty, BorJournal of Mining and Metallurgy. Section B: Metallurgy1450-53392014-01-01501616810.2298/JMMB140121007R1450-53391400007RDetermination of microstructural changes by severely plastically deformed copper-aluminum alloy: Optical studyRomčević N.0Gilić M.1Anžel I.2Rudolf R.3Mitrić M.4Romčević M.5Hadžić B.6Joksimović D.7Petrović-Damjanović M.8Kos M.9Institute of Physics, BelgradeInstitute of Physics, BelgradeUniversity of Maribor, Faculty of Mechanical Engineering, Maribor, SloveniaUniversity of Maribor, Faculty of Mechanical Engineering, Maribor, Slovenia + Zlatarna Celje d.d., Celje, SloveniaInstitute Vinca, BelgradeInstitute of Physics, BelgradeInstitute of Physics, BelgradeMegatrend University, BelgradeInstitute of Physics, BelgradeUniversity of Maribor, Faculty of Mechanical Engineering, Maribor, Slovenia + Sykofin d.o.o., Maribor, SloveniaOur work deals with the problem of producing a complex metal-ceramic composite using the processes of internal oxidation (IO) and severe plastic deformation. For this purpose, Cu-Al alloy with 0.4wt.% of Al was used. IO of sample serves in the first step of the processing as a means for attaining a fine dispersion of nanosized oxide particles in the metal matrix. Production technology continues with repeated application of severe plastic deformation (SPD) of the resulting metalmatrix composite to produce the bulk nanoscaled structural material. SPD was carried out with equal channel angular pressing (ECAP), which allowed that the material could be subjected to an intense plastic strain through simple shear. Microstructural characteristics of one phase and multiphase material was studied on internally oxidized Cu with 0.4wt.% of Al sample composed of one phase copper-aluminum solid solution in the core and fine dispersed oxide particles in the same matrix in the mantle region. In this manner AFM, X-ray diffraction and Raman spectroscopy were used. Local structures in plastically deformed samples reflect presence of Cu, CuO, Cu2O, Cu4O3 or Al2O3 structural characteristics, depending on type of sample. [Projekat Ministarstva nauke Republike Srbije, br. III45003]http://www.doiserbia.nb.rs/img/doi/1450-5339/2014/1450-53391400007R.pdfmetalsoxidesatomic force microscopyRaman spectroscopymicrostructure
spellingShingle Romčević N.
Gilić M.
Anžel I.
Rudolf R.
Mitrić M.
Romčević M.
Hadžić B.
Joksimović D.
Petrović-Damjanović M.
Kos M.
Determination of microstructural changes by severely plastically deformed copper-aluminum alloy: Optical study
Journal of Mining and Metallurgy. Section B: Metallurgy
metals
oxides
atomic force microscopy
Raman spectroscopy
microstructure
title Determination of microstructural changes by severely plastically deformed copper-aluminum alloy: Optical study
title_full Determination of microstructural changes by severely plastically deformed copper-aluminum alloy: Optical study
title_fullStr Determination of microstructural changes by severely plastically deformed copper-aluminum alloy: Optical study
title_full_unstemmed Determination of microstructural changes by severely plastically deformed copper-aluminum alloy: Optical study
title_short Determination of microstructural changes by severely plastically deformed copper-aluminum alloy: Optical study
title_sort determination of microstructural changes by severely plastically deformed copper aluminum alloy optical study
topic metals
oxides
atomic force microscopy
Raman spectroscopy
microstructure
url http://www.doiserbia.nb.rs/img/doi/1450-5339/2014/1450-53391400007R.pdf
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